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    METHOD OF PRODUCING ALIPHATIC ALDEHYDE COMPOUND HAVING TERMINAL CONJUGATED DIENE STRUCTURE AND INTERMEDIATE THEREFOR
    2.
    发明公开
    METHOD OF PRODUCING ALIPHATIC ALDEHYDE COMPOUND HAVING TERMINAL CONJUGATED DIENE STRUCTURE AND INTERMEDIATE THEREFOR 审中-公开
    生产具有末端共轭二烯结构的脂族醛化合物的方法及其中间体

    公开(公告)号：EP3235798A1

    公开(公告)日：2017-10-25

    申请号：EP17164722.5

    申请日：2017-04-04

    申请人： Shin-Etsu Chemical Co., Ltd.

    发明人： BABA, Akihiro ,  MIYAKE, Yuki ,  KINSHO, Takeshi

    IPC分类号： C07C41/20 ,  C07C41/30 ,  C07C43/178 ,  C07C45/42 ,  C07C47/21

    CPC分类号： C07C43/315 ,  C07C41/48 ,  C07C45/42 ,  C07C45/81 ,  C07C45/82 ,  C07C303/28 ,  C07C47/21 ,  C07C47/02 ,  C07C43/313 ,  C07C43/303 ,  C07C309/66

    摘要： Provided are a method for producing a terminal conjugated dienal compound without an oxidation reaction and a terminal hydroxyacetal compound useful as an intermediate in the method. More specifically, provided are a method for producing an (E)-dienal compound comprising the steps of: a metalation reaction of an alkynal acetal compound(1) to obtain an organic metal compound (2), an addition reaction of (2) to ethylene oxide to obtain a hydroxyalkynal acetal compound (3), a reduction reaction of (3) to obtain an (E)-hydroxyalkenal acetal compound (4), a functional group conversion reaction of (4) to obtain an (E)-alkenal acetal compound (5) having a leaving group X, an elimination reaction of (5) to obtain an (E)-dienal acetal compound (6), and a hydrolysis reaction of (6) to obtain the (E)-dienal compound (7); and others.

    摘要翻译： 本发明提供一种无氧化反应的末端共轭双烯醛化合物的制造方法以及作为该方法中的中间体有用的末端羟基缩醛化合物。 更具体而言，提供（E） - 二烯醛化合物的制造方法，其包括以下步骤：使炔醛缩醛化合物（1）金属化以获得有机金属化合物（2），（2）与 （3）的还原反应以获得（E） - 羟基烯醛缩醛化合物（4），（4）的官能团转化反应以获得（E） - alk烯醛 （E） - 二烯缩醛化合物（6）的消去反应和（6）的水解反应，得到（E） - 二烯醛化合物（5） 7）; 和别的。

    METHOD FOR PRODUCING 2'-TRIFLUOROMETHYL GROUP-SUBSTITUTED AROMATIC KETONE
    3.
    发明公开
    METHOD FOR PRODUCING 2'-TRIFLUOROMETHYL GROUP-SUBSTITUTED AROMATIC KETONE 审中-公开
    生产2'-三氟甲基取代的芳香酮的方法

    公开(公告)号：EP3196183A1

    公开(公告)日：2017-07-26

    申请号：EP15841268.4

    申请日：2015-09-07

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： NAKATANI, Jiro ,  NOZOE, Tatsuhiro

    IPC分类号： C07C45/42 ,  C07C49/80

    CPC分类号： C07C45/42 ,  C07C45/455 ,  C07C49/80

    摘要： The present invention is a method of producing a 2'-trifluoromethyl-substituted aromatic ketone comprising reacting a 2-halogen-substituted benzotrifluoride compound with magnesium metal to convert the compound to a Grignard reagent; and reacting the Grignard reagent with an acid anhydride; and then hydrolyzing the resultant to produce a 2'-trifluoromethyl-substituted aromatic ketone. The method of producing a 2'-trifluoromethyl-substituted aromatic ketone of the present invention enables 2'-trifluoromethyl-substituted aromatic ketone to be produced without using expensive raw materials by generating a Grignard reagent as an intermediate and reacting this Grignard reagent with an acid anhydride in an efficient productivity. The 2'-trifluoromethyl-substituted aromatic ketone that is produced by the method of producing a 2'-trifluoromethyl-substituted aromatic ketone of the present invention can be used as fine chemicals, raw materials for pharmaceuticals and agrochemicals, raw materials for resins and plastics, electronics and information related materials, optical materials, and the like.

    摘要翻译： 本发明是一种制备2'-三氟甲基取代的芳族酮的方法，该方法包括使2-卤素取代的三氟甲苯化合物与镁金属反应以将该化合物转化成格利雅试剂; 并使格氏试剂与酸酐反应; 然后水解生成物以产生2'-三氟甲基取代的芳族酮。 生产本发明的2'-三氟甲基取代的芳族酮的方法使得能够在不使用昂贵的原料的情况下通过生成格利雅试剂作为中间体来生产2'-三氟甲基取代的芳族酮并且使该格利雅试剂与酸 酸酐以有效的生产率生产。 通过本发明的2'-三氟甲基取代的芳香族酮的制造方法制造的2'-三氟甲基取代芳香族酮可以作为精细化学品，药品和农药的原料，树脂和塑料的原料 ，电子和信息相关材料，光学材料等。

    Omega-halo-2-alkynal, method for producing same, and method for producing conjugated Z-alken-yn-yl acetate using same
    4.
    发明公开
    Omega-halo-2-alkynal, method for producing same, and method for producing conjugated Z-alken-yn-yl acetate using same 有权
    ω-卤代-2-炔醛，其制备方法，从而用于共轭Z-烯烃 - 炔基乙酸酯的制备方法

