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    PURIFICATION METHOD FOR ALPHA-SULFO FATTY ACID SALT
    1.
    发明申请
    PURIFICATION METHOD FOR ALPHA-SULFO FATTY ACID SALT 有权

    公开(公告)号：US20250027009A1

    公开(公告)日：2025-01-23

    申请号：US18714323

    申请日：2022-11-22

    Applicant: BASF SE

    Inventor： Ben Chuan Zhu ,  Fang Qin Lin ,  Yan Xiao ,  Shou Dao Zhang ,  Claudia Brunn ,  Detlev Stanislowski

    IPC: C11C1/00 ,  A61K8/46 ,  A61Q19/00

    Abstract: The present invention is related to a method for purifying crude α-sulfo fatty acid salt obtained by the reaction of fatty acid and sulfur oxides, comprising the following steps: a) diluting the crude α-sulfo fatty acid in a solvent and adjusting the ph from 2 to 4; b) heating up the slurry of a-sulfo fatty acid salt obtained in the step a) until being fully solubilized: c) cooling down the solution of α-sulfo fatty acid salt obtained in the step b) to room temperature gradually to obtain the crystals; d) filtering the crystal obtained in the step c) to remove the motherinsing the filter cake at least twice with acid aqueous solution to obtain the purified α-sulfo fatty acid salt.

    Aqueous surfactant compositions
    2.
    发明授权
    Aqueous surfactant compositions 有权

    公开(公告)号：US10792237B2

    公开(公告)日：2020-10-06

    申请号：US15115706

    申请日：2015-01-23

    Applicant: BASF SE

    Inventor： Claudia Brunn ,  Ansgar Behler ,  Detlev Stanislowski ,  Monika Barbenheim

    IPC: A61Q19/10 ,  A61Q5/02 ,  A61Q19/00 ,  A61Q5/00 ,  A61K8/00 ,  A61K8/72 ,  A61K8/44 ,  A61K8/46 ,  A61Q9/02 ,  A61Q11/00 ,  C11D1/28 ,  C11D1/90 ,  C11D1/94 ,  C11D17/00

    Abstract: An aqueous surfactant composition comprising one or more alpha-sulfo fatty acid disalts (A) of the general formula (I), R1CH(SO3M1)COOM2  (I), wherein the radical R1 is a linear or branched alkyl or alkenyl radical with 6 to 18 carbon atoms and the radicals M1 and M2, independently of one another, are selected from the group H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, one or more amidoalkylbetaines (B) of the general formula (II), R2—CO—NH—(CH2)y—N+(CH3)2—CH2—COO−  (II) in which the radical R2 is a linear or branched alkyl or alkenyl radical with 7 to 19 carbon atoms and the index y is an integer in the range 2 to 4, and water, where specific limiting conditions are to be observed. The compositions are transparent, storage-stable, characterized by good foaming ability and good viscosity, and are suitable for cosmetic products and also detergents and cleaners.

    Aqueous surfactant compositions
    4.
    发明授权
    Aqueous surfactant compositions 有权

    公开(公告)号：US10954473B2

    公开(公告)日：2021-03-23

    申请号：US16301466

    申请日：2017-05-11

    Applicant: BASF SE

    Inventor： Claudia Brunn ,  Ansgar Behler ,  Hans-Christian Raths ,  Detlev Stanislowski ,  Gerhard Hermanns

    IPC: A61K8/00 ,  C11D1/94 ,  A61K8/04 ,  A61K8/23 ,  A61K8/36 ,  A61K8/44 ,  A61K8/46 ,  A61K8/60 ,  A61Q5/02 ,  A61Q9/02 ,  A61Q11/00 ,  A61Q19/10 ,  C11D1/37 ,  C11D3/04 ,  C11D10/04 ,  C11D3/00 ,  C11D1/04 ,  C11D1/28 ,  C11D1/66 ,  C11D1/90 ,  C11D1/12

    Abstract: Aqueous surfactant compositions comprising one or more alpha-sulfo fatty acid disalt (A) of general formula (I) R1CH(SO3M1)COOM2  (I), in which the radical R1 is a linear or branched alkyl or alkenyl radical having 6 to 18 carbon atoms and the radicals M1 and M2, independently of each other, are selected from H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, one or more sulfoketone (B) selected from compounds (F) and compounds (G) wherein the compounds (F) have general formula (VI) R6CH2—CO—CHR7(SO3M8)  (VI), in which the radicals R6 and R7, independently of each other, are a linear or branched alkyl radical having 6 to 18 carbon atoms and the radical M8 is selected from H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, and the compounds (G) have general formula (VII) (SO3M9)R8CH—CO—CHR9(SO3M10)  (VII), in which the radicals R8 and R9, independently of each other, are a linear or branched alkyl radical having 6 to 18 carbon atoms and the radicals M9 and M10, independently of each other, are selected from H, Li, Na, K, Ca/2, Mg/2, ammonium and, alkanolamine, and water, wherein the amount of the compound (A) is greater than the amount of the compound (B), both based on the total aqueous surfactant composition. The compositions have good foaming ability, good skin compatibility, a pleasant sensory feel to the foam, and are suitable for cosmetic products, detergent, and cleaners.

