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    Method for isolating polymers from solutions
    1.
    发明授权
    Method for isolating polymers from solutions 失效
    从溶液中分离聚合物的方法

    公开(公告)号：US06506281B1

    公开(公告)日：2003-01-14

    申请号：US09719891

    申请日：2001-03-02

    申请人： Clemens Casper ,  Jörgen Weinschenck ,  Klemens Kohlgrüber ,  Jürgen Heuser ,  Christian Kords ,  Thomas Elsner

    发明人： Clemens Casper ,  Jörgen Weinschenck ,  Klemens Kohlgrüber ,  Jürgen Heuser ,  Christian Kords ,  Thomas Elsner

    IPC分类号： B01D122

    CPC分类号： B01D3/06 ,  C08G64/406 ,  Y10S159/08 ,  Y10S159/10

    摘要： A process of evaporating a viscous polymer solution is described. The process includes: (a) providing a viscous polymer solution including at least 30 wt. % of solvents and monomers; (b) introducing the viscous polymer solution into a heated helix (5), the heated helix having a vapor exit velocity of 200 to 300 m/s, (a film flow including a two-phase mixture of polymer melt, and solvent vapors and monomer vapors being formed within the helix); (c) forwarding the film flow from helix (5) into a heated vapor separator (6); (d) expanding the two-phase mixture of polymer melt, and solvent vapors and monomer vapors of the film flow within vapor separator (6) at an absolute pressure of 10 mbar to 800 mbar, (a bottom product including a concentrated melt of the polymer is formed within the vapor separator); and (e) withdrawing the bottom product from vapor separator (6). Each of the helix (5) and vapor separator (6) have a separate heating device, and each of heating device independently provides a temperature that is above the softening point of the polymer.

    摘要翻译： 描述蒸发粘性聚合物溶液的方法。 该方法包括：（a）提供粘性聚合物溶液，其包含至少30wt。 ％的溶剂和单体; （b）将粘性聚合物溶液引入加热的螺旋（5）中，加热的螺旋具有200-300m / s的蒸气出口速度（包括聚合物熔体和溶剂蒸气的两相混合物的膜流和 单体蒸气在螺旋内形成）; （c）将膜流从螺旋（5）转移到加热的蒸气分离器（6）中; （d）在10毫巴至800毫巴的绝对压力下，将蒸气分离器（6）内的聚合物熔体和溶剂蒸气和单体蒸气的溶剂蒸气和单体蒸气膨胀（包括含有 聚合物形成在蒸气分离器内）; 和（e）从蒸气分离器（6）中取出底部产物。 螺旋（5）和蒸汽分离器（6）中的每一个具有单独的加热装置，并且每个加热装置独立地提供高于聚合物软化点的温度。

    Strand evaporator
    3.
    发明授权
    Strand evaporator 失效
    绞线蒸发器

    公开(公告)号：US06780281B1

    公开(公告)日：2004-08-24

    申请号：US10130757

    申请日：2002-05-22

    申请人： Thomas Elsner ,  Jürgen Heuser ,  Christian Kords ,  Klemens Kohlgrüber

    发明人： Thomas Elsner ,  Jürgen Heuser ,  Christian Kords ,  Klemens Kohlgrüber

    IPC分类号： B01D108

    CPC分类号： B01D1/06 ,  B01D1/04 ,  B01D3/008 ,  B01D19/0021 ,  B29C47/0019 ,  B29C47/003 ,  B29C47/76 ,  C08F6/003 ,  Y10S159/10 ,  Y10S159/15

    摘要： A strand devolatilizer that includes a degassing container, a product inlet, a product distributor, a product outlet and a vapor outlet is disclosed. The product distributor is in the form of a tube distributor with at least one distributor tube (1) and a plurality of die tubes (2) arranged in parallel, each containing a plurality of apertures (15) in the tube wall. The die tubes (2) are preferably arranged in several planes one above the other and staggered laterally relative to one another.

    摘要翻译： 公开了一种包含脱气容器，产品入口，产品分配器，产品出口和蒸汽出口的脱脂剂。 产品分配器是具有管分配器的形式，具有至少一个分配器管（1）和平行布置的多个模具管（2），每个在管壁中包含多个孔（15）。 模具管（2）优选地布置在多个平面中，并且彼此相对并且彼此横向错开。

    Process for separating volatile components from polymers
    5.
    发明授权
    Process for separating volatile components from polymers 失效
    挥发性组分与聚合物分离的方法

    公开(公告)号：US07144981B2

    公开(公告)日：2006-12-05

    申请号：US10684600

    申请日：2003-10-14

    申请人： Thomas König ,  Klemens Kohlgrüber ,  Ulrich Liesenfelder ,  Michael Bierdel ,  Helmut Meyer ,  Richard Weider ,  Jörg Krüger

    发明人： Thomas König ,  Klemens Kohlgrüber ,  Ulrich Liesenfelder ,  Michael Bierdel ,  Helmut Meyer ,  Richard Weider ,  Jörg Krüger