    公开(公告)号：EP2789602A1

    公开(公告)日：2014-10-15

    申请号：EP14163480.8

    申请日：2014-04-04

    申请人： SHIN-ETSU CHEMICAL CO., LTD

    发明人： Yamashita, Miyoshi ,  Fukumoto, Takehiko ,  Kinsho, Takeshi

    IPC分类号： C07C67/10 ,  C07C69/145 ,  C07C45/51 ,  C07C47/24

    CPC分类号： C07C67/10 ,  C07C17/2635 ,  C07C45/42 ,  C07C45/43 ,  C07C47/24 ,  C07C67/11 ,  C07C69/145 ,  C07C21/22

    摘要： Provided is a method for industrially producing a conjugated Z-alken-yn-yl acetate such as Z-13-hexadecen-11-yn-yl acetate which is a sex pheromone component of a pine processionary moth, and an intermediate for the conjugated Z-alken-yn-yl acetate under mild conditions at a high yield. More specifically, provided is a method for producing a conjugated Z-alken-yn-yl acetate (5) comprising the steps of: reacting an ω-halo-2-alkynal (1) with an alkylidene triphenylphosphorane (3) through a Wittig reaction to obtain a conjugated Z-alken-yn-yl halide (4), and acetoxylating the conjugated Z-alken-yn-yl halide (4) into a conjugated Z-alken-yn-yl acetate (5).

    摘要翻译： 提供了一种用于在工业上制备共轭的Z-链烯炔基乙酸酯的方法：如Z-13十六碳烯-11-炔基乙酸酯的所有其是松树processionary蛾的性信息素组分，以及中间的共轭的Z- 温和的条件下 - 烯烃 - 炔基乙酸酯以高收率。 更具体地，提供了一种用于制备共轭的Z-链烯炔基乙酸酯（5）包括以下步骤的方法：使至E-卤代-2-炔醛（1）与通过Wittig反应的烷叉triphenylphosphoranes（3） 以得到共轭Z-烯烃 - 炔基卤化物（4），和共轭acetoxylating的Z烯烃 - 炔基卤化物（4）成共轭的Z-烯烃 - 炔基乙酸酯（5）。

    VERFAHREN ZUR HERSTELLUNG VON DEOXYBENZOINEN
    7.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON DEOXYBENZOINEN 审中-公开
    用于生产DEOXYBENZOINEN

    公开(公告)号：EP1456161A1

    公开(公告)日：2004-09-15

    申请号：EP02792928.0

    申请日：2002-12-06

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： HAREMZA, Sylke

    IPC分类号： C07C45/00 ,  C07C45/42 ,  C07C49/83 ,  C07C49/84

    CPC分类号： C07C45/42 ,  C07C45/00 ,  C07C49/84 ,  C07C49/83

    摘要： The invention relates to a method for producing 1,2-diarylethanones by reacting an arylacetonitrile with an aromatic compound and by hydrolysing the ketimine compound that has been formed, at least one dialkyl ether of a monoalkylene or polyalkylene glycol, or a cyclic ether with at least two oxygen atoms being used as a solvent for the reaction. The method produces excellent yields at an ambient temperature and does not require the solvent to be dried.

    PROCESS FOR PRODUCING HINOKITIOL
    8.
    发明授权
    PROCESS FOR PRODUCING HINOKITIOL 有权
    VERFAHREN ZUR HERSTELLUNG VON HINOKITIOL

    公开(公告)号：EP1069104B1

    公开(公告)日：2004-01-28

    申请号：EP99910743.6

    申请日：1999-03-29

    申请人： Asahi Kasei Kabushiki Kaisha

    发明人： NAGATO, Yasuhiro ,  SHIMIZU, Katsuya ,  YAMAMOTO, Shinichi

    IPC分类号： C07C45/64 ,  C07C49/717

    CPC分类号： C07C49/717 ,  C07C45/42 ,  C07C45/69 ,  C07C2601/18 ,  Y02P20/582 ,  C07C49/693

    摘要： A process for producing hinokitiol which comprises obtaining 1-isopropylcyclopentadiene from cyclopentadiene and an isopropylating agent represented by the general formula R-X (wherein R represents isopropyl; and X represents halogeno, etc.) (the step 1); reacting the obtained product with a dihaloketene to give a ketene-adduct (the step 2); and then decomposing this ketene-adduct (the step 3); wherein the above step 1 involves the following three steps: (a) the step of preparing a cyclopentadienyl metal; (b) the step of isopropylating the cyclopentadienyl metal in an aprotic polar solvent to give isopropylcyclopentadiene; and (c) the step of isomerizing 5-isopropylcyclopentadiene contained in the product selectively into 1-isopropylcyclopentadiene under heating.

    摘要翻译： 一种生产桧醇的方法，其包括从环戊二烯获得1-异丙基环戊二烯和由通式R-X表示的异丙基化剂的步骤，其中R是异丙基，X是卤素等（第一步），使其与 二卤代乙烯以获得乙烯酮加合物（第二步），并分解乙烯酮加合物（第三步），所述第一步包括以下三个步骤：a）环戊二烯基金属的制备步骤; b）通过在非质子极性溶剂中异丙基化环戊二烯合金而获得异丙基环戊二烯的步骤; 和C）将产物中的5-异丙基环戊二烯以热量异构化为1-异丙基环戊二烯的步骤。