摘要:
A method for imaging a sample using a high speed dynamic mode atomic force microscope may include scanning a tip of a cantilever probe over a surface of the sample, regulating a vibration amplitude of the tip to remain constant at a set point value (Aset), via a first signal generated in a first feedback controller, measuring a mean tapping deflection of the tip, regulating the mean tapping deflection via a second signal generated in a second feedback controller, tracking and measuring an adjustment to the measured mean tapping deflection during the regulating. The method may further include generating an image topography of the sample based on the first signal, the second signal, and the measured adjustment of the mean tapping deflection of the cantilever probe.
摘要:
An atomic force microscope (AFM) and corresponding method to provide low force (sub-20 pN) AFM control and mechanical property measurement is provided. The preferred embodiments employ real-time false deflection correction/discrimination by adaptively modifying the drive ramp to accommodate to deflection artifacts.
摘要:
The present invention provides a scanning probe microscope and a probe contact detection method which are capable of improving a phenomenon that when the sample surface with which the probe is in contact is an inclined plane, the value of the pressing force to detect the contact between the probe and sample surface is changed as compared to the horizontal plane. A scanning probe microscope for scanning a surface of a sample with a probe by bringing the probe into contact with the surface of the sample, comprises a cantilever having the probe at its tip; a displacement detection unit to detect both a bending amount and a torsion amount of the cantilever; and a contact determination unit to determine a primary contact of the probe with the surface of the sample, based on the bending amount and the torsion amount detected by the displacement detection unit in all directions from an undeformed condition of the cantilever.
摘要:
The invention relates to a method for estimating a phase shift between an in-phase component and a quadrature component provided by a lock-in amplifier, comprising the steps of: Providing an input signal (U), Providing a first reference signal (V ref ), Providing a second reference signal ( V ref, + 90° phase shifted ) that is phase shifted by +90° with respect to the first reference signal (V ref ), Calculating said in-phase component (X) with the lock-in amplifier, which calculation comprises at least multiplying said first reference signal with the input signal and low-pass filtering the result to yield said in-phase component (x), Calculating said quadrature component (Y) with the lock-in amplifier, which calculation comprises at least multiplying said second reference signal with the input signal and low-pass filtering the result to yield said quadrature component (Y), and Estimating the phase (Z) using the in-phase component and the quadrature component by means of a CORDIC algorithm.
摘要:
The present invention relates to a method for controlling a scanning probe microscope having a probe (2) with a tip (21) for interacting with a sample (4), and a nanoscanner (1) for retaining the sample (4) or the probe (2), comprising the steps of monitoring the extension of the piezo element (1) along a first direction (R) along which the tip (21) is moved towards the sample (4), and adjusting the level of the probe (2) along the first direction (R) by means of an additional actuator (3), when the nanoscanner (1) exhibits an extension below or above a threshold value. The invention further relates to a device(100) for controlling a scanning probe microscope.
摘要:
A scanning probe microscope includes a cantilever 12 having a probe 11 at a free thereof, a displacement detection unit 15 to output a displacement signal of the cantilever 12, a vibrating unit 14 to vibrate the cantilever 12, and a scanning unit 20 to three-dimensionally relatively move the sample 19 and probe 11. A mixed signal generation unit 30 includes an amplitude information detecting section 31 to provide a vibrating signal to the vibrating unit 14 and generate an amplitude signal including information of an amplitude of the displacement signal, and a phase difference information detecting section 32 to generate a phase signal including information of a phase difference between the displacement signal and the synchronous signal, and adds the displacement signal and the synchronous signal to generate a mixed signal. A controller 25 to control the scanning unit 20 includes a Z control section 26, which controls the distance between the sample 19 and the probe 11 on the basis of the mixed signal.
摘要:
A scanning probe microscope (SPM) has a piezoelectric actuator-based tube scanner to which a probe is attached and which is moveable in three planes by the application of a voltage to the piezoelectric tube. A set of flexures flex with the displacement of the tube and strain gauges attached to the flexures measure the flex of the flexures to provide feedback as to the displacement of the tube during the scanning of an object. The strain gauges and flexures form a kinematic sensing frame or arrangement in which a single constraint is provided for each degree of freedom and in which the constraints are at least substantially orthogonal to one another.
摘要:
An improved mode of AFM imaging (Peak Force Tapping (PFT) Mode) uses force as the feedback variable to reduce tip-sample interaction forces while maintaining scan speeds achievable by all existing AFM operating modes. Sample imaging and mechanical property mapping are achieved with improved resolution and high sample throughput, with the mode being workable across varying environments, including gaseous, fluidic and vacuum. Ease of use is facilitated by eliminating the need for an expert user to monitor imaging.
摘要:
A method includes generating, using a sensor, a data signal. The data signal includes a first component based on a motion in a first direction of an actuator configured to provide motion between a sample and a probe in the first direction, the first direction substantially in the plane of the sample; and a second component based on at least one of topographic variations of the sample in a second direction, and a materials property of the sample. The method further includes generating, using a processor, a compensatory signal based on the first component of the data signal generated by the sensor; and providing the compensatory signal to the actuator.