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公开(公告)号：EP2668136A2
公开(公告)日：2013-12-04
申请号：EP12739986.3
申请日：2012-01-27
CPC分类号： C01G19/02 , C01P2006/80
摘要： Provided herein are methods for the preparation of high purity stannous oxide comprising: (a) reacting a Sn salt with a C2-12 dicarboxylic acid in the aqueous phase to form a suspension comprising a Sn-dicarboxylate complex; (b) washing the Sn-dicarboxylate complex with water to obtain a wash solution comprising a washed Sn-dicarboxylate complex essentially free of the anion of the Sn salt; and (c) reacting the washed Sn-dicarboxylate complex with a base to form high purity SnO, wherein the high purity SnO has an alpha radiation count of less than about 0.002 cph/cm2.
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公开(公告)号：EP2668136B1
公开(公告)日：2018-04-11
申请号：EP12739986.3
申请日：2012-01-27
CPC分类号： C01G19/02 , C01P2006/80
摘要： Provided herein are methods for the preparation of high purity stannous oxide comprising: (a) reacting a Sn salt with a C2-12 dicarboxylic acid in the aqueous phase to form a suspension comprising a Sn-dicarboxylate complex; (b) washing the Sn-dicarboxylate complex with water to obtain a wash solution comprising a washed Sn-dicarboxylate complex essentially free of the anion of the Sn salt; and (c) reacting the washed Sn-dicarboxylate complex with a base to form high purity SnO, wherein the high purity SnO has an alpha radiation count of less than about 0.002 cph/cm2.
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公开(公告)号：EP4440982A1
公开(公告)日：2024-10-09
申请号：EP22902358.5
申请日：2022-11-30
IPC分类号： C01B21/086
CPC分类号： Y02E60/10 , C01B21/086 , C01B21/093 , H01M10/0525 , H01M2300/002520130101 , H01M10/0567 , H01M10/0568
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公开(公告)号：EP1836184B1
公开(公告)日：2008-06-04
申请号：EP05855436.1
申请日：2005-12-22
IPC分类号： C07D333/06
CPC分类号： C07D333/06
摘要： A method for the formation of 3-alkylthiophenes or 3-arylthiophenes from 3--halothiophenes. More particularly, improvements on the Kumada coupling reaction for the production of 3-alkylthiophenes or 3- arylthiophenes by reacting a 3-hâlothiophene with an alkylmagnesiumhalide or arylmagnesiumhalide Grignard reagent in the presence of a catalyst and a 2-methyl tetrahydrofuran solvent. The 2-methyl tetrahydrofuran solvent allows for higher concentrations of the Grignard reagent with minimal or no dithienyl side product generation, achieving higher product yields and at a lower cost than other known methods.
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公开(公告)号：EP1836186A1
公开(公告)日：2007-09-26
申请号：EP05855005.4
申请日：2005-12-21
IPC分类号： C07D333/28
CPC分类号： C07D333/28
摘要： An improved process and catalyst system for the isomerization of halothiophenes. More particularly, an improved process for the isomerization of 2-halothiophenes to 3-halothiopenes by reacting a w-halothiophene with a catalyst and in the presence of a base. The addition of a base additive to the acidic zeolite catalyst allows the desired isomerization to take place while suppressing side-reactions that result in the decomposition of the thiophene rings. The catalyst lifetime is thus increased and the amount of catalyst needed for the reaction is reduced, lowering cost.
摘要翻译： 用于卤代噻吩异构化的改进方法和催化剂体系。 更具体地说，是一种改进的2-卤代噻吩异构化为3-卤代硫代环戊烯的方法，该方法是使一种间卤代噻吩与一种催化剂反应并在碱存在下反应。 向酸性沸石催化剂中添加碱添加剂可以实现所需的异构化反应，同时抑制导致噻吩环分解的副反应。 催化剂寿命因此增加并且反应所需的催化剂量减少，从而降低了成本。
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公开(公告)号：EP3341327A1
公开(公告)日：2018-07-04
申请号：EP16839974.9
申请日：2016-08-23
摘要： A method for preparing a fast-drying particulate hydroxyapatite composition includes the steps of reacting a calcium salt aqueous solution with a phosphate salt aqueous solution to obtain a product solution including hydroxyapatite particles in aqueous suspension and a dissolved byproduct salt; purifying the product solution by removing at least a portion of the dissolved byproduct salt to form a purified product; and dehydrating the purified product by diluting the purified product with a non-water fluid to form a diluted product in a water/non-water mixed solution and subsequently removing at least a portion of the water/non-water mixed solution to form a dehydrated product.
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7.发明公开HALOGENATED THIOPHENE MONOMER FOR THE PREPARATION OF REGIOREGULAR POLYTHIOPHENES 审中-公开卤代噻吩单体进行常规REGIO聚噻吩的制造
公开(公告)号：EP1836233A1
公开(公告)日：2007-09-26
申请号：EP05855516.0
申请日：2005-12-22
发明人： WERNER, Christian , HOYER, Susanne , GENNBURG, Wolfgang , KELLERMEIER, Bernd , KANSCHIK-CONRADSEN, Andreas
IPC分类号： C08G61/12
CPC分类号： C08G61/126
摘要： Conductive polymers and a method of forming conductive polymers. More particularly, a method of forming head-to-tail coupled regioregular poly-.(3-substituted) thiophenes having improved charge carrier mobility and current modulation. Also, monomers having two different halogen leaving groups and which form regioregular poly-(3-substituted) thiophenes more efficiently and economically than other processes. Polythiophene polymers, films and articles are also provided.
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公开(公告)号：EP1836184A1
公开(公告)日：2007-09-26
申请号：EP05855436.1
申请日：2005-12-22
IPC分类号： C07D333/06
CPC分类号： C07D333/06
摘要： A method for the formation of 3-alkylthiophenes or 3-arylthiophenes from 3--halothiophenes. More particularly, improvements on the Kumada coupling reaction for the production of 3-alkylthiophenes or 3- arylthiophenes by reacting a 3-hâlothiophene with an alkylmagnesiumhalide or arylmagnesiumhalide Grignard reagent in the presence of a catalyst and a 2-methyl tetrahydrofuran solvent. The 2-methyl tetrahydrofuran solvent allows for higher concentrations of the Grignard reagent with minimal or no dithienyl side product generation, achieving higher product yields and at a lower cost than other known methods.
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公开(公告)号：EP1463770A1
公开(公告)日：2004-10-06
申请号：EP03702017.9
申请日：2003-01-07
发明人： APEN, Paul, G. , ZHEREBIN, Ruslan , LI, Bo , KOROLEV, Boris, A. , LAU, Kreisler, S. , KANSCHIK-CONRADSEN, Andreas , KELLERMEIER, Bernd , DEMEL, Sonja , WERNER, Christian , SULLIVAN, Edward, J.
IPC分类号： C08G61/12
摘要： The present invention provides adamantane or diamantane compositions that are useful as a dielectric material in microelectronic applications such as microchips.
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公开(公告)号：EP1463770B1
公开(公告)日：2007-07-04
申请号：EP03702017.9
申请日：2003-01-07
发明人： APEN, Paul, G. , ZHEREBIN, Ruslan , LI, Bo , KOROLEV, Boris, A. , LAU, Kreisler, S. , KANSCHIK-CONRADSEN, Andreas , KELLERMEIER, Bernd , DEMEL, Sonja , WERNER, Christian , SULLIVAN, Edward, J.
IPC分类号： C08G61/12
摘要： The present invention provides adamantane or diamantane compositions that are useful as a dielectric material in microelectronic applications such as microchips.
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