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1.发明授权METHOD AND ARRANGEMENT FOR SEPARATING TWO SOLUTIONS MIXED IN DISPERSION INTO TWO SOLUTION PHASES IN A LIQUID-LIQUID EXTRACTION SEPARATION CELL 有权方法和系统用于在两个解析相分离分散液混合溶液中的使细胞与液 - 液萃取的两地分居
公开(公告)号：EP2393566B1
公开(公告)日：2017-05-31
申请号：EP10738251.7
申请日：2010-02-08
申请人： OUTOTEC (FINLAND) OY
发明人： NYMAN, Bror , EKMAN, Eero , PEKKALA, Pertti , LAITALA, Hannu , SAARIO, Rami
CPC分类号： B01D11/0453 , B01D11/0449 , B01D17/0211 , B01D17/0214 , B01D2011/005 , C22B3/0005 , C22B3/005 , C22B3/02 , Y02P10/234
摘要： The invention relates to a method and arrangement for separating two solutions mixed in dispersion into two solution phases in a liquid-liquid extraction separation cell. The arrangement includes a first guide wall extending along the whole width of the cell with respect to the vertical direction at an inclined angle. The first guide wall includes a bottom edge, which is located at a distance from the cell bottom, so that a clearance gap is formed between the bottom edge and the cell bottom. The arrangement also includes a second guide wall essentially parallel with the first guide wall and placed at a distance therefrom. Between the first guide wall and the second guide wall an uptake shaft is formed extending diagonally upwards at the inclined angle. The second guide wall is pressed tightly against the cell bottom, and includes a number of vertical slots.
摘要翻译： 本发明涉及一种用于分离两种溶液混合在分散成两两相溶液中的液 - 液萃取分离细胞的方法和装置。 该装置包括一第一导向壁沿着电池的整个宽度相对于处倾斜角度延伸到垂直方向。 第一引导壁包括底边缘，所有这些都位于从细胞底部的距离，所以没有间隙的间隙的底部边缘和底部电池之间形成。 所以该装置包括第二导向壁基本上与第一引导壁平行且以一定距离放置在那里。 第一引导壁和第二引导壁摄取轴之间形成在倾斜角度延伸斜向上。 第二导向壁被紧紧地压在池的底部，并且包括多个垂直槽。
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公开(公告)号：EP3165616B1
公开(公告)日：2018-03-21
申请号：EP14896593.2
申请日：2014-07-03
发明人： SHU, Yuzhang , ZHANG, Qi , YANG, Guifen , SUN, Baohua , WEI, Linkui
摘要： The invention discloses a treatment method of a chlorine-containing zinc oxide secondary material, which comprises the following steps: 1) leaching the chlorine-containing zinc oxide secondary material I through an acid solution; 2) selectively extracting zinc through P204-kerosene solvent; 3) implementing stripping-electrolysis zinc recovery; 4) repeating steps 1)-4); 5) taking out the raffinate obtained from the Step (4), mixing the residual taken out raffinate with chlorine-containing zinc oxide secondary material II when balance on chlorine ion input and taking out is achieved; carrying out liquid-solid separation; leaching the separated deposit through acid raffinate of the step 1); 6) after separated solution achieves preset conditions, purifying the chlorine-containing aqueous phase; 7) evaporating and concentrating to crystallize out KCI and NaCl products. The invention is environment- friendly and energy-saving, and free from process wastewater emission; production cost is greatly reduced and secondary pollution of the currentdechloridation process is eliminated thoroughly.
