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    COMBINED FILTERING PROCESS FOR RECYCLING PRECIOUS METAL FROM FISCHER-TROPSCH SYNTHETIC PRODUCT
    3.
    发明公开
    COMBINED FILTERING PROCESS FOR RECYCLING PRECIOUS METAL FROM FISCHER-TROPSCH SYNTHETIC PRODUCT 审中-公开
    KOMBINIERTES FILTERUNGSVERFAHREN ZUR WIEDERAUFBEREITON EINES METALLS AUS EINEM SYNTHETISCHEN FISCHER-TROPSCH-PRODUKT

    公开(公告)号：EP2868756A1

    公开(公告)日：2015-05-06

    申请号：EP13808849.7

    申请日：2013-04-25

    申请人： Sunshine Kaidi New Energy Group Co., Ltd.

    发明人： CHEN, Yilong ,  JIN, Jiaqi ,  ZHANG, Yanfeng ,  SONG, Kan ,  ZHAN, Xiaodong ,  JIANG, Manyi

    IPC分类号： C22B7/00 ,  C07C1/04

    CPC分类号： C22B61/00 ,  B01J8/006 ,  B01J8/007 ,  B01J8/22 ,  B01J23/75 ,  C10G31/09 ,  C10G2300/1022 ,  C10G2300/205 ,  C10G2300/208 ,  C10G2300/706 ,  C21B15/00 ,  C21B2200/00 ,  C22B7/009 ,  C22B11/026 ,  C22B23/04 ,  Y02P10/214 ,  Y02W30/54

    摘要： A combined filtering process for recycling a precious metal from a Fischer-Tropsch synthetic product with the steps of: 1) after the product of a Fischer-Tropsch synthesis reaction is filtered by an inner filter, the product is introduced into a first filter buffer tank from an outlet on the upper part of a Fischer-Tropsch synthesis reactor, where a gas-phase product or a partially liquid-phase product filtered from the product by the first filter buffer tank is discharged from the top part, and where liquid-phase and solid-phase products discharged from the bottom part of the first filter buffer tank are introduced into a refining filter for product refinement; 2) the liquid-phase product that is mainly a catalyst slurry is introduced from the bottom part of the Fischer-Tropsch reactor into a dynamic filter for filtering, where the filtered liquid-phase product containing small particles of a spent catalyst and precious metal ions dissolved in the product is separated from the bottom part of the dynamic filter, introduced into a second filter buffer tank, and introduced from the bottom part of the second filter buffer tank into the refining filter for refinement; and, 3) a white clay cake is first formed on a filter plate in the refining filter, then, with respect to the product introduced into the refining filter, when the white clay cake is formed, a product refinement process is utilized for refinement processing of the product.

    摘要翻译： 一种用于从费 - 托合成产品回收贵金属的组合过滤方法，其步骤为：1）在通过内过滤器过滤费 - 托合成反应产物之后，将产物引入第一过滤缓冲罐 从费 - 托合成反应器的上部的出口，其中从第一过滤缓冲罐从产物过滤的气相产物或部分液相产物从顶部排出，并且其中液相 将从第一过滤缓冲罐的底部排出的固相物质引入精制过滤器中进行产品精制; 2）主要是催化剂浆液的液相产物从费 - 托反应器的底部引入用于过滤的动态过滤器，其中过滤的含有废催化剂和少量金属离子的小颗粒的液相产物 溶解在产品中的动态过滤器的底部分离，引入第二过滤缓冲罐，并从第二过滤器缓冲罐的底部引入精炼过滤器进行精制; 和3）首先在精制过滤器中的过滤板上形成白色粘土饼，然后相对于引入精制过滤器的产品，当形成白色粘土饼时，利用产品精制方法进行精制加工 的产品。

    Process for recovering group VI-B metals from spent catalysts
    4.
    发明公开
    Process for recovering group VI-B metals from spent catalysts 审中-公开
    Verfahren zurRückgewinnungvon Gruppe-VI-B-Mmetallen aus verbrauchten Katalysatoren

    公开(公告)号：EP2410066A2

    公开(公告)日：2012-01-25

    申请号：EP11185542.5

    申请日：2007-09-14

    申请人： Albemarle Netherlands BV

    发明人： Sitters, Johannes Cornelis ,  Free, Harmannus Willem Homan ,  Oogjen, Bob Gerardus

