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101.发明授权
公开(公告)号：US5015308A
公开(公告)日：1991-05-14
申请号：US378169
申请日：1989-07-11
申请人： Hiroshi Yamagata
发明人： Hiroshi Yamagata
CPC分类号： C23C14/14 , C22C45/08 , C23C14/0641 , Y10T428/12736
摘要： The present invention provides a corrosion-resistant and heat-resistant aluminum-based alloy thin film consisting of a composite having a composition represented by the general formula, Al.sub.a Ni.sub.b X.sub.c N.sub.d, wherein: X is a metal element selected from Y and Zr and a, b, c and d are as follows, in atomic percentages: 70.ltoreq.a.ltoreq.93, 0.5.ltoreq.b.ltoreq.7.5, 0.5.ltoreq.c.ltoreq.12 and 1.ltoreq.d.ltoreq.18, the composite being at least 50% (by volume) composed of an amorphous phase. The thin films are produced by depositing a material having the composition represented by the above-defined general formula onto a substrate by a thin film formation technique, such as sputtering, vacuum deposition or ion plating. In the production process, only nitrogen may be supplied as gas. The novel aluminum-based alloy thin film has superior corrosion-resistance and heat-resistance together with high levels of hardness and wear resistance. Further, the thin films can be subjected to a high degree of bending.
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公开(公告)号：US4950452A
公开(公告)日：1990-08-21
申请号：US324049
申请日：1989-03-16
CPC分类号： C22C45/08
摘要： The present invention provides high strength, heat resistant aluminum-based alloys having a composition represented by the general formula Al.sub.a M.sub.b Ce.sub.c, wherein M is at least one metal element selected from the group consisting of V, Cr, Mn, Fe, Co, Ni, Cu and Nb; and a, b and c are atomic percentages falling within the following ranges:50.ltoreq.a.ltoreq.93, 0.5.ltoreq.b.ltoreq.35 and 0.5.ltoreq.c.ltoreq.25,the aluminum alloy containing at least 50% by volume of amorphous phase. The aluminum-based alloys are especially useful as high strength, high heat resistant materials in various applications and since they exhibit superplasticity in the vicinity of their crystallization temperature, they can be easily processed into various bulk materials by extrusion, press woring or hot-forging at the temperatures within the range of the crystallization temperature .+-.100.degree. C.
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公开(公告)号：US4909867A
公开(公告)日：1990-03-20
申请号：US243501
申请日：1988-09-12
CPC分类号： C22C45/08
摘要： The present invention provides high-strength and heat resistant aluminum alloys having a composition represented by the general formula Al.sub.a M.sub.b La.sub.c (wherein M is at least one metal element selected from the group consisting of Fe, Co, Ni, Cu, Mn and Mo; and a, b and c are atomic percentages falling within the following ranges:65.ltoreq.a.ltoreq.93, 4.ltoreq.b.ltoreq.25 and 3.ltoreq.c.ltoreq.15),the aluminum alloys containing at least 50% by volume of amorphous phase. The aluminum alloys are especially useful as high strength and high heat resistant materials in various applications and, since the aluminum alloys specified above exhibit a superplasticity in the vicinity of their crystallization temperature, they can be readily worked into bulk forms by extrusion, press working or hot forging in the vicinity of the crystallization temperature.
