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    METHOD FOR PRODUCING SILICONE POLYMER
    1.
    发明公开
    METHOD FOR PRODUCING SILICONE POLYMER 审中-公开

    公开(公告)号：EP4119596A1

    公开(公告)日：2023-01-18

    申请号：EP21767681.6

    申请日：2021-03-05

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： KATO, Hidetoshi ,  SEKI, Hiroyasu

    IPC分类号： C08G77/06 ,  C08G77/18 ,  C08G77/34

    摘要： The present invention provides a silicone polymer production method that can achieve a significantly improved yield due to the needlessness of a rinsing step and can produce a stable a silicone polymer. The production method for a silicone polymer includes a step for preparing at least one silane compound selected from the compounds represented by the general formula (1); R a Si(OR 1 ) 4-a (1) (wherein R is a hydrogen atom or a monovalent organic group, R 1 is a monovalent organic group, and a is an integer of 1 or 2) and the compounds represented by the general formula (2); Si(OR 2 ) 4 (2) (wherein R 2 is a monovalent organic group), a step for hydrolyzing it with a quaternary ammonium compound in the presence of water, and a step for bringing it into contact with a cation exchange resin.

    METHOD FOR PURIFYING DIMETHYL SULFOXIDE
    3.
    发明公开
    METHOD FOR PURIFYING DIMETHYL SULFOXIDE 审中-公开
    VERFAHREN ZUR REINIGUNG VON DIMETHYLSULFOXID

    公开(公告)号：EP2993166A1

    公开(公告)日：2016-03-09

    申请号：EP14791804.9

    申请日：2014-04-22

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： ISHINO, Michiko ,  TANAKA, Koji ,  ABE, Hiromitsu ,  INOUE, Hideki

    IPC分类号： C07C315/06 ,  C07C317/04

    CPC分类号： C07C315/06 ,  C07C317/04

    摘要： The present invention provides a method for purifying dimethyl sulfoxide economically and at good yield so as to satisfy the specifications of the United States Pharmacopoeia and reduce odor. The method is characterized in that a solution having 35 parts by weight or more of water admixed per 100 parts by weight of raw dimethyl sulfoxide is distilled.

    摘要翻译： 本发明提供了经济地和良好收率地纯化二甲基亚砜以满足美国药典的规格并减少气味的方法。 该方法的特征在于，蒸馏每100重量份生二甲基亚砜混合了35重量份以上的水的溶液。

    METHOD FOR PRODUCING OPTICALLY ACTIVE TRANS-1,2-DIAMINOCYCLOHEXANE
    4.
    发明公开
    METHOD FOR PRODUCING OPTICALLY ACTIVE TRANS-1,2-DIAMINOCYCLOHEXANE 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON OPTISCH AKTIVEM TRANS-1,2-DIAMINOCYCLOHEXAN

    公开(公告)号：EP2977368A1

    公开(公告)日：2016-01-27

    申请号：EP14768179.5

    申请日：2014-03-13

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： MORII, Seiji ,  MORIMOTO, Masao

    IPC分类号： C07C209/84 ,  C07C211/36

    CPC分类号： C07C209/84 ,  C07B2200/07 ,  C07C2601/14 ,  C07C211/36

    摘要： The present invention is a method for producing optically active trans-1,2-diaminocyclohexane, in which a crystal of optically active trans-1,2-diaminocyclohexane is obtained by crystallization from a solution of optically active trans-1,2-diaminocyclohexane. According to the present invention, optically active trans-1, 2-diaminocyclohexane with high purity is obtained in a favorable yield from a solution of optically active trans-1,2-diaminocyclohexane. The optically active trans-1,2-diaminocyclohexane with high purity, which is produced by a method for producing optically active trans-1,2-diaminocyclohexane of the present invention, is useful as a raw material for a large number of medicines.

