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    Fluorinated isopropyl derivatives
    1.
    发明授权
    Fluorinated isopropyl derivatives 失效
    氟化异丙基衍生物

    公开(公告)号：US3911024A

    公开(公告)日：1975-10-07

    申请号：US12589771

    申请日：1971-03-18

    申请人： CROIX LOUISE S

    发明人： CROIX LOUISE S

    IPC分类号： C07C43/12 ,  C07C43/00 ,  C07C41/04

    CPC分类号： C07C43/12

    摘要： This invention relates to certain novel fluorinated isopropyl methyl ethers represented by the following formula:

    wherein X is chlorine of fluorine, X'' is chlorine or fluorine, and R is CH3 or C2H5. The compounds can be prepared by reacting the corresponding halogenated isopropyl alcohol with a lower alkyl sulfate or halide in the presence of an alkaline metal hydroxide. The compounds are useful as solvents or dispersants for fluorinated materials, and the compounds (CF3)2CHOCH3, CF2CL(CF3)CHOCH3, and (CF2Cl)2CHOCH3, exhibit anesthetic properties in mammals.

    摘要翻译： 本发明涉及由下式表示的某些新的氟化异丙基甲基醚：CF2X ANGLE CH-O-R CF2X'其中X是氟的氯，X'是氯或氟，R是CH3或C2H5。 化合物可以通过在碱金属氢氧化物的存在下使相应的卤代异丙醇与低级烷基硫酸盐或卤化物反应来制备。 这些化合物可用作氟化材料的溶剂或分散剂，化合物（CF 3）2 CHOCH 3，CF 2 CL（CF 3）CHOCH 3和（CF 2 Cl）2 CHOCH 3在哺乳动物中表现出麻醉性质。

    Method of preparing of cf{11 chc10chf{11
    3.
    发明授权
    Method of preparing of cf{11 chc10chf{11 失效
    制备CF（11CHC10CHF）的方法

    公开(公告)号：US3637477A

    公开(公告)日：1972-01-25

    申请号：US3637477D

    申请日：1970-02-20

    申请人： AIR REDUCTION

    发明人： CROIX LOUISE S

    IPC分类号： C07C43/12 ,  C07C41/04 ,  C07C41/12

    CPC分类号： C07C43/12 ,  C07C43/123

    摘要： Trifluoroethanol, an alkali metal hydroxide, and difluorochloromethane are reacted to prepare 2,2,2-trifluoroethyl difluoromethyl ether which is recovered and chlorinated in the presence of photoenergy to prepare 1-chloro-2,2,2-trifluoroethyl difluoromethyl ether which exhibits excellent anesthetic properties in inhalation susceptible mammals.

    摘要翻译： 使三氟乙醇，碱金属氢氧化物和二氟氯甲烷反应以制备2,2,2-三氟乙基二氟甲基醚，其在光能存在下回收和氯化以制备显示出优异的1-氯-2,2,2-三氟乙基二氟甲基醚 吸入敏感哺乳动物的麻醉性质。

    Process for the continuous preparation of addition products of ethylene oxide
    5.
    发明授权
    Process for the continuous preparation of addition products of ethylene oxide 失效
    连续制备乙烯氧化添加剂的方法

    公开(公告)号：US3436426A

    公开(公告)日：1969-04-01

    申请号：US3436426D

    申请日：1967-11-13

    申请人： HENKEL & CIE GMBH

    发明人： FISCHER HANNES ,  STEIN WERNER

    IPC分类号： C07C43/205 ,  C07B61/00 ,  C07C41/00 ,  C07C41/02 ,  C07C41/03 ,  C07C43/11 ,  C07C67/00 ,  C08G65/00 ,  C08G65/28 ,  C07C41/04

    CPC分类号： C07C41/03 ,  C07B61/00 ,  C07C43/11 ,  C07C43/23 ,  C07C43/1785

    摘要： Addition products of ethylene oxide are formed by passing alcohols, phenols, or their addition products with ethylene oxide or propylene oxide, with ethylene oxide in a molar ratio of 1:1 to 1:4 in the presence of conventional alkaline catalysts, through an extended tube-like reactor having a small cross-section, and surrounded by a heat exchanger, the mixture is at such a pressure that it is in the liquid state and reaches 170-230 DEG C. in the first half of the reactor zone, and in the second half passes through a maximum of 240-330 DEG C., and has a residence time in the reactor zone of 8-150 seconds, and the product leaving the zone is immediately cooled to below 100 DEG C. The process adds on up to four moles of ethylene oxide. Examples describe the addition of ethylene oxide to lauryl alcohol, nonylphenol, a mixture of C12-C14 fatty alcohols and a mixture of unsaturated predominantly C18 alcohols.

