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    VISIBLE LIGHT CATALYSED SATURATED CARBON HYDROGEN BOND DIRECT OXIDATION METHOD
    5.
    发明公开
    VISIBLE LIGHT CATALYSED SATURATED CARBON HYDROGEN BOND DIRECT OXIDATION METHOD 审中-公开

    公开(公告)号：EP3572394A1

    公开(公告)日：2019-11-27

    申请号：EP17893061.6

    申请日：2017-10-26

    Applicant: Shanghaitech University

    Inventor： ZUO, Zhiwei ,  HU, Anhua

    IPC: C07C45/36 ,  C07C29/50 ,  C07C17/14 ,  C07C281/02 ,  C07C49/78 ,  C07C49/403 ,  C07C23/10 ,  C07C22/04

    Abstract: The present invention provides a direct oxidation method for saturated hydrocarbon bonds in an organic compound. The method allows an organic compound with a saturated hydrocarbon bond to react with an oxidizing reagent in the presence of cerium complex under visible light irradiation, thus oxidizing the saturated hydrocarbon bond to afford an oxidation product. The present reaction only needs to be carried out at room temperature, while the reaction efficiency remains high. In addition, only visible light is required to provide the energy for activation, rendering the present strategy a milder and greener reaction method. The cerium catalyst used in the method is low in cost, simple and efficient, while the oxidizing reagent used is also stable in nature and low in industrial cost, rendering the catalytic system highly practical. Furthermore, environmental pollution caused by heavy transition metals and peroxides can be avoided in such strategy.

    PYRAZOLE COMPOUND OR SALT THEREOF, AND PREPARATION METHOD, HERBICIDE COMPOSITION AND USE THEREOF
    6.
    发明公开
    PYRAZOLE COMPOUND OR SALT THEREOF, AND PREPARATION METHOD, HERBICIDE COMPOSITION AND USE THEREOF 审中-公开
    吡唑类化合物或其盐及其制备方法，除草剂组合物及其用途

    公开(公告)号：EP3293178A1

    公开(公告)日：2018-03-14

    申请号：EP16880317.9

    申请日：2016-03-04

    Applicant: Qingdao Kingagroot Chemical Compounds Co., Ltd

    Inventor： LIAN, Lei ,  ZHENG, YuRong ,  LI, Song ,  PENG, XueGang ,  JIN, Tao ,  CUI, Qi

    IPC: C07D231/00 ,  C07C22/04 ,  C07C23/08 ,  A01N43/56 ,  A01N25/00 ,  A01P13/00

    Abstract: Disclosed are a pyrazole compound or a salt thereof, a preparation method therefor, a herbicidal composition and use thereof. The pyrazole compound or a salt thereof has a structure as shown in formula (I):

    wherein, R represents

    wherein, R', R", and R'" represent hydrogen, C1-C4 alkyl, C1-C4 halogenated alkyl, C1-C4 alkoxy or halogen, R', R", and R'" may be the same or different; R 1 represents C1-C3 alkyl; R 2 represents hydrogen or C1-C4 alkyl; R 3 represents hydrogen or C1-C6 alkyl, optionally substituted phenyl, optionally substituted pyridyl, optionally substituted alkenyl, optionally substituted alkynyl, C1-C6 alkyl carbonyl, C1-C6 alkoxyl carbonyl, C1-C6 alkyl carbonyl methyl, etc. A compound having a pyrazole structure not only has excellent herbicidal effect on barnyard grass, but also is safe to rice in post-emergence application. More surprisingly, it also has good control efficacy on barnyard grass resistant to major herbicides, such as penoxsulam, quinclorac, cyhalofop-butyl, propanil, etc.

    Abstract translation: 公开了吡唑化合物或其盐，其制备方法，除草组合物及其用途。 吡唑化合物或其盐具有式（I）所示的结构：其中，R表示其中R'，R“和R”'表示氢，C1-C4烷基，C1-C4卤代烷基，C1- C4烷氧基或卤素，R'，R“和R”'可以相同或不同; R1代表C1-C3烷基; R2代表氢或C1-C4烷基; R 3表示氢或C 1 -C 6烷基，任选取代的苯基，任选取代的吡啶基，任选取代的烯基，任选取代的炔基，C 1 -C 6烷基羰基，C 1 -C 6烷氧基羰基，C 1 -C 6烷基羰基甲基等。 吡唑结构不仅对稗草具有优良的除草效果，而且对出苗后的水稻应用也是安全的。 更令人惊讶的是，它对稗草对五种主要除草剂如五氟磺草胺，二氯喹啉酸，氰氟草酯，敌稗等的抗性也具有良好的防治效果。

    METHOD FOR THE PREPARATION OF TRICHLOROMETHYL-GROUP-SUBSTITUTED BENZENE
    8.
    发明公开
    METHOD FOR THE PREPARATION OF TRICHLOROMETHYL-GROUP-SUBSTITUTED BENZENE 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON MIT EINER TRICHLORMETHYLGRUPPE SUBSTITUIERTEM BENZOL

    公开(公告)号：EP3045440A1

    公开(公告)日：2016-07-20

    申请号：EP14843701.5

    申请日：2014-09-12

    Applicant: Shanghai Fanglun New Material Technology Co. Ltd. ,  Wang Nongyue

    Inventor： WANG, Nongyue ,  QU, Xiongwei ,  LI, Guohua ,  ZHAO, Quanzhong ,  SHAO, Jianming ,  WEN, Guoqiang

    IPC: C07C17/14 ,  C07C17/10 ,  C07C17/38 ,  C07C51/60 ,  B01J19/12 ,  C07C22/04 ,  C07C53/44

    CPC classification number: C07C17/08 ,  C07C17/093 ,  C07C17/12 ,  C07C17/14 ,  C07C17/383 ,  C07C51/60 ,  C07C25/125 ,  C07C53/44 ,  C07C22/04 ,  C07C22/06

    Abstract: The present application relates to a method for photochlorination, and specifically to photochlorination by a photochemical reaction of an aromatic compound with gaseous chlorine so as to prepare a trichloromethyl-substituted benzene, and to a method using bis-(trichloromethyl)-benzene as the trichloromethyl-substituted benzene to prepare by further reaction bis-(chloroformyl)-benzene. Through the control of temperature, illuminance and consumption of gaseous chlorine, the method of this application can greatly improve the purity of trichloromethyl-substituted benzene and further prepare polymer-grade bis-(chloroformyl)-benzene with low cost. The present application also relates to a method for purifying trichloromethyl-substituted benzene, and specifically to a method for purifying trichloromethyl-substituted benzene via molecular distillation. The present application further relates to a photochlorination reactor for use in photochlorination reactions (such as those of the present application).

    Abstract translation: 本申请涉及一种光氯化法，特别涉及通过芳族化合物与气态氯的光化学反应进行光氯化，以制备三氯甲基取代的苯，以及使用双（三氯甲基） - 苯作为三氯甲基的方法 通过进一步反应双 - （氯甲酰基） - 苯制备。 通过控制气态氯的温度，照度和消耗，本方法可以大大提高三氯甲基取代苯的纯度，进一步制备低成本的聚合物级双（氯甲酰基） - 苯。 本申请还涉及三氯甲基取代的苯的纯化方法，特别涉及通过分子蒸馏纯化三氯甲基取代的苯的方法。 本申请还涉及用于光氯化反应的光氯化反应器（例如本申请的那些）。

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