    IPC分类号： C08F6/00

    CPC分类号： C08F6/003

    摘要： A process for concentrating polymers by evaporation is disclosed. The process entails (i) obtaining a mixture containing a polymer and volatile component, the volatile components being present in the mixture at an amount less than 20 wt. % relative to the weight of the mixture, and (ii) introducing the mixture in a downward direction under pressure through a plurality of nozzles arranged vertically and next to one another into a degassing container to form an extrudate. The volatile component contains at least one of residual monomers, oligomers and solvents, and the throughput of the mixture per nozzle is 0.3 to 2 kg/h. The vapor pressure of the volatile component of the extrudate is more than 2.5 bar, and the absolute pressure in the degassing container is 50 to 5000 Pa. The polymer prepared by the process is characterized in that it contains volatile components in an amount of less than 300 ppm.

    摘要翻译： 公开了通过蒸发浓缩聚合物的方法。 该方法需要（i）获得含有聚合物和挥发性组分的混合物，所述挥发性组分以小于20重量％的量存在于混合物中。 相对于混合物重量的％，和（ii）通过垂直且彼此相邻布置的多个喷嘴在压力下向下引入混合物到脱气容器中以形成挤出物。 挥发性组分含有残留单体，低聚物和溶剂中的至少一种，并且每个喷嘴的混合物的生产量为0.3至2kg / h。 挤出物的挥发性成分的蒸气压大于2.5巴，脱气容器中的绝对压力为50〜5000Pa。本方法制备的聚合物的特征在于，其含有挥发性成分的量小于 300 ppm。

    Apparatus for carrying out mass transfer processes
    6.
    发明授权
    Apparatus for carrying out mass transfer processes 失效
    用于进行传质过程的装置

    公开(公告)号：US06761797B2

    公开(公告)日：2004-07-13

    申请号：US09995139

    申请日：2001-11-27

    申请人： Klemens Kohlgrüber ,  Frank Weyrich

    发明人： Klemens Kohlgrüber ,  Frank Weyrich

    IPC分类号： B01D100

    CPC分类号： B29B13/00 ,  B01D3/06 ,  B01D19/0047 ,  B01J4/001 ,  B01J19/24 ,  B29B2013/005 ,  B29K2069/00 ,  Y10S159/10

    摘要： Apparatus for carrying out mass transfer processes with high-viscosity liquids comprising a vertically arranged vessel (1) having a feeder (4) for the liquid to be treated, an outlet (7) for volatile components and an outlet (6) for the treated liquid, the feeder means (4) being equipped with a distributor element (3) having a multiplicity of orifices (8, 10) for subdividing the high-viscosity liquid to be treated into a multiplicity of individual streams, wherein essentially vertically arranged wire loops (2) are disposed in the vicinity of the orifices (8, 10), along which wire loops the high-viscosity liquid runs off under the action of gravity.

    摘要翻译： 用于使用高粘度液体进行质量传递过程的装置，包括垂直布置的容器（1），其具有用于待处理液体的进料器（4），用于挥发性组分的出口（7）和用于处理过的 进料装置（4）装备有具有多个孔（8,10）的分配器元件（3），用于将待处理的高粘度液体细分成多个单独的流，其中基本垂直布置的线环 （2）设置在所述孔（8,10）附近，所述高粘度液体沿重力作用沿着所述孔排出。

    Polyamide composition and method for producing the same
    8.
    发明授权
    Polyamide composition and method for producing the same 失效
    聚酰胺组合物及其制备方法

    公开(公告)号：US06710159B2

    公开(公告)日：2004-03-23

    申请号：US10239982

    申请日：2002-09-26

    申请人： Heinrich Morhenn ,  Dieter Göbbels ,  Cliff Scherer ,  Frank Weyrich ,  Konrad Triebeneck ,  Klemens Kohlgrüber

    发明人： Heinrich Morhenn ,  Dieter Göbbels ,  Cliff Scherer ,  Frank Weyrich ,  Konrad Triebeneck ,  Klemens Kohlgrüber

    IPC分类号： C08G6908

    CPC分类号： C08G69/28 ,  C08G69/16 ,  C08G69/46

    摘要： A process for producing a polyamide or copolyamide freed from volatile constituents by removing the volatile constituents, in particular the monomers and dimers, in at least two stages from the polymer melt by using an, in particular, gaseous entrainer is described. The invention also relates to polyamide compositions made of polyamide 6 or a copolyamide with a reduced volatile constituent content, as well as moulding compositions made of the above-mentioned polyamides, and moulded articles and fibers which are produced from these moulding compositions.

    摘要翻译： 描述了通过使用特别是气体夹带剂从聚合物熔体至少两个阶段除去挥发性成分，特别是单体和二聚体，从而形成不含挥发性成分的聚酰胺或共聚酰胺的方法。 本发明还涉及由聚酰胺6或具有降低的挥发性组分含量的共聚酰胺制成的聚酰胺组合物以及由上述聚酰胺制成的模塑组合物，以及由这些模塑组合物制备的模塑制品和纤维。