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    Method for producing monocyclic aromatic hydrocarbon-styrene compound adduct
    1.
    发明专利
    Method for producing monocyclic aromatic hydrocarbon-styrene compound adduct 有权
    生产单环芳烃 - 苯乙烯化合物添加剂的方法

    公开(公告)号：JP2005330230A

    公开(公告)日：2005-12-02

    申请号：JP2004150413

    申请日：2004-05-20

    申请人： Nippon Petrochemicals Co Ltd ,  新日本石油化学株式会社

    发明人： YANAGAWA SHINICHIRO ,  HAYASHI TERUZO

    IPC分类号： C07C2/04 ,  C07B61/00 ,  C07C15/18

    摘要： PROBLEM TO BE SOLVED: To increase the production of a tricyclic aromatic hydrocarbon while maintaining or reducing the production of a bicyclic aromatic hydrocarbon and suppressing the production of unsaturated styrene compound oligomers.
    SOLUTION: A method for producing a monocyclic aromatic hydrocarbon-styrene compound adduct is provided, comprising the step(1) of carrying out a reaction between a monocyclic aromatic hydrocarbon and a styrene compound in a liquid phase in the presence of a solid catalyst in a fixed bed circulation-type reactor, the step(2) of circulating part of the resultant reaction product, the step(3) of obtaining respectively a bicyclic aromatic hydrocarbon and a tricyclic aromatic hydrocarbon as monocyclic aromatic hydrocarbon-styrene compound adducts and the step(4) of circulating part of the resultant bicyclic aromatic hydrocarbon to the reactor, thus adding the styrene compound to the monocyclic aromatic hydrocarbon having at least one hydrogen atom directly bound to an aromatic ring hydrocarbon atom.
    COPYRIGHT: (C)2006,JPO&NCIPI

    摘要翻译： 待解决的问题：增加三环芳烃的生产，同时保持或减少双环芳烃的产生并抑制不饱和苯乙烯化合物低聚物的生产。 提供了一种制备单环芳香烃 - 苯乙烯化合物加合物的方法，包括在固体存在下在液相中进行单环芳族烃和苯乙烯化合物之间的反应的步骤（1） 催化剂在固定床循环型反应器中，循环部分所得反应产物的步骤（2），分别得到双环芳族烃和三环芳烃作为单环芳烃 - 苯乙烯化合物加合物的步骤（3）和 将部分所得双环芳族烃循环到反应器中的步骤（4），从而将苯乙烯化合物加入到具有至少一个与芳环烃原子直接结合的氢原子的单环芳烃中。 版权所有（C）2006，JPO＆NCIPI

    PRODUCTION OF NORBORNENE COMPOUND HAVING CHAIN POLYENE GROUP
    7.
    发明专利
    PRODUCTION OF NORBORNENE COMPOUND HAVING CHAIN POLYENE GROUP 失效

    公开(公告)号：JPH08133993A

    公开(公告)日：1996-05-28

    申请号：JP27537594

    申请日：1994-11-09

    申请人： MITSUI PETROCHEMICAL IND

    发明人： ISHIDA TATSUKAZU ,  YASUDA MASAAKI ,  ONISHI HITOSHI ,  KIHARA NORIAKI

    IPC分类号： B01J31/14 ,  B01J31/24 ,  C07B61/00 ,  C07C2/04 ,  C07C13/42

    摘要： PURPOSE: To obtain the subject compound, excellent in weather and heat resistances, etc., and capable of providing an unsaturated α-olefin-polyene copolymer having a high vulcanization rate by reacting a vinylnorbornene compound with a conjugated diene compound in the presence of a catalyst. CONSTITUTION: A vinylnorbornene compound of formula I (R and R are each H or a 1-5C alkyl) (preferably 5-vinylnorbornene, etc.) is reacted with a conjugated diene compound of formula II (R and R are each H or a 1-5C alkyl; R is H or a 1-4C alkyl, with the proviso that R and R are not simultaneously H) (e.g. isoprene) in the presence of a catalyst to afford the objective compound of formula III. Furthermore, a catalyst comprising a transition metallic complex in which an organic ligand is coordinated with Co chloride and triethylaluminum is preferred as the catalyst. 9146/28}1,2-Bis(diphenylphosphino)ethane]cobalt (II) chloride, etc., are preferred as the transition metallic complex. The reaction is preferably carried out at 70-150 deg.C under 10-70kg/cm ethylene pressure.