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3.发明公开METHOD AND ARRANGEMENT FOR SEPARATING TWO SOLUTIONS MIXED IN DISPERSION INTO TWO SOLUTION PHASES IN A LIQUID-LIQUID EXTRACTION SEPARATION CELL 有权方法和系统用于在两个解析相分离分散液混合溶液中的使细胞与液 - 液萃取的两地分居
公开(公告)号：EP2393566A1
公开(公告)日：2011-12-14
申请号：EP10738251.7
申请日：2010-02-08
申请人： Outotec OYJ
发明人： NYMAN, Bror , EKMAN, Eero , PEKKALA, Pertti , LAITALA, Hannu , SAARIO, Rami
CPC分类号： B01D11/0453 , B01D11/0449 , B01D17/0211 , B01D17/0214 , B01D2011/005 , C22B3/0005 , C22B3/005 , C22B3/02 , Y02P10/234
摘要： The invention relates to a method and arrangement for separating two solutions mixed in dispersion into two solution phases in a liquid-liquid extraction separation cell. The arrangement includes a first guide wall extending along the whole width of the cell with respect to the vertical direction at an inclined angle. The first guide wall includes a bottom edge, which is located at a distance from the cell bottom, so that a clearance gap is formed between the bottom edge and the cell bottom. The arrangement also includes a second guide wall essentially parallel with the first guide wall and placed at a distance therefrom. Between the first guide wall and the second guide wall an uptake shaft is formed extending diagonally upwards at the inclined angle. The second guide wall is pressed tightly against the cell bottom, and includes a number of vertical slots.
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4.发明授权METHOD FOR SEPARATING IMPURITIES FROM AN ACIDIC SOLUTION CONTAINING NICKEL AND COBALT AND/OR SCANDIUM 有权从含有镍和钴和/或钪的酸性溶液中分离杂质的方法
公开(公告)号：EP2977473B1
公开(公告)日：2017-12-13
申请号：EP14770382.1
申请日：2014-03-17
发明人： GOTO, Masahiro , KUBOTA, Fukiko , BABA, Yuzo , OZAKI, Yoshitomo , HAYATA, Jiro , HIGAKI, Tatsuya , NAGAKURA, Toshihiko , MATSUMOTO, Shinya
CPC分类号： C22B59/00 , C22B3/005 , C22B3/44 , C22B23/0453 , C22B23/0461 , Y02P10/234
摘要： Provided is a method for efficiently separating nickel, cobalt and/or scandium, and impurities from an acidic solution containing impurities such as manganese, iron, zinc, and aluminum. A valuable-metal extracting agent of the present invention is expressed by general formula (1). In the formula, R 1 and R 2 each represent the same or different alkyl groups, R 3 represents a hydrogen atom or an alkyl group, and R 4 represents a hydrogen atom or a given group, other than an amino group, that bonds with an ± carbon as an amino acid. In general formula (1), the inclusion of a glycine unit, a histidine unit, a lysine unit, an asparagine acid unit, or a normal methylglycine unit is preferred.
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5.发明公开METHOD FOR PROCESSING ZINC OXYCHLORIDE-CONTAINING SECONDARY MATERIAL 有权VERFAHREN ZUR VERARBEITUNG EINES ZINKOXYCHLORIDHALTIGENSEKUNDÄRMATERIALS
公开(公告)号：EP3165616A4
公开(公告)日：2017-06-14
申请号：EP14896593
申请日：2014-07-03
发明人： SHU YUZHANG , ZHANG QI , YANG GUIFEN , SUN BAOHUA , WEI LINKUI
摘要： The invention discloses a treatment method of a chlorine-containing zinc oxide secondary material, which comprises the following steps: 1) leaching the chlorine-containing zinc oxide secondary material I through an acid solution; 2) selectively extracting zinc through P204-kerosene solvent; 3) implementing stripping-electrolysis zinc recovery; 4) repeating steps 1)-4); 5) taking out the raffinate obtained from the Step (4), mixing the residual taken out raffinate with chlorine-containing zinc oxide secondary material II when balance on chlorine ion input and taking out is achieved; carrying out liquid-solid separation; leaching the separated deposit through acid raffinate of the step 1); 6) after separated solution achieves preset conditions, purifying the chlorine-containing aqueous phase; 7) evaporating and concentrating to crystallize out KCI and NaCl products. The invention is environment- friendly and energy-saving, and free from process wastewater emission; production cost is greatly reduced and secondary pollution of the currentdechloridation process is eliminated thoroughly.
