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    Production of propylene glycol monoalkyl ether
    3.
    发明授权
    Production of propylene glycol monoalkyl ether 有权
    丙二醇单烷基醚的生产

    公开(公告)号：US09586881B2

    公开(公告)日：2017-03-07

    申请号：US14880653

    申请日：2015-10-12

    Applicant: Lyondell Chemical Technology, L.P.

    Inventor： Xiangmin Li ,  Lawrence M. Candela ,  Mark A. Liepa ,  David W. Leyshon

    IPC: C07C41/03 ,  C07C41/44 ,  C07C41/42

    CPC classification number: C07C41/03 ,  C07C41/42 ,  C07C41/44 ,  C07C43/13

    Abstract: Processes for producing propylene glycol monoalkyl ether are described herein and include contacting propylene oxide and an alcohol in the presence of an alkali or alkaline earth metal alkoxide catalyst to produce an alkoxylation mixture including propylene glycol monoalkyl ether; distilling the alkoxylation mixture to produce a first overhead stream including propylene oxide and the alcohol and a first bottoms stream including propylene glycol monoalkyl ether; distilling the first bottoms stream to produce a second overhead stream including purified propylene glycol monoalkyl ether and a second bottoms stream including heavier byproducts; further distilling the second bottoms stream to form a resulting bottoms stream including caustic and heavier byproducts; introducing an alkali metal borohydride into at least a portion of the resulting bottoms stream to form an alkali metal borohydride containing stream; and introducing the alkali metal borohydride containing stream into one or more distillations upstream of recovery of the second overhead stream.

    Abstract translation: 本文描述了制备丙二醇单烷基醚的方法，包括在碱金属或碱土金属醇盐催化剂的存在下使环氧丙烷与醇接触以产生包括丙二醇单烷基醚的烷氧基化混合物; 蒸馏所述烷氧基化混合物以产生包含环氧丙烷和所述醇的第一塔顶物流和包含丙二醇单烷基醚的第一塔底物流; 蒸馏第一塔底物流以产生包括纯化的丙二醇单烷基醚和包含较重副产物的第二塔底物流的第二塔顶物流; 进一步蒸馏第二塔底物流以形成包含苛性和重副产物的所得底部物流; 将至少一部分所得的塔底物流中的碱金属硼氢化物引入以形成含碱金属硼氢化物的流; 并将含有碱金属硼氢化物的料流引入到第二塔顶馏出物回收上游的一个或多个蒸馏物中。

    PROCESS FOR PRODUCING ALKYLENE OXIDE ADDUCT AND ALKYLENE OXIDE ADDUCT
    4.
    发明申请
    PROCESS FOR PRODUCING ALKYLENE OXIDE ADDUCT AND ALKYLENE OXIDE ADDUCT 审中-公开
    生产氧化亚烷基氧化物和氧化亚铁添加剂的方法

    公开(公告)号：US20160368847A1

    公开(公告)日：2016-12-22

    申请号：US15117683

    申请日：2014-03-10

    Applicant: TAKEMOTO YUSHI KABUSHIKI KAISHA

    Inventor： Akihiro Furuta ,  Kazuhisa Okada

    IPC: C07C41/03 ,  C07C43/13

    CPC classification number: C07C41/03 ,  B01J19/0093 ,  C07C43/13 ,  C07C213/04 ,  C08G65/26 ,  C08G65/2609 ,  C08G65/2621 ,  C08G65/2696 ,  C07C43/11 ,  C07C217/50

    Abstract: This is to provide a process for producing an alkylene oxide adduct which can continuously produce the alkylene oxide adduct with an optional size from a small size to a large size, a temperature and a pressure at the time of the addition reaction can be controlled with high precision, and as a result, the alkylene oxide adduct with high quality having no coloring and narrow molecular weight distribution can be continuously produced, and the above can be accomplished simultaneously, and such an alkylene oxide adduct.An alkylene oxide adduct was produced by using a microflow reactor having a flow passage with an inner diameter of 0.05 to 3.5 mm, continuously supplying a predetermined amount of alkylene oxide and a predetermined amount of an organic compound having an active hydrogen atom(s) to the flow passage in a liquid state, and these materials were reacted while passing therethrough under the conditions of a temperature of the flow passage of 70 to 200° C. and a pressure of the supply port of the flow passage of 1 to 10 MPa.

