摘要:
A fuel activation and energy release apparatus is provided for increasing energy output of a fluid substance. The apparatus comprises a fluidly sealable reactor chamber, adapted to withstand a predetermined fluid pressure and temperature; a fluid injection port, adapted to provide a one-way fluid communication from an external fluid reservoir to said reactor chamber; a fluid ejection port, adapted to provide a one-way fluid communication from said reactor chamber to an external region, so as to controllably release said fluid substance from said reactor chamber and at least one first electromagnetic radiation (EMR) waveguide. The first EMR waveguide having a first waveguide input port and a first waveguide output port, operably coupled within said reactor chamber and adapted to couple electromagnetic radiation of a predetermined first wavelength to a fluid substance injected into said reactor chamber.
摘要:
[PROBLEMS] To provide new means for arranging a flow route of a reaction object along a center axis in a waveguide for transmitting a waveguide and effectively and uniformly performing a chemical reaction or the like by the function of micro wave irradiation to the reaction object. [MEANS FOR SOLVING PROBLEMS] A micro wave chemical reaction device includes a square waveguide for transmitting a micro wave of TE10 mode or a circular waveguide for transmitting a micro wave of TM01 mode or TE01 mode, and a flow route insulated from the space in the waveguide by a partition wall of a low micro wave loss and arranged to extend substantially coaxially along the center axis of the waveguide. A reaction object to be chemically reacted is contained inside the flow route and the function of the micro wave is applied to the reaction object inside the flow route. Since the function of the micro wave continues over a long distance along the transmission direction, the micro wave can be effectively used.
摘要:
A vessel system for accelerating the solid phase synthesis of peptides comprises a vessel system for the accelerated synthesis of peptides by the solid phase method, said vessel system comprising: a reaction cell or vessel (45) that is transparent to microwave radiation; a first passageway (46) in fluid communication with said cell (45) for transferring solid phase resin between a resin source external to said cell and said cell; a second passageway (47) in fluid communication between at least one amino acid source and said cell (45) for adding amino acids to said cell; a third passageway (50) in gaseous communication with an inert gas source (70) and with a vent (71) for applying gas pressure to and releasing gas pressure from said cell (45) so that the controlled flow of gases to and from said cell can be used to add and remove fluids and flowing solids to and from said cell (45).
摘要:
The invention performs uniform chemical reactions with high efficiency by action of microwave onto reaction targets placed within a flow path along a center axis of a waveguide for transmission of microwave. The microwave chemical reaction device includes a circular waveguide for transmission of TM or TE mode microwave or a square waveguide for transmission of TE mode microwave and a flow path shielded from a space within the waveguide by a bulkhead of low microwave loss and coaxially extending along the center axis of the waveguide. Reaction targets to be subjected to chemical reactions are accommodated in the flow path and the microwave acts on the reaction targets within the flow path.
摘要:
An instrument and process for accelerating the solid phase synthesis of peptides is disclosed. The method includes the steps of deprotecting a protected first amino acid (10) linked to a solid phase resin (14) by admixing the protected linked acid (10) with a deprotecting solution in a microwave transparent vessel while irradiating the admixed acid and solution with microwaves, then activating a second amino acid (20) by adding the second acid (20) and an activating solution (22) to the same vessel while irradiating the vessel with microwaves, then coupling the second amino acid (20) to the first acid (10) while irradiating the composition in the same vessel with microwaves, and cleaving the linked peptide from the solid phase resin (14) by admixing the linked peptide with a cleaving composition in the same vessel while irradiating the composition with microwaves.
摘要:
There is described a microwave heating system, comprising a bowl, a dome adapted to be fit to the bowl, such that a volume is formed by the bowl and dome, and a rotor device adapted to support at least one reaction vessel and being rotatably supported by the bowl, the rotor device comprising a base plate comprising at least one through-hole, and at least one tubular member having a longitudinal axis and being adapted to receive a reaction vessel and to be coupled to the base plate in such a way that the longitudinal axis of the at least one tubular member passes through the at least one through-hole, wherein the base plate and the at least one tubular member comprise metal, and wherein the bowl is adapted to be connected to a microwave source, such that a microwave field can be supplied to the volume, whereby the microwave field is attenuated in a region between the rotor device and the dome compared to a region between the bowl and the rotor device.
摘要:
Provided is an information processing apparatus that can detect occurrence of an abnormality in a microwave irradiation apparatus, including: a supplied electric power value accepting unit 13 that accepts a supplied electric power value, which is a difference between an electric power value of microwaves incident on a microwave irradiation apparatus 2 and an electric power value of microwaves reflected by the microwave irradiation apparatus 2; a temperature accepting unit 15 that accepts a temperature of a content; an electric energy calculating unit 14 that calculates an electric energy corresponding to a microwave irradiation time, using the supplied electric power value; a temperature change calculating unit 16 that calculates a temperature change corresponding to the microwave irradiation time, using the accepted temperature; a judging unit 20 that, using the electric energy, the temperature change, and a relational expression for associating the electric energy and the temperature change, judges whether or not the relational expression is satisfied within a tolerable range by the electric energy and the temperature change; and an output unit 21 that performs output regarding occurrence of an abnormality, in a case where it is judged that the relational expression is not satisfied within the tolerable range by the electric energy and the temperature change.
摘要:
The present invention provides a chemical reaction apparatus that can efficiently irradiate a content with microwaves. The chemical reaction apparatus includes: a horizontal flow-type reactor 13 in which a content horizontally flows with an unfilled space being provided thereabove; a microwave generator 14 that generates microwaves; and at least one waveguide 15 that transmits the microwaves generated by the microwave generator 14 to the unfilled space in the reactor 13. In this manner, microwaves can be irradiated over a larger surface area, and the microwave irradiation efficiency increases.
摘要:
Die vorliegende Erfindung betrifft einen Druckbehälter (1) zur Aufnahme von zu beheizenden Proben (P), wobei der Druckbehälter (1) eine verschließbare Reaktionskammer (2) als Druckraum zum Auslösen und/oder Fördern chemischer und/oder physikalischer Druckreaktionen aufweist, und wobei der Druckbehälter (1) eine Koppelöffnung sowie einen Mikrowellen-durchlässigen Bereich (80) zwischen der Koppelöffnung (K) und der Reaktionskammer (2) aufweist, über die Mikrowellen in die Reaktionskammer (2) eingekoppelt werden können. Der Mikrowellen-durchlässigen Bereich (80) weist ein Druckaufnahmeteil (71) auf, um den Druck der Reaktionskammer (2) gegenüber der Koppelöffnung (K) abzustützen. Der Mikrowellen-durchlässigen Bereich (80) weist alternativ ein Druckaufnahmeteil (71) aus einem keramischen und chemikalienbeständigen Material auf, welches derart ausgebildet ist, dass die physikalischen Eigenschaften des Mikrowellen-durchlässigen Bereichs (80) bezüglich Mikrowellentransparenz und Stabilität während einer Druckreaktion des Druckbehälters (1) konstant gehalten werden. Der Mikrowellen-durchlässigen Bereich (80) ist alternativ vollständig durch ein keramisches und chemikalienbeständiges Material gebildet ist, welches den Boden des Druckbehälters (1) bildet.