摘要翻译： 本发明公开了一种含氯氧化锌辅助材料的处理方法，包括以下步骤：1）通过酸溶液浸出含氯氧化锌辅助材料I; 2）通过P204-煤油溶剂选择性提取锌; 3）实施汽提 - 电解锌回收; 4）重复步骤1）-4）; 5）取出步骤（4）得到的萃余液，将取出的萃余液与含氯氧化锌辅助材料II混合，待氯离子输入和取出达到平衡后， 进行液固分离; 通过步骤1）的酸提余液浸提分离的沉积物; 6）分离后的溶液达到预设条件后，净化含氯水相; 7）蒸发浓缩结晶出KCl和NaCl产品。 本发明环保节能，免受工艺废水排放; 大大降低了生产成本，彻底杜绝了目前氯化工艺的二次污染。
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6.发明公开METHOD FOR SEPARATING IMPURITIES FROM AN ACIDIC SOLUTION CONTAINING NICKEL AND COBALT AND/OR SCANDIUM 有权从含有镍和钴和/或钪的酸性溶液中分离杂质的方法
公开(公告)号：EP2977473A1
公开(公告)日：2016-01-27
申请号：EP14770382.1
申请日：2014-03-17
发明人： GOTO, Masahiro , KUBOTA, Fukiko , BABA, Yuzo , OZAKI, Yoshitomo , HAYATA, Jiro , HIGAKI, Tatsuya , NAGAKURA, Toshihiko , MATSUMOTO, Shinya
CPC分类号： C22B59/00 , C22B3/005 , C22B3/44 , C22B23/0453 , C22B23/0461 , Y02P10/234
摘要： Provided is a method for efficiently separating nickel, cobalt and/or scandium, and impurities from an acidic solution containing impurities such as manganese, iron, zinc, and aluminum. A valuable-metal extracting agent of the present invention is expressed by general formula (1). In the formula, R 1 and R 2 each represent the same or different alkyl groups, R 3 represents a hydrogen atom or an alkyl group, and R 4 represents a hydrogen atom or a given group, other than an amino group, that bonds with an α carbon as an amino acid. In general formula (1), the inclusion of a glycine unit, a histidine unit, a lysine unit, an asparagine acid unit, or a normal methylglycine unit is preferred.
摘要翻译： 本发明提供从含有锰，铁，锌，铝等杂质的酸性溶液中有效地分离镍，钴和/或钪及杂质的方法。 本发明的有价金属提取剂由通式（1）表示。 式中，R 1和R 2分别表示相同或不同的烷基，R 3表示氢原子或烷基，R 4表示氢原子或与α碳键合的氨基以外的给定基团， 一种氨基酸。 在通式（1）中，优选包含甘氨酸单元，组氨酸单元，赖氨酸单元，天冬酰胺酸单元或正常甲基甘氨酸单元。
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公开(公告)号：EP3165616A1
公开(公告)日：2017-05-10
申请号：EP14896593.2
申请日：2014-07-03
发明人： SHU, Yuzhang , ZHANG, Qi , YANG, Guifen , SUN, Baohua , WEI, Linkui
摘要： The invention discloses a treatment method of a chlorine-containing zinc oxide secondary material, which comprises the following steps: 1) leaching the chlorine-containing zinc oxide secondary material I through an acid solution; 2) selectively extracting zinc through P204-kerosene solvent; 3) implementing stripping-electrolysis zinc recovery; 4) repeating steps 1)-4); 5) taking out the raffinate obtained from the Step (4), mixing the residual taken out raffinate with chlorine-containing zinc oxide secondary material II when balance on chlorine ion input and taking out is achieved; carrying out liquid-solid separation; leaching the separated deposit through acid raffinate of the step 1); 6) after separated solution achieves preset conditions, purifying the chlorine-containing aqueous phase; 7) evaporating and concentrating to crystallize out KCI and NaCl products. The invention is environment- friendly and energy-saving, and free from process wastewater emission; production cost is greatly reduced and secondary pollution of the currentdechloridation process is eliminated thoroughly.