    AQUEOUS SURFACTANT COMPOSITIONS
    5.
    发明申请
    AQUEOUS SURFACTANT COMPOSITIONS 审中-公开

    公开(公告)号：US20190292492A1

    公开(公告)日：2019-09-26

    申请号：US16301466

    申请日：2017-05-11

    Applicant: BASF SE

    Inventor： Claudia Brunn ,  Ansgar Behler ,  Hans-Christian Raths ,  Detlev Stanislowski ,  Gerhard Hermanns

    IPC: C11D1/94 ,  C11D1/37 ,  C11D3/04 ,  A61K8/46 ,  A61K8/36 ,  A61K8/60 ,  A61K8/44 ,  A61K8/23 ,  A61Q5/02 ,  A61Q19/10 ,  A61Q9/02 ,  A61Q11/00 ,  A61K8/04

    Abstract: Aqueous surfactant compositions comprising one or more alpha-sulfo fatty acid disalt (A) of general formula (I) R1CH(SO3M1)COOM2   (I), in which the radical R1 is a linear or branched alkyl or alkenyl radical having 6 to 18 carbon atoms and the radicals M1 and M2, independently of each other, are selected from H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, one or more sulfoketone (B) selected from compounds (F) and compounds (G) wherein the compounds (F) have general formula (VI) R6CH2—CO—CHR7(SO3M8) (VI), in which the radicals R6 and R7, independently of each other, are a linear or branched alkyl radical having 6 to 18 carbon atoms and the radical M8 is selected from H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, and the compounds (G) have general formula (VII) (SO3M9)R8CH—CO—CHR9(SO3M10) (VII), in which the radicals R8 and R9, independently of each other, are a linear or branched alkyl radical having 6 to 18 carbon atoms and the radicals M9 and M10, independently of each other, are selected from H, Li, Na, K, Ca/2, Mg/2, ammonium and, alkanolamine, and water, wherein the amount of the compound (A) is greater than the amount of the compound (B), both based on the total aqueous surfactant composition. The compositions have good foaming ability, good skin compatibility, a pleasant sensory feel to the foam, and are suitable for cosmetic products, detergent, and cleaners.

    Aqueous surfactant compositions
    6.
    发明授权
    Aqueous surfactant compositions 有权

    公开(公告)号：US10370618B2

    公开(公告)日：2019-08-06

    申请号：US15505623

    申请日：2015-08-07

    Applicant: BASF SE

    Inventor： Ansgar Behler ,  Claudia Brunn ,  Detlev Stanislowski

    IPC: A61K8/23 ,  C11D1/10 ,  A61K8/46 ,  C11D1/28 ,  C11D1/37 ,  C11D3/00 ,  C11D11/00 ,  A61K8/44 ,  A61Q5/02 ,  A61Q19/10 ,  A61K8/36 ,  A61Q9/02 ,  A61Q11/00

    Abstract: Aqueous surfactant compositions containing one or more alpha-sulfo fatty acid disalts (A) of the general formula (I), R1CH(SO3M1)COOM2  (I), in which the radical R1 is a linear or branched alkyl or alkenyl radical with 6 to 18 carbon atoms and the radicals M1 and M2, independently of one another, are selected from the group H, Li, Na, K, Ca/2, Mg/2, ammonium and alkanolamines, one or more N-acylglutamic acid compounds (B) of the general formula (II), M3OOC—CH2—CH2—CH(NH—CO—R2)—COOM4  (II) in which the radical R2 is a linear or branched alkyl or alkenyl radical with 7 to 19 carbon atoms and the radicals M3 and M4, independently of one another, are selected from the group H, Li, Na, K, Ca/2, Mg/2, ammonium and alkanolamines, and water, with specific limiting conditions, are disclosed. The compositions are transparent, storage-stable, exhibit good foaming ability, and are suitable for cosmetic products, detergents, and cleaners.

    AQUEOUS SURFACTANT COMPOSITIONS
    8.
    发明申请
    AQUEOUS SURFACTANT COMPOSITIONS 审中-公开
    水性表面活性剂组合物

    公开(公告)号：US20170007520A1

    公开(公告)日：2017-01-12

    申请号：US15115706

    申请日：2015-01-23

    Applicant: BASF SE

    Inventor： Claudia Brunn ,  Ansgar Behler ,  Detlev Stanislowski ,  Monika Barbenheim

    IPC: A61K8/46 ,  A61Q5/02 ,  A61Q19/10 ,  C11D17/00 ,  A61Q11/00 ,  C11D1/28 ,  C11D1/90 ,  C11D1/94 ,  A61K8/44 ,  A61Q9/02

    Abstract: An aqueous surfactant composition comprising one or more alpha-sulfo fatty acid disalts (A) of the general formula (I), R1CH(SO3M1)COOM2  (I), wherein the radical R1 is a linear or branched alkyl or alkenyl radical with 6 to 18 carbon atoms and the radicals M1 and M2, independently of one another, are selected from the group H, Li, Na, K, Ca/2, Mg/2, ammonium, and alkanolamine, one or more amidoalkylbetaines (B) of the general formula (II), R2—CO—NH—(CH2)y-N+(CH3)2—CH2—COO−  (II) in which the radical R2 is a linear or branched alkyl or alkenyl radical with 7 to 19 carbon atoms and the index y is an integer in the range 2 to 4, and water, where specific limiting conditions are to be observed. The compositions are transparent, storage-stable, characterized by good foaming ability and good viscosity, and are suitable for cosmetic products and also detergents and cleaners.

    Abstract translation: 该组合物是透明的，储存稳定的，其特征在于具有良好的起泡能力和良好的粘度，并且适用于化妆品以及洗涤剂和清洁剂。

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