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104.发明授权An apparatus for forming aluminum-transition metal alloys having high strength at elevated temperatures 失效一种用于在高温下形成具有高强度的铝 - 过渡金属合金的装置
公开(公告)号：US4805686A
公开(公告)日：1989-02-21
申请号：US52197
申请日：1987-05-15
申请人： David J. Skinner , Paul A. Chipko , Kenji Okazaki
发明人： David J. Skinner , Paul A. Chipko , Kenji Okazaki
摘要： The invention provides an aluminum based alloy consisting essentially of the formula Al.sub.bal Fe.sub.a X.sub.b, wherein X is at least one element selected from the group consisting of Zn, Co, Ni, Cr, Mo, V, Zr, Ti, Y and Ce, "a" ranges from about 7-15 wt. %, "b" ranges from about 2-10 wt. % and the balance is aluminum. The alloy has a predominately microeutectic microstructure, and is produced by a method and apparatus for forming rapidly solidified metal within an ambient atmosphere. Generally stated, the apparatus includes a moving casting surface which has a quenching region for solidifying molten metal thereon. A reservoir holds molten metal and has orifice means for depositing a stream of molten metal onto the casting surface quenching region. A heating mechanism heats the molten metal contained within the reservoir, and a gas source provides a non-reactive gas atmosphere at the quenching region to minimize oxidation of the deposited metal. A conditioning mechanism disrupts a moving gas boundary layer carried along by the moving casting surface to minimize disturbances of the molten metal stream that would inhibit quenching of the molten metal on the casting surface at a quench rate of at least about 10.sup.6 .degree. C./sec. Particles composed of the alloys of the invention can be heated in a vacuum and compacted to form a consolidated metal article have high strength and good ductility at both room temperature and at elevated temperatures of about 350.degree. C. The consolidated article is composed of an aluminum solid solution phase containing a substantially uniform distribution of dispersed intermetallic phase precipitates therein. These precipitates are fine intermetallics measuring less than about 100 nm in all dimenisons thereof.
摘要翻译： 本发明提供一种基本上由式AlbalFeaXb组成的铝基合金，其中X是选自Zn，Co，Ni，Cr，Mo，V，Zr，Ti，Y和Ce中的至少一种元素，“a” 范围为约7-15重量％ ％，“b”为约2-10wt。 ％，余额为铝。 该合金具有主要的微共晶组织，并且通过在环境气氛中形成快速固化的金属的方法和装置来制备。 一般说来，该装置包括一个移动的铸造表面，该铸造表面具有用于在其上固化熔融金属的淬火区域。 储存器保持熔融金属，并且具有用于将熔融金属流沉积到铸造表面淬火区域上的孔口装置。 加热机构加热储存器中所含的熔融金属，并且气体源在淬火区域提供非反应性气体气氛以使沉积的金属的氧化最小化。 调节机构破坏由移动的铸造表面携带的移动的气体边界层，以最小化熔融金属流的扰动，其将以至少约106℃/秒的骤冷速率抑制铸造表面上的熔融金属的淬火 。 由本发明的合金构成的颗粒可以在真空中加热并压实以形成在室温和在约350℃的高温下具有高强度和良好延展性的固结金属制品。固结制品由铝 固溶体相包含其中分散的金属间相沉淀物的基本均匀的分布。 这些沉淀物是在其所有二维中测量小于约100nm的细金属间化合物。
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公开(公告)号：US4787943A
公开(公告)日：1988-11-29
申请号：US45970
申请日：1987-04-30
CPC分类号： C22C1/0416 , B22F9/008 , C22C45/08
摘要： An aluminum alloy containing about 2 to 6 weight percent titanium, about 3 to 11 weight percent of a rare earth of the Lanthanide Series and up to about 3 weight percent of at least one Group VIII metal, balance aluminum, is disclosed. The alloy is preferably prepared by rapid solidification in powder, particulate or ribbon form, and is subsequently compacted under controlled conditions.