    摘要翻译： 本发明是光学活性反式-1,2-二氨基环己烷的制造方法，其中通过从旋光反式-1,2-二氨基环己烷的溶液中结晶得到光学活性的反式-1,2-二氨基环己烷的结晶。 根据本发明，由光学活性的反式-1,2-二氨基环己烷的溶液以良好的收率得到高纯度的光学活性的反式-1,2-二氨基环己烷。 通过本发明的光学活性反式-1,2-二氨基环己烷的制造方法制造的高纯度光学活性的反式-1,2-二氨基环己烷作为大量药物的原料是有用的。

    PROCESS FOR PRODUCTION OF 2,2'-BIS(TRIFLUOROMETHYL)- 4,4'-DIAMINOBIPHENYL
    8.
    发明公开
    PROCESS FOR PRODUCTION OF 2,2'-BIS(TRIFLUOROMETHYL)- 4,4'-DIAMINOBIPHENYL 审中-公开
    用于生产2,2'-双（三氟甲基）-4,4-二氨基

    公开(公告)号：EP2100874A1

    公开(公告)日：2009-09-16

    申请号：EP07831211.3

    申请日：2007-11-05

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： NAKATANI, Jiro

    IPC分类号： C07C209/36 ,  C07C209/86 ,  C07C211/52 ,  C07B61/00

    CPC分类号： C07C211/52 ,  C07C209/365

    摘要： The present invention is a method for producing of 2,2'-bis(trifluoromethyl)-4,4'-diaminobiphenyl, wherein 2,2'-bis(trifluoromethyl)biphenyl is produced from o-chlorobenzotrifluoride, further, 2,2'-bis(trifluoromethyl)biphenyl is dinitrated in 1,2-dichloropropane solution, and 2,2'-bis(trifluoromethyl)-4,4'-dinitrobiphenyl is isolated and reduced. The method for producing of 2,2'-bis(trifluoromethyl)-4,4'-diaminobiphenyl of the present invention is an industrially excellent method for producing with high safety and high production efficiency.

    摘要翻译： 本发明是用于2,2'-双（三氟甲基）-4,4-二氨基，worin 2,2'-双制造方法（三氟甲基）联苯从邻氯三氟甲苯，进一步，2,2'产生的 双（三氟甲基）联苯二硝化在1,2-二氯丙烷溶液，和2,2'-双（三氟甲基）-4,4-二硝基分离并减少了。 为2,2'-双（三氟甲基）本发明的-4,4-二氨基的制造方法是用于具有高安全性和高生产效率生产一种工业上优异的方法。

    PROCESSES FOR THE RECOVERY OF OPTICALLY ACTIVE DIACYLTARTATIC ACIDS
    9.
    发明公开
    PROCESSES FOR THE RECOVERY OF OPTICALLY ACTIVE DIACYLTARTATIC ACIDS 审中-公开
    VERFAHREN ZUR GEWINNUNG OPTISCH AKTIVERDIACYLTARTARSÄUREN

    公开(公告)号：EP1586551A1

    公开(公告)日：2005-10-19

    申请号：EP03780993.6

    申请日：2003-12-22

    申请人： Toray Fine Chemicals Co., Ltd.

    发明人： MORII, Seiji ,  FUJINO, Toshihiro ,  SATO, Haruyo

    IPC分类号： C07C67/52 ,  C07C69/76 ,  C07C69/78 ,  C07C69/92 ,  C07B57/00

    CPC分类号： C07C67/52 ,  C07B2200/07 ,  Y02P20/582 ,  C07C69/76

    摘要： When a salt of an amine and an optically active diacyltartaric acid, or a diastereomer salt of an optically active amine and an optically active diacyltartaric acid, obtained by optically resolving a racemic amine using the optically active diacyltartaric acid, is salt-exchanged with an acid aqueous solution, the optically active diacyltartaric acid is added in the acid aqueous solution beforehand.
    Furthermore, a raw material containing a racemic amine and an optically active diacyltartaric acid is optically resolved, and the diastereomer salt of the optically active amine and the optically active diacyltartaric acid respectively of one isomer type, is separated. The obtained diastereomer salt is dissociated using an acid aqueous solution containing the optically active diacyltartaric acid, for recovering the optically active diacyltartaric acid, and the obtained' optically active diacyltartaric acid is recycled into an optical resolution step as a raw material of the optical resolution step.

    摘要翻译： 当通过光学拆分外消旋胺使用光学活性二酰基酒石酸获得的胺和光学活性二酰基酒石酸盐或光学活性胺和光学活性二酰基酒石的非对映异构体盐与酸盐交换时 将光学活性的二酰基酒石酸预先加入到酸性水溶液中。 此外，含有外消旋胺和光学活性二酰基酒石酸的原料被光学拆分，分离出一种异构体类型的光学活性胺和光学活性二酰基酒石的非对映异构体盐。 使用含有光学活性二酰基酒石酸的酸性水溶液使得到的非对映异构体盐解离，以回收光学活性的二酰基酒石酸，将得到的“光学活性二酰基酒石酸”作为光学拆分步骤的原料再循环到光学拆分步骤 。