Polysulfide-based polyurethane sealant for insulating glass
    1.
    发明授权
    Polysulfide-based polyurethane sealant for insulating glass 失效
    用于中空玻璃的聚硫醚基聚氨酯密封剂

    公开(公告)号:US06383324B1

    公开(公告)日:2002-05-07

    申请号:US09448125

    申请日:1999-11-24

    IPC分类号: B32B1700

    摘要: An insulated glass sealant having the best characteristics of polysulfides and polyurethanes rather than the worst is made from a polysulfide-based polyurethane prepared by a one-step procedure wherein a randomly copolymeric hydroxyl-terminated polysulfide polyacetal is reacted with a polyisocyanate at a ratio of from about 1:1 to about 1:1.2 on an equivalents basis. The copolymeric hydroxyl-terminated polysulfide polyacetal is made by the condensation of formaldehyde with a mixture of a dithiodialkylene glycol and an aliphatic or cycloaliphatic diol.

    摘要翻译: 具有多硫化物和聚氨酯的最佳特性而不是最差的绝缘玻璃密封剂由通过一步法制备的多硫化物基聚氨酯制备,其中无规共聚的羟基封端的多硫化物聚缩醛与多异氰酸酯以 约1:1至约1:1.2。 共聚羟基封端的多硫化物聚缩醛是通过甲醛与二硫代二亚烷基二醇和脂族或脂环族二醇的混合物的缩合形成的。

    3-9-diphosphaspiroundecane-stabilized polymer compositions
    5.
    发明授权
    3-9-diphosphaspiroundecane-stabilized polymer compositions 失效
    3-9-二磷杂螺十一烷稳定的聚合物组合物

    公开(公告)号:US5308901A

    公开(公告)日:1994-05-03

    申请号:US126744

    申请日:1993-09-27

    IPC分类号: C07F9/6574 C08K5/527 C08K5/52

    CPC分类号: C07F9/65746 C08K5/527

    摘要: The present invention provides an improved process for making diphosphaspiroundecanes and product-by-process, wherein the process comprises reacting a hydroxyl-substituted organic compound, phosphorous trichloride and pentaerythritol to form an organic-substituted diphosphaspiroundecane such that formation of said organic-substituted diphosphaspiroundecane takes place in the presence of a tri-n-alkylamine having n-alkyl moieties such that each n-alkyl moiety has at least three carbon atoms. The present invention is also directed to bis-3,9-(2,6-di-t-alkyl-4-alkylphenoxy)-2,4,8,10-tetroxa-3,9-diphosphasprio[5.5]undecanes and polymer composition containing an effective amount of same.

    摘要翻译: 本发明提供了制备二磷杂螺十一烷和逐步处理的改进方法,其中该方法包括使羟基取代的有机化合物,三氯化磷和季戊四醇反应形成有机取代的二磷杂螺十一烷,使得形成所述有机取代的二磷杂螺十一烷取 在具有正烷基部分的三正烷基胺存在下,使得每个正烷基部分具有至少三个碳原子。 本发明还涉及二-3,9-(2,6-二叔烷基-4-烷基苯氧基)-2,4,8,10-四氧杂-3,9-二磷杂五[5.5]十一烷和聚合物 组合物含有效量相同。

    3-9-diphosphaspiroundecanes and process for making
3-9-diphosphaspiroundecanes
    6.
    发明授权
    3-9-diphosphaspiroundecanes and process for making 3-9-diphosphaspiroundecanes 失效
    3-9-二磷酸吡啶类化合物及其制备方法3-9-双羟基磷酸酯

    公开(公告)号:US5137950A

    公开(公告)日:1992-08-11

    申请号:US765409

    申请日:1991-09-25

    IPC分类号: C07F9/6574 C08K5/52 C08K5/527

    CPC分类号: C07F9/65746 C08K5/527

    摘要: The present invention provides an improved process for making diphosphaspiroundecanes and product-by-process, wherein the process comprises reacting a hydroxyl-substituted organic compound, phosphorous trichloride and pentaerythritol to form an organic-substituted diphosphaspiroundecane such that formation of said organic-substituted diphosphaspiroundecane takes place in the presence of a tri-n-alkylamine having n-alkyl moieties such that each n-alkyl moiety has at least three carbon atoms. The present invention is also directed to bis-3,9-(2,6-di-t-alkyl-4-alkylphenoxy)-2,4,8,10-tetroxa-3,9-diphosphasprio[5.5]undecanes and polymer compositions containing an effective amount of same.