    Abstract translation: 通过使用具有内径为0.05〜3.5mm的流路的微流反应器，连续供给预定量的烯化氧和预定量的具有活性氢原子的有机化合物，制备环氧烷加合物， 流动通道处于液态，并且在流路温度为70〜200℃，流路供给口的压力为1〜10MPa的条件下使这些材料通过时反应。

    Alkoxylation of crude bisphenol A
    7.
    发明授权
    Alkoxylation of crude bisphenol A 有权
    粗双酚A的烷氧基化

    公开(公告)号：US09365475B2

    公开(公告)日：2016-06-14

    申请号：US14164433

    申请日：2014-01-27

    Applicant: BAKER HUGHES INCORPORATED

    Inventor： Philip L. Leung

    IPC: C07C41/03 ,  C07C41/09 ,  C08G65/26 ,  C08G65/30

    CPC classification number: C07C41/09 ,  C07C41/03 ,  C08G65/2609 ,  C08G65/2648 ,  C08G65/30 ,  C07C43/23

    Abstract: Crude bisphenol A containing a ketone solvent remaining form its manufacture and having a melting point of 150° C. or higher may be reacted with one or more alkylene oxide, in the absence of any added ketone solvent, at reduced temperatures compared with conventional, molten methods to give a fully alkoxylated adduct product having reduced color. By at least partially alkoxylating the bisphenol A, its potential for crystallization is disrupted and the partially alkoxylated bisphenol A has a lower melting point than the original bisphenol A permitting it to be more readily further alkoxylated at the reaction temperature. The alkoxylation reaction may be conducted at a temperature in the range of about 30 to about 140° C. Suitable catalysts may include tertiary amines or caustic compounds such as NaOH and KOH.

    Abstract translation: 在不存在任何添加的酮溶剂的情况下，含有保留在其制造中并且具有150℃或更高的熔点的酮溶剂的粗双酚A与常规的熔融态相比可以在降低的温度下与一种或多种环氧烷反应 得到具有降低颜色的完全烷氧基化的加合物产物的方法。 通过至少部分烷氧基化双酚A，其结晶的可能性被破坏，并且部分烷氧基化双酚A具有比原始双酚A更低的熔点，从而允许其在反应温度下更容易进一步烷氧基化。 烷氧基化反应可以在约30至约140℃的温度范围内进行。合适的催化剂可包括叔胺或苛性化合物如NaOH和KOH。

    Use of tris(2-hydroxyphenyl)methane derivatives for tertiary mineral oil production
    10.
    发明授权
    Use of tris(2-hydroxyphenyl)methane derivatives for tertiary mineral oil production 有权
    三（2-羟基苯基）甲烷衍生物用于三次矿物油生产的用途

    公开(公告)号：US09212545B2

    公开(公告)日：2015-12-15

    申请号：US13653946

    申请日：2012-10-17

    Applicant: Wintershall Holding GmbH

    Inventor： Günter Oetter ,  Björn Heinz ,  Markus Hansch ,  Horst Weiss ,  Peter Deglmann ,  Vandana Kurkal-Siebert ,  Frank Heilmann ,  Ravindra Aglave ,  Lorenz Siggel ,  Benjamin Wenzke

    IPC: E21B43/16 ,  C07C41/03 ,  C09K8/584 ,  C07C39/10 ,  C08G65/26 ,  C08G65/334

    CPC classification number: E21B43/16 ,  C07C39/10 ,  C07C41/03 ,  C08G65/2612 ,  C08G65/3344 ,  C09K8/584 ,  C09K2208/30 ,  C07C43/23

    Abstract: A process for mineral oil production, in which an aqueous formulation comprising tris(2-hydroxyphenyl)methane of the general formula (I) is injected into a mineral oil deposit through an injection well and the crude oil is withdrawn from the deposit through a production well, where the R1, R2 and R radicals in the formula (I) are each defined as follows: R is independently 1 to 2 hydrocarbyl radicals per phenyl ring, R1 is preferably H or OH, R2 are independently radicals of the general formula (III), —(R5—O—)n—R6—X  (III) where n is a number from 1-50, and where the R5 radicals are R7 groups R6 is a single bond or an alkylene group having 1 to 10 carbon atoms, X is H or an acidic end group, R10 is, for example, C1-C6-hydrocarbyl radical, enables improved mineral oil production.

    Abstract translation: 一种矿物油生产方法，其中包含通式（I）的三（2-羟基苯基）甲烷的水性制剂通过注射井注入矿物油沉积物中，并且原油通过生产从沉积物中取出 其中式（I）中的R 1，R 2和R基团各自定义如下：R 1每个苯环独立地为1至2个烃基，R 1优选为H或OH，R 2独立地为通式（ III）， - （R 5 -O-）n -R 6 -X（III）其中n为1-50的数，其中R 5为R 7基团，R 6为单键或具有1〜10碳的亚烷基 原子，X是H或酸性端基，R10是例如C 1 -C 6 - 烃基，能够改善矿物油的生产。

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