Manufacture of gamma-iron(III) oxide
    1.
    发明授权
    Manufacture of gamma-iron(III) oxide 失效
    制造γ-铁(III)氧化物

    公开(公告)号:US4061725A

    公开(公告)日:1977-12-06

    申请号:US732899

    申请日:1976-10-15

    摘要: Acicular gamma-iron(III) oxide is manufactured by reacting an iron(II) salt solution with an aqueous solution of an alkali metal hydroxide and oxidizing the resulting suspension of iron(II) hydroxide in three stages. In a first stage, at most from 0.1 to 4% by weight of the amount of iron(II) hydroxide originally present is oxidized in the course of from 0.1 to 4 hours, in a second stage from 10 to 25% by weight of the said original amount are oxidized in the course of from 1.5 to 6 hours and in a third stage the remaining amount is oxidized. After the oxidation, the goethite formed is reduced to magnetite and the latter is then oxidized to acicular gamma-iron(III) oxide.

    摘要翻译: 通过使铁(II)盐溶液与碱金属氢氧化物的水溶液反应并将所得的氢氧化铁(II)悬浮液分三个阶段进行氧化,从而制造针状γ-铁(III)。 在第一阶段中,最初存在的氢氧化铁(II)的量的0.1至4重量%在0.1至4小时的过程中被氧化,在第二阶段中氧化为10至25重量% 所述原始量在1.5至6小时的过程中被氧化,在第三阶段中剩余量被氧化。 氧化后,形成的针铁矿被还原成磁铁矿,后者被氧化成针状的γ-铁(III)氧化物。

    Magnetic recording media
    7.
    发明授权
    Magnetic recording media 失效
    磁记录媒体

    公开(公告)号:US3996407A

    公开(公告)日:1976-12-07

    申请号:US533973

    申请日:1974-12-18

    摘要: Magnetic recording media comprising a non-magnetizable flexible base and a firmly adhering magnetic coating based on a dispersion, containing a silane, of a magnetic pigment in a polymeric binder, and a process for their manufacture. The silane is an aminoalkylsilane R.sub.n Si(OR').sub.4-n, wherein n is 1, 2 or 3, R' is alkyl of 1 to 8 carbon atoms and R is aminoalkyl of the formula with one or more primary and/or secondary amino groups and from 3 to 11 carbon atoms. Magnetic recording media comprising a magnetic coating containing such a silane exhibit better abrasion resistance and better electromagnetic properties than comparable coatings.

    摘要翻译: 磁性记录介质包括不可磁化的柔性基底和基于包含硅烷的分散体的牢固粘附的磁性涂层,所述分散体包含聚合物粘合剂中的磁性颜料及其制造方法。 硅烷是氨基烷基硅烷RnSi(OR')4-n,其中n是1,2或3,R'是1至8个碳原子的烷基,R是具有一个或多个伯和/或仲氨基的氨基烷基 基团和3至11个碳原子。 包含含有这种硅烷的磁性涂层的磁记录介质比同类涂层表现出更好的耐磨性和更好的电磁特性。