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20 条记录 (耗时 0.017 秒)

    Thermoplastic thermosettable polyamide from poly(oxytetramethylene) diamine and poly(oxytetramethylene) oligomer polyamine
    12.
    发明授权
    Thermoplastic thermosettable polyamide from poly(oxytetramethylene) diamine and poly(oxytetramethylene) oligomer polyamine 失效
    来自聚（氧四亚甲基）二胺和聚（氧四亚甲基）低聚物多胺的热塑性热固性聚酰胺

    公开(公告)号：US5140097A

    公开(公告)日：1992-08-18

    申请号：US608128

    申请日：1990-11-01

    申请人： George P. Speranza ,  Wei-Yang Su ,  Robert L. Zimmerman ,  Donald H. Champion

    发明人： George P. Speranza ,  Wei-Yang Su ,  Robert L. Zimmerman ,  Donald H. Champion

    IPC分类号： C08G69/40

    CPC分类号： C08G69/40

    摘要： Polyamide reaction products comprising: a dicarboxylic acid and a diamine component comprising a mixture of poly(oxytetramethylene) diamines and oligomers of said poly(oxytetramethylene) diamines,said mixture containing from about 85 to about 99.5 wt. % of said poly(oxytetramethylene) diamines and, correspondingly, from about 15 to about 0.5 wt. % of said oligomers,said poly(oxytetramethylene) diamines having the formula: ##STR1## wherein n represents 0 or a positive number having a value of 1 to about 30,said oligomers having the formula: ##STR2## wherein n represents 0 or a positive number having a value of 1 to about 30.

    摘要翻译： 聚酰胺反应产物包括：二羧酸和二胺组分，其包含聚（氧四亚甲基）二胺和所述聚（氧四亚甲基）二胺的低聚物的混合物，所述混合物含有约85-约99.5wt。 ％的所述聚（氧四亚甲基）二胺，相应地为约15至约0.5wt。 所述低聚物的所述聚（氧四亚甲基）二胺具有下式：其中n表示0或具有1至约30的值的正数，所述具有下式的低聚物：（II） 其中n表示0或具有1至约30的值的正数。

    Method for the production of N-methylpyrrolidine
    13.
    发明授权
    Method for the production of N-methylpyrrolidine 失效
    制备N-甲基吡咯烷的方法

    公开(公告)号：US4892959A

    公开(公告)日：1990-01-09

    申请号：US184660

    申请日：1988-04-22

    申请人： Donald H. Champion ,  John F. Knifton ,  Wei-Yang Su

    发明人： Donald H. Champion ,  John F. Knifton ,  Wei-Yang Su

    IPC分类号： C07D295/023

    CPC分类号： C07D295/023

    摘要： A method is disclosed for the improved production of N-methylpyrrolidine at moderate conditions which comprises the steps of reacting N-methylpyrrolidone with hydrogen over a copper chromite catalyst at a moderate temperature and a pressure of 1000 psig to 5000 psig and thereafter isolating the N-methylpyrrolidine by extraction with an aliphatic hydrocarbon solvent having a boiling point less than 70.degree. C. or greater than 90.degree. C.

    摘要翻译： 公开了一种在中等条件下改进生产N-甲基吡咯烷的方法，其包括在中等温度和1000psig至5000psig的压力下，使亚硝酸铬催化剂上的N-甲基吡咯烷酮与氢反应的步骤，然后分离N- 通过用沸点小于70℃或大于90℃的脂族烃溶剂萃取，得到甲基吡咯烷酮。