    IPC分类号： C22B34/34 ,  C22B34/36 ,  C22B23/00 ,  C22B7/00 ,  C22B1/02 ,  B01J23/888 ,  C10G45/08

    CPC分类号： C22B7/009 ,  B01J23/28 ,  B01J23/30 ,  B01J23/85 ,  B01J23/883 ,  B01J23/8885 ,  B01J37/031 ,  B01J38/68 ,  C10G49/04 ,  C10G2300/706 ,  C22B23/026 ,  C22B34/345 ,  C22B34/365 ,  Y02P10/214 ,  Y02P10/224 ,  Y02P10/23 ,  Y02P10/234

    摘要： The invention relates to a process for recovering Group VIB metals from a catalyst, in particular a spent bulk catalyst, comprising one or more Group VIB metals and one or more Group VIII metals. Further, the invention relates to a solid Group VIB metal compound obtainable by the process according to the invention having the general formula H 2 XO 4 , wherein X = W 1-y Mo y , wherein y is between 0 and 1 and to its use in a process for the manufacture of a fresh catalyst. The process comprises the steps of: a) oxidizing the one or more Group VIB metals to one or more Group VIB metal oxides; separating the one or more Group VIB metal oxides from the one or more Group VIII metals; dissolving the one or more Group VIB metal oxides in water to produce an aqueous solution of one or more Group VIB metal oxides; d) precipitating the one or more Group VIB metal oxides from the aqueous solution by adding alkaline earth metal (Group IIa) ions to the aqueous solution; e) optionally filtering and washing the precipitate; and f) transforming the precipitate by adding an acid to form a solid metal compound comprising one or more Group VIB metals.

    摘要翻译： 本发明涉及一种从催化剂中回收VIB族金属的方法，特别是废组分催化剂，其包含一种或多种VIB族金属和一种或多种VIII族金属。 此外，本发明涉及通过根据本发明的方法获得的具有通式H 2 XO 4的固体VIB族金属化合物，其中X = W 1-y Mo y，其中y在0和1之间，并且其使用 在制造新鲜催化剂的过程中。 该方法包括以下步骤：a）将一种或多种VIB族金属氧化成一种或多种VIB族金属氧化物; 从一种或多种VIII族金属分离一种或多种VIB族金属氧化物; 将一种或多种VIB族金属氧化物溶解在水中以产生一种或多种VIB族金属氧化物的水溶液; d）通过向该水溶液中加入碱土金属（IIa）族离子，从水溶液中沉淀出一种或多种VIB族金属氧化物; e）任选地过滤和洗涤沉淀物; 和f）通过加入酸形成包含一种或多种VIB族金属的固体金属化合物来转化沉淀物。

    REMOVAL OF FINE PARTICLES FROM A FISCHER TROPSCH STREAM
    8.
    发明公开
    REMOVAL OF FINE PARTICLES FROM A FISCHER TROPSCH STREAM 审中-公开
    细颗粒由费 - 托断电

    公开(公告)号：EP2158294A2

    公开(公告)日：2010-03-03

    申请号：EP08763112.3

    申请日：2008-05-27

    申请人： The Petroleum Oil and Gas Corporation of South Africa (Pty) Ltd.

    发明人： KNOTTENBELT, Cyril David ,  TAYLOR, Patrick Otto ,  ADAMS, Vernon Jeremay ,  NICHOLSON, Volan Richard

    IPC分类号： C10G2/00 ,  B01D39/10 ,  B01D39/12

    CPC分类号： B01D61/142 ,  C10G2/30 ,  C10G2300/4081 ,  C10G2300/706

    摘要： This invention relates to a process for the removal of catalyst particles from a hydrocarbon stream (14) derived from the reaction of synthesis gas (12) with a particulate Fischer Tropsch catalyst in a Fischer Tropsch reactor (10). The process includes a primary separation step (16) which makes use of a filter, wherein the filter has a pore size which is 70% to 95 of the average size of the particles of the Fischer Tropsch catalyst, thereby forming a primary filtered hydrocarbon stream (18) containing fine catalyst particles. The benefit of this selection of filter pore size is that it mitigates fines build-up on the filter of the primary separator. The primary filtered hydrocarbon stream (18) is then passed to a secondary separation step in a cross-flow filtration unit (20) which removes fine catalyst particles from the primary filtered hydrocarbon stream to provide a retenate (24) containing the catalyst fines, and permeate (22) containing a hydrocarbon product.