公开(公告)号：US08546619B2

公开(公告)日：2013-10-01

申请号：US12735886

申请日：2009-02-26

Applicant: Jacob Oren

Inventor： Jacob Oren

IPC: C07C201/12 ,  C07C205/08

CPC classification number: C07C201/10 ,  C07C201/12 ,  C07C205/15

Abstract: The invention provides a process for preparing bronopol, which process comprises charging a reaction vessel with water, bromopicrin, nitromethane and paraformaldehyde, gradually feeding a base into said reaction vessel under stirring, bringing the reaction to completion and separating bronopol from the aqueous reaction mixture.

Abstract translation: 本发明提供了一种制备青霉酚的方法，该方法包括向反应容器中加入水，溴氰菊酯，硝基甲烷和多聚甲醛，在搅拌下逐渐向碱性物质中加入碱，使反应完成，并从反应混合物中分离出丙三醇。

公开(公告)号：US09018324B2

公开(公告)日：2015-04-28

申请号：US14110943

申请日：2012-04-05

Applicant: Jacob Oren

Inventor： Jacob Oren

IPC: C07C67/14 ,  C08F220/68 ,  C08F120/22 ,  C08F220/22

CPC classification number: C07C67/10 ,  C07C67/14 ,  C08F22/10 ,  C08F120/22 ,  C08F220/22 ,  C08F220/68 ,  C07C69/653

Abstract: The invention relates to a process for preparing pentabromobenzyl acrylate through the reaction of pentahalobenzyl halide with a salt of acrylic acid in water-immiscible solvent, wherein said salt is in aqueous form and the reaction is carried out in the presence of a phase transfer catalyst. A process for polymerizing the pentabromobenzyl acrylate in halogenated aromatic solvent and the poly (pentabromobenzyl acrylate) obtained are also disclosed.

Abstract translation: 本发明涉及一种通过五卤代苄基卤化物与丙烯酸盐在水不混溶溶剂中的反应制备丙烯酸五溴苄酯的方法，其中所述盐为水溶液形式，反应在相转移催化剂存在下进行。 还公开了在卤代芳族溶剂中聚合丙烯酸五溴苄酯和获得的聚（五溴苄基丙烯酸酯）的方法。

公开(公告)号：US20110065964A1

公开(公告)日：2011-03-17

申请号：US12735886

申请日：2009-02-26

Applicant: Jacob Oren

Inventor： Jacob Oren

IPC: C07C201/12

CPC classification number: C07C201/10 ,  C07C201/12 ,  C07C205/15

Abstract: The invention provides a process for preparing bronopol, which process comprises charging a reaction vessel with water, bromopicrin, nitromethane and paraformaldehyde, gradually feeding a base into said reaction vessel under stirring, bringing the reaction to completion and separating bronopol from the aqueous reaction mixture.

Abstract translation: 本发明提供了一种制备青霉酚的方法，该方法包括向反应容器中加入水，溴氰菊酯，硝基甲烷和多聚甲醛，在搅拌下逐渐向碱性物质中加入碱，使反应完成，并从反应混合物中分离出丙三醇。

公开(公告)号：US4585636A

公开(公告)日：1986-04-29

申请号：US661710

申请日：1984-10-17

Applicant: Alexander Iosef ,  Menachem Bar-on ,  Jacob Oren ,  Dagobert Kellerman

Inventor： Alexander Iosef ,  Menachem Bar-on ,  Jacob Oren ,  Dagobert Kellerman

IPC: C01B25/234 ,  C01B25/46 ,  C01B25/16

CPC classification number: C01B25/461 ,  C01B25/234 ,  C01B25/462

Abstract: The present invention relates to an improved process for the manufacture of purified phosphoric acid from phosphate rock. According to the invention, phosphate rock is decomposed by a mineral acid selected from hydrochloric acid, sulfuric acid or mixtures thereof. The dissolution liquor obtained is reacted with a calcium-containing compound such as calcium oxide, calcium carbonate, tricalcium phosphate and fines of phosphate rock producing an aqueous solution containing monocalcium phosphate in an amount corresponding to between 0.4% to 5.5% by wt CaO. After the separation of the precipitated solids, the clarified solution is extracted by an organic solvent having the property to extract the phosphate component. The phosphoric acid is subsequently recovered from the solvent extract by known methods such as washing or distillation.

Abstract translation: 本发明涉及从磷酸盐岩制造纯化磷酸的改进方法。 根据本发明，磷酸盐岩由选自盐酸，硫酸或其混合物的无机酸分解。 将得到的溶解液与含钙化合物如氧化钙，碳酸钙，磷酸三钙和磷酸盐岩的细粉反应，生成含有相当于0.4〜5.5重量％CaO的磷酸一钙的水溶液。 析出的固体分离后，通过具有提取磷酸盐成分性质的有机溶剂提取澄清溶液。 随后通过已知的方法例如洗涤或蒸馏从溶剂提取物中回收磷酸。

公开(公告)号：US20140121338A1

公开(公告)日：2014-05-01

申请号：US14110943

申请日：2012-04-05

Applicant: Jacob Oren

Inventor： Jacob Oren

IPC: C07C67/14 ,  C08F220/68

CPC classification number: C07C67/10 ,  C07C67/14 ,  C08F22/10 ,  C08F120/22 ,  C08F220/22 ,  C08F220/68 ,  C07C69/653

Abstract: The invention relates to a process for preparing pentabromobenzyl acrylate through the reaction of pentahalobenzyl halide with a salt of acrylic acid in water-immiscible solvent, wherein said salt is in aqueous form and the reaction is carried out in the presence of a phase transfer catalyst. A process for polymerizing the pentabromobenzyl acrylate in halogenated aromatic solvent and the poly (pentabromobenzyl acrylate) obtained are also disclosed.

Abstract translation: 本发明涉及一种通过五卤代苄基卤化物与丙烯酸盐在水不混溶溶剂中的反应制备丙烯酸五溴苄酯的方法，其中所述盐为水溶液形式，反应在相转移催化剂存在下进行。 还公开了在卤代芳族溶剂中聚合丙烯酸五溴苄酯和获得的聚（五溴苄基丙烯酸酯）的方法。

公开(公告)号：US5340445A

公开(公告)日：1994-08-23

申请号：US896833

申请日：1992-06-11

Applicant: Joshua Hermolin ,  Hugo Keselman ,  Jacob Oren

Inventor： Joshua Hermolin ,  Hugo Keselman ,  Jacob Oren

IPC: C07B61/00 ,  B01D3/10 ,  B01D3/34 ,  C07C209/84 ,  C07C211/57 ,  C07C213/10 ,  C07C217/84 ,  C07C217/90

CPC classification number: C07C209/84 ,  B01D3/10 ,  B01D3/34 ,  C07C213/10 ,  C07C2102/08

Abstract: Diaminodiphenyl-compounds of the structure selected from: ##STR1## wherein R.sub.1 and R.sub.2 can be: H, --CH.sub.3, --C.sub.2 H.sub.5, --C.sub.3 H.sub.7, --C.sub.4 H.sub.9 or ##STR2## Y can be: C(CH.sub.3).sub.2, ##STR3## n=0; 1. are purified by distilling the crude product obtained under vacuum in one step, in the presence of one or more alkaline bases.

Abstract translation: 其中R 1和R 2可以是：H，-CH 3，-C 2 H 5，-C 3 H 7，-C 4 H 9或Y可以是：C（CH 3）2， 图像> n = 0; 通过在一个或多个碱性碱的存在下，在一个步骤中蒸馏在真空下获得的粗产物来纯化。