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    Flame retardant composition
    3.
    发明申请
    Flame retardant composition 审中-公开
    阻燃组合物

    公开(公告)号：US20070252116A1

    公开(公告)日：2007-11-01

    申请号：US11797144

    申请日：2007-05-01

    申请人： Mark Gelmont ,  Michael Peled ,  Dina Alon ,  Ron Frim

    发明人： Mark Gelmont ,  Michael Peled ,  Dina Alon ,  Ron Frim

    IPC分类号： C09K21/00

    CPC分类号： C09K21/14 ,  C08K5/0066 ,  C08L75/04

    摘要： A flame retardant composition which comprises a first liquid, which is selected from the group consisting of non-halogenated polyols and mixtures thereof; a second liquid, which is selected from the group consisting of halogenated polyols or mixtures thereof; and tetrabromobisphenol A.

    摘要翻译： 一种阻燃组合物，其包含选自非卤化多元醇及其混合物的第一液体; 第二液体，其选自卤代多元醇或其混合物; 和四溴双酚A.

    Process of preparing bromopicrin
    6.
    发明申请
    Process of preparing bromopicrin 有权
    溴氰菊酯制备方法

    公开(公告)号：US20100152501A1

    公开(公告)日：2010-06-17

    申请号：US11989585

    申请日：2006-08-22

    申请人： Jakob Oren ,  Leah Golan ,  Ron Frim

    发明人： Jakob Oren ,  Leah Golan ,  Ron Frim

    IPC分类号： C07C205/02

    CPC分类号： C07C201/12 ,  C07C205/08

    摘要： Process of preparing high purity bromopicrin, and high purity bromopicrin produced therefrom. Providing a mixture of nitromethane and bromine, and preferably water, and absent of organic solvent. Adding an aqueous solution of an alkaline substance to the mixture, thereby providing a reaction mixture containing bromopicrin, the adding performed such that no excess of the alkaline substance occurs in the reaction mixture during the adding. Collecting the organic phase (containing the bromopicrin) from the reaction mixture. No need for subjecting the organic phase of the reaction mixture to distillation or extraction, for obtaining near quantitative yield of bromopicrin having purity of at least equal to or greater than 96 weight percent. Process parameters controlling selectivity of reaction forming bromopicrin are molar ratio of bromine and nitromethane in the mixture; reaction temperature while bromopicrin is formed; concentration of the alkaline substance in the aqueous solution; and reaction time.

    摘要翻译： 制备高纯度溴氰菊酯和由其制备的高纯度溴氰菊酯的方法。 提供硝基甲烷和溴的混合物，优选水，并且不存在有机溶剂。 向混合物中加入碱性物质的水溶液，由此提供含有溴氰菊酯的反应混合物，进行添加，使得在添加期间反应混合物中不会发生过量的碱性物质。 从反应混合物中收集有机相（含溴氰菊酯）。 不需要使反应混合物的有机相进行蒸馏或萃取，以获得纯度至少等于或大于96重量％的溴定额素的近定量产率。 控制反应形成溴氰菊酯的选择性的工艺参数是混合物中溴和硝基甲烷的摩尔比; 反应温度，同时形成溴化铁; 碱性物质在水溶液中的浓度; 和反应时间。

    Continuous process of preparing bromopicrin
    9.
    发明授权
    Continuous process of preparing bromopicrin 有权
    制备溴氰菊酯的连续工艺

    公开(公告)号：US08415513B2

    公开(公告)日：2013-04-09

    申请号：US12601547

    申请日：2008-05-26

    申请人： Jakob Oren ,  Nasif Yassin ,  Ron Frim

    发明人： Jakob Oren ,  Nasif Yassin ,  Ron Frim

    IPC分类号： C07C205/00

    CPC分类号： C07C201/12 ,  C07C205/08

    摘要： A continuous process of preparing bromopicrin is disclosed. The process is effected by transferring a continuous flow of a first mixture and a continuous flow of a second mixture into a first reactor, the first mixture containing nitromethane and bromine and the second mixture containing an aqueous solution of an alkaline substance, to thereby obtain a reaction mixture which comprises bromopicrin in said first reactor; and collecting the bromopicrin from the reaction mixture. Highly pure bromopicrin obtained by this process is also disclosed.

    摘要翻译： 公开了制备溴氰菊酯的连续方法。 该方法通过将第一混合物的连续流和第二混合物的连续流转移到第一反应器中，第一混合物含有硝基甲烷和溴，第二混合物含有碱性物质的水溶液，从而获得 在所述第一反应器中包含溴化苦素的反应混合物; 并从反应混合物中收集溴氰菊酯。 还公开了通过该方法获得的高纯度溴氰菊酯。