    Preparation of methyl-beta-phenyl-ethyl-ether
    8.
    发明授权
    Preparation of methyl-beta-phenyl-ethyl-ether 失效
    甲基 - 苯乙烯 - 乙醚的制备

    公开(公告)号：US3734970A

    公开(公告)日：1973-05-22

    申请号：US3734970D

    申请日：1970-09-21

    申请人： CHATURVEDI Y

    发明人： CHATURVEDI Y

    IPC分类号： C07C41/16 ,  C07C41/04

    CPC分类号： C07C41/16 ,  C07C43/205

    摘要： METHYL-B-PHENYL-ETHYL-ETHER IS PREPARED BY TREATING ALUMINUM-B-PHENYL-ETHOXIDE WITH DIMETHYLSULPHATE AT WATER BATH TEMPERATURE. THE UNREACTED DIMETHYL SUPPHATE IS DESTROYED BY BOILING WITH CAUSTIC SODIA SOLUTION AND THE LIGHTER LAYER CONTAINING METHYL-B-PHENYL-ETHER IS SEPARATED BY FRACTIONATION. THE ALUMINIUM-B-PHENYL-ETHOXIDE IS PREPARED BY TREATING B-PHENYL-ETHYL-ALCOHOL WITH AL/HG COUPLE IN THE PRESENCE OF CARBON TETRACHLORIDE.

    Method for the preparation of fluorinated ethers
    9.
    发明授权
    Method for the preparation of fluorinated ethers 失效
    氟化物的制备方法

    公开(公告)号：US3558721A

    公开(公告)日：1971-01-26

    申请号：US3558721D

    申请日：1967-12-22

    申请人： ALLIED CHEM

    发明人： YAO CHARLES CHENG-YU

    IPC分类号： A47B57/00 ,  A47G29/02 ,  C07C43/12 ,  C07C41/04 ,  C07C41/06

    CPC分类号： C07C43/12 ,  Y10S516/01

    摘要： IN A METHOD FOR PREPARING FLUORINE-CONTAINING ETHERS OF THE FORMULA

    F-C(-R1)(-R2)-O-A-E

    WHEREIN R1 AND R2 ARE INDEPENDENTLY EITHER FLUORINE OR CERTAIN FLUORINE-CONTAINING ALIPHATIC RADICALS, OR, TAKEN TOGETHER, FORM A FLUORINE-CONTAINING CYCLOALIPHATIC STRUCTURE, WITH THE PROVISO THAT ONLY ONE OF R1 OR R2 MAY BE FLUORINE, WHEREIN A IS A LINEAR, BRANCHED CHAIN OR CYCLIC ALKYLENE OR HALOALKYLENE RADICAL, AND WHEREIN E IS CL, BR OR I, BY REACTING A FLUORINATED KETONE OR ACYL FLUORIDE WITH AN IONIZABLE INORGANIC FLUORIDE TO FORM AN ORGANIC FLUORIDE SALT, AND REACTING THE ORGANIC FLUORIDE SALT WITH AN OLEFIN AND A HALOGEN TO FORM THE FLUORINE-CONTAINING ETHER, YIELDS ARE IMPROVED, REACTION TIMES ARE SHORTENED, AND BY-PRODUCT FORMATION IS REDUCED BY IMPROVEMENTS COMPRISING USE OF SUPERATMOSPHERIC REACTION PRESSURE, OR USE OF SUPERATMOSPHERIC REACTION PRESSURE TOGETHER WITH OBSERVATION OF CERTAIN CRITICAL REACTANT MOLAR RATIOS, AND/OR OPERATION WITHIN CERTAIN TEMPERATURE LIMITS.