摘要翻译： 本发明公开了一种含氯氧化锌辅助材料的处理方法，包括以下步骤：1）通过酸溶液浸出含氯氧化锌辅助材料I; 2）通过P204-煤油溶剂选择性提取锌; 3）实施汽提 - 电解锌回收; 4）重复步骤1）-4）; 5）取出步骤（4）得到的萃余液，将取出的萃余液与含氯氧化锌辅助材料II混合，待氯离子输入和取出达到平衡后， 进行液固分离; 通过步骤1）的酸提余液浸提分离的沉积物; 6）分离后的溶液达到预设条件后，净化含氯水相; 7）蒸发浓缩结晶出KCl和NaCl产品。 本发明环保节能，免受工艺废水排放; 大大降低了生产成本，彻底杜绝了目前氯化工艺的二次污染。
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8.发明公开
公开(公告)号：EP2977473A4
公开(公告)日：2016-03-16
申请号：EP14770382
申请日：2014-03-17
发明人： GOTO MASAHIRO , KUBOTA FUKIKO , BABA YUZO , OZAKI YOSHITOMO , HAYATA JIRO , HIGAKI TATSUYA , NAGAKURA TOSHIHIKO , MATSUMOTO SHINYA
CPC分类号： C22B59/00 , C22B3/005 , C22B3/44 , C22B23/0453 , C22B23/0461 , Y02P10/234
摘要： Provided is a method for efficiently separating nickel, cobalt and/or scandium, and impurities from an acidic solution containing impurities such as manganese, iron, zinc, and aluminum. A valuable-metal extracting agent of the present invention is expressed by general formula (1). In the formula, R 1 and R 2 each represent the same or different alkyl groups, R 3 represents a hydrogen atom or an alkyl group, and R 4 represents a hydrogen atom or a given group, other than an amino group, that bonds with an ± carbon as an amino acid. In general formula (1), the inclusion of a glycine unit, a histidine unit, a lysine unit, an asparagine acid unit, or a normal methylglycine unit is preferred.
摘要翻译： 提供了一种用于有效地分离镍，钴和/或钪，并从含杂质的酸性溶液中的杂质的方法：如锰，铁，锌和铝。 本发明的有价金属萃取剂是由通式（1）中过表达。 在该式中，R 1和R 2各自代表相同或不同的烷基，R 3 darstellt氢原子或烷基，和R 4代表氢原子或一个给定的组，比氨基以外，债券做了与 到±碳作为氨基酸。 在通式（1），甘氨酸单元，组氨酸单元，在天冬酰胺酸单元的赖氨酸单元或正常甲基甘氨酸单元的夹杂物是优选的。
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9.发明公开
公开(公告)号：EP2393566A4
公开(公告)日：2013-10-30
申请号：EP10738251
申请日：2010-02-08
申请人： OUTOTEC OYJ
发明人： NYMAN BROR , EKMAN EERO , PEKKALA PERTTI , LAITALA HANNU , SAARIO RAMI
CPC分类号： B01D11/0453 , B01D11/0449 , B01D17/0211 , B01D17/0214 , B01D2011/005 , C22B3/0005 , C22B3/005 , C22B3/02 , Y02P10/234
摘要： The invention relates to a method and arrangement for separating two solutions mixed in dispersion into two solution phases in a liquid-liquid extraction separation cell. The arrangement includes a first guide wall extending along the whole width of the cell with respect to the vertical direction at an inclined angle. The first guide wall includes a bottom edge, which is located at a distance from the cell bottom, so that a clearance gap is formed between the bottom edge and the cell bottom. The arrangement also includes a second guide wall essentially parallel with the first guide wall and placed at a distance therefrom. Between the first guide wall and the second guide wall an uptake shaft is formed extending diagonally upwards at the inclined angle. The second guide wall is pressed tightly against the cell bottom, and includes a number of vertical slots.
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10.发明授权ASYMMETRIC LIGANDS USEFUL FOR TRANSITION METAL CATALYZED BOND FORMING REACTIONS AND EPOXIDE REACTIONS THEREWITH 失效不对称配体的使用过渡金属催化合成及相关EPOXIDREAKTIONEN
公开(公告)号：EP0782577B1
公开(公告)日：2002-06-12
申请号：EP95935015.8
申请日：1995-09-11
IPC分类号： C07F9/50 , C07C227/12
CPC分类号： C07F9/5537 , B01J31/189 , B01J31/2208 , B01J31/2409 , B01J31/2414 , B01J31/2452 , B01J31/2457 , B01J2531/0258 , B01J2531/824 , C07C213/04 , C07C227/12 , C07D207/416 , C07F9/5022 , C07F9/65515 , C07F9/6552 , C22B3/005 , Y02P10/234
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