摘要翻译： 公开了含有约2至6重量％的钛，约3至11重量％的稀土镧系和至多约3重量％的至少一种第Ⅷ族金属余量的铝的铝合金。 合金优选通过粉末，颗粒或带形式的快速凝固制备，随后在受控条件下压实。
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106.发明授权Aluminum-transition metal alloys having high strength at elevated temperatures 失效在高温下具有高强度的铝 - 过渡金属合金
公开(公告)号：US4743317A
公开(公告)日：1988-05-10
申请号：US631261
申请日：1984-07-19
申请人： David J. Skinner , Paul A. Chipko , Kenji Okazaki
发明人： David J. Skinner , Paul A. Chipko , Kenji Okazaki
摘要： The invention provides an aluminum based alloy consisting essentially of the formula Al.sub.bal Fe.sub.a X.sub.b, wherein X is at least one element selected from the group consisting of Zn, Co, Ni, Cr, Mo, V, Zr, Ti, Y, Si and Ce, "a" ranges from about 7-15 wt %, "b" ranges from about 1.5-10 wt % and the balance is aluminum. The alloy has a predominately microeutectic microstructure.The invention also provides a method and apparatus for forming rapidly solidified metal, such as the metal alloys of the invention, within an ambient atmosphere. Generally stated, the apparatus includes a moving casting surface which has a quenching region for solidifying molten metal thereon. A reservoir holds molten metal and has orifice means for depositing a stream of molten metal onto the casting surface quenching region. A heating mechanism heats the molten metal contained within the reservoir, and a gas source provides a non-reactive gas atmosphere at the quenching region to minimize oxidation of the deposited metal. A conditioning mechanism disrupts a moving gas boundary layer carried along by the moving casting surface to minimize disturbances of the molten metal stream that would inhibit quenching of the molten metal on the casting surface at a quench rate of at least about 10.sup.6 .degree. C./sec.Particles composed of the alloys of the invention can be heated in a vacuum and compacted to form a consolidated metal article have high strength and good ductility at both room temperature and at elevated temperatures of about 350.degree. C. The consolidated article is composed of an aluminum solid solution phase containing a substantially uniform distribution of dispersed intermetallic phase precipitates therein. These precipitates are fine intermetallic measuring less than about 100 nm in all dimensions thereof.
摘要翻译： 本发明提供一种基本上由式AlbalFeaXb组成的铝基合金，其中X是选自Zn，Co，Ni，Cr，Mo，V，Zr，Ti，Y，Si和Ce中的至少一种元素， a“为约7-15重量％，”b“为约1.5-10重量％，余量为铝。 该合金具有主要的微共晶组织。 本发明还提供了一种用于在环境气氛中形成快速固化的金属（例如本发明的金属合金）的方法和装置。 一般说来，该装置包括一个移动的铸造表面，该铸造表面具有用于在其上固化熔融金属的淬火区域。 储存器保持熔融金属，并且具有用于将熔融金属流沉积到铸造表面淬火区域上的孔口装置。 加热机构加热储存器中所含的熔融金属，并且气体源在淬火区域提供非反应性气体气氛以使沉积的金属的氧化最小化。 调节机构破坏由移动的铸造表面携带的移动的气体边界层，以最小化熔融金属流的扰动，其将以至少约106℃/秒的骤冷速率抑制铸造表面上的熔融金属的淬火 。 由本发明的合金构成的颗粒可以在真空中加热并压实以形成在室温和在约350℃的高温下具有高强度和良好延展性的固结金属制品。固结制品由铝 固溶体相包含其中分散的金属间相沉淀物的基本均匀的分布。 这些沉淀物在其所有尺寸上均为小于约100nm的细金属间测量。
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107.发明授权Amorphous Al-based alloys essentially containing Ni and/or Fe and Si and process for the production thereof 失效基本上含有Ni和/或Fe和Si的无定形Al基合金及其生产方法
公开(公告)号：US4731133A
公开(公告)日：1988-03-15
申请号：US829061
申请日：1986-02-13
申请人： Salim Dermarkar
发明人： Salim Dermarkar
CPC分类号： C22C45/08
摘要： The invention is directed to microcrystalline Al-based alloys produced by annealing an alloy formed initially in a substantially amorphous state by rapid solidification (about 10.sup.4 K/sec) and having a composition consisting essentially of, in atomic %:from 5 to 30% Sifrom 11 to 22% Niwherein the Ni may be partially substituted by Fe up to 10%, by V or B up to 5 atomic % each, or totally substituted by Mn up to 22 atomic %, and wherein Fe+Ni+Si.ltoreq.42%. In the microcrystalline state, in the vicinity of the first crystallization peak, there is a metastable hexagonal phase whose crystalline parameters are about a=0.661 nm and c=0.378 nm.
摘要翻译： 本发明涉及通过快速凝固（约104K /秒）将初始形成为基本无定形状态的合金退火而制备的微晶Al基合金，其组成基本上由原子％：5至30％的Si 11％〜22％的Ni，其中Ni可以部分被Fe取代至多10％，V或B至多5原子％，或完全被Mn取代为22原子％以下，其中Fe + Ni + / = 42％。 在微晶状态下，在第一结晶峰附近存在晶体参数为a = 0.661nm，c = 0.378nm的亚稳态六方晶相。
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108.发明授权Process for preparing amorphous phases of intermetallic compounds by a chemical reaction 失效通过化学反应制备金属间化合物的无定形相的方法
公开(公告)号：US4639363A
公开(公告)日：1987-01-27
申请号：US711442
申请日：1985-03-12
申请人： Masao Komatsu , Hiroshi Fujita
发明人： Masao Komatsu , Hiroshi Fujita
CPC分类号： B22F9/004 , C22C16/00 , C22C45/10 , Y10S420/90
摘要： Amorphous phases are prepared by heat treatment of intermetallic compounds of Zr-Al alloys in hydrogen-containing gas.
摘要翻译： 通过在含氢气体中热处理Zr-Al合金的金属间化合物来制备无定形相。
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公开(公告)号：US4595429A
公开(公告)日：1986-06-17
申请号：US506993
申请日：1983-06-23
申请人： Gerard Le Caer , Jean-Marie Dubois
发明人： Gerard Le Caer , Jean-Marie Dubois
CPC分类号： C22C45/08
摘要： The present invention relates to substantially amorphous or microcrystalline aluminium-base alloys.Such alloys are of the following chemical composition:Al.sub.a M.sub.b M'.sub.c X.sub.d Y.sub.ein which:50.ltoreq.a.ltoreq.95 atom %M representing one or more metals of the group Mn, Ni, Cu, Zr, Ti, V, Cr, Fe and Co with:0.ltoreq.b.ltoreq.40 atom %M' representing Mo and/or W with:0.ltoreq.c.ltoreq.15 atom %X representing one or more elements of the group Ca, Li, Mg, Ge, Si and Zn, with:0.ltoreq.d.ltoreq.20 atom %Y representing the inevitable production impurities such as O, N, C, H, He, Ga, etc . . . , the proportion of which does not exceed 3 atom %.The alloys according to the invention can be produced by means of known methods in the form of wires, strips, bands, sheets or powders in the amorphous or microcrystallized state, the grain size of which is less than 1000 nm, preferably 100 nm. They may be used either directly or as means for reinforcing other materials, or as surface coatings which are resistant to corrosion or wear.
摘要翻译： 本发明涉及基本上无定形或微晶铝基合金。 这种合金具有以下化学组成：AlaMbM'cXdYe其中：代表Mn，Ni，Cu，Zr，Ti，V，Cr，Fe中的一种或多种金属的50％ 和Co：0表示Mo和/或W的原子％M表示Mo和/或W，其中：0表示Ca，Li，Mg组中的一种或多种元素 ，Ge，Si和Zn，其中：0≤d≤20原子％Y代表不可避免的生产杂质如O，N，C，H，He，Ga等。 。 。 ，其比例不超过3原子％。 根据本发明的合金可以通过已知方法以无定形或微晶态的线，条，带，片或粉末的形式制备，其晶粒尺寸小于1000nm，优选为100nm。 它们可以直接使用或作为增强其他材料的手段，或作为耐腐蚀或磨损的表面涂层使用。
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公开(公告)号：US11827959B2
公开(公告)日：2023-11-28
申请号：US18079934
申请日：2022-12-13
IPC分类号： C22C1/05 , C22C29/06 , C22C29/12 , C22C29/14 , C22C29/16 , C22C45/08 , C22C29/18 , C22C1/059
CPC分类号： C22C29/18 , C22C1/058 , C22C1/059 , C22C29/06 , C22C29/12 , C22C29/14 , C22C29/16 , C22C45/08
摘要： Metallic matrix composites are synthesized by mixing a first reactant, a second reactant and a nucleator compound to obtain a reaction mixture, and heating the reaction mixture to an auto-activation temperature to initiate a self-propagating high-temperature synthesis reaction between the first and second reactants. The metallic matrix composite can include a metallic matrix and an in situ formed reinforcement. The reinforcement can be formed of discrete particles substantially uniformly dispersed within the metallic matrix. Each of the particles can have a reinforcement constituent disposed about a core formed of the nucleator compound.
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