    Macrocyclic oxamides
    14.
    发明授权
    Macrocyclic oxamides 失效
    大环酰胺

    公开(公告)号：US5298618A

    公开(公告)日：1994-03-29

    申请号：US979737

    申请日：1992-11-23

    申请人： George P. Speranza ,  Donald H. Champion ,  Martin J. Plishka

    发明人： George P. Speranza ,  Donald H. Champion ,  Martin J. Plishka

    IPC分类号： C07D245/02 ,  C07D255/02 ,  C07D257/02 ,  C07D259/00 ,  C07D273/00 ,  C07D273/08 ,  C07D487/18 ,  C22B3/36

    CPC分类号： C22B3/0036 ,  C07D245/02 ,  C07D255/02 ,  C07D257/02 ,  C07D259/00 ,  C07D273/00 ,  Y02P10/234

    摘要： Macrocyclic oxamides may be made easily, in good yield and in one step by reacting an oxalic compound, such as oxalic acid or oxalic esters, with a diamine, where the amine groups are separated by at least five atoms. The oxalic compounds may include, but are not limited to such materials as dimethyl oxalate and diethyl oxalate. The diamines may include, but are not limited to such materials as alkylenediamines; polyalkylene glycol diamines; alkyl-bis-(aminoalkyl)amines; imino bis-(alkyl)amines; and N,N' bis-(aminoalkyl)-N,N'-dialkylalkylenediamines and bis-(aminoalkyl)piperazines; and mixtures thereof. The macrocyclic oxamides made by this process may be used to selectively separate metal ions from solution, or complexed together with a metal ion act as a catalyst.

    摘要翻译： 大环氧酰胺可以容易地制备，以良好的产率和一步法，草酸化合物如草酸或草酸酯与二胺反应，其中胺基被至少五个原子分开。 草酸化合物可以包括但不限于草酸二甲酯和草酸二乙酯等材料。 二胺可以包括但不限于如亚烷基二胺等材料; 聚亚烷基二醇二胺; 烷基 - 双 - （氨基烷基）胺; 亚氨基双（烷基）胺; 和N，N'-双 - （氨基烷基）-N，N'-二烷基亚烷基二胺和双 - （氨烷基）哌嗪; 及其混合物。 通过该方法制备的大环氧酰胺可以用于选择性地从溶液中分离金属离子，或者与金属离子络合在一起作为催化剂。

    Process for the production of cyclohexane by liquid phase hydrogenation of benzene
    15.
    发明授权
    Process for the production of cyclohexane by liquid phase hydrogenation of benzene 失效
    通过苯的液相氢化生产环己烷的方法

    公开(公告)号：US5189233A

    公开(公告)日：1993-02-23

    申请号：US749346

    申请日：1991-08-23

    申请人： John M. Larkin ,  James H. Templeton ,  Donald H. Champion

    发明人： John M. Larkin ,  James H. Templeton ,  Donald H. Champion

    IPC分类号： C07C5/10

    CPC分类号： C07C5/10 ,  C07C2101/14 ,  C07C2521/04 ,  C07C2523/72 ,  C07C2523/755 ,  C07C2523/86

    摘要： Disclosed is an improvement in a process for production of cyclohexane by liquid phase hydrogenation of benzene wherein no diluent is necessary, which comprises contacting benzene and hydrogen in the presence of a mixed catalyst bed comprising a first catalyst which is a less active hydrogenation catalyst selected from elements of Group VIII of the Periodic Table and a second, more active catalyst, comprising a Group VIII metal supported on an oxide, such as, for example, alumina, silica or titania at a temperature of about 40.degree. C. to about 300.degree. C. and pressure sufficient to keep the benzene liquid at the chosen reaction temperature.

    摘要翻译： 公开了通过苯的液相氢化制备环己烷的方法的改进，其中不需要稀释剂，其包括在混合催化剂床的存在下使苯和氢接触，所述混合催化剂床包含第一催化剂，所述第一催化剂是选自 元素周期表第VIII族和第二种更有活性的催化剂，其包含负载在氧化物上的第VIII族金属，例如氧化铝，二氧化硅或二氧化钛，温度为约40℃至约300℃ C.和足以将苯液体保持在所选择的反应温度的压力。

    Two-step method for preparing cyclic ureas
    16.
    发明授权
    Two-step method for preparing cyclic ureas 失效
    制备环脲的两步法

    公开(公告)号：US5206362A

    公开(公告)日：1993-04-27

    申请号：US837131

    申请日：1992-02-19

    申请人： George P. Speranza ,  Donald H. Champion

    发明人： George P. Speranza ,  Donald H. Champion

    IPC分类号： C07D245/02 ,  C07D257/02 ,  C07D259/00 ,  C07D273/00 ,  C07D273/08

    CPC分类号： C07D273/00 ,  C07D245/02

    摘要： Disclosed is a two-step method for the preparation of cyclic urea products which comprises: heating a diamine with urea in a mole ratio of about 1 at a temperature from about 120.degree. C. to 140.degree. C. until a mole of ammonia is liberated and slowly heating the intermediate with an alcohol or polyether solvent to a temperature from about 160.degree. C. to 200.degree. C. to produce the cyclic urea products.

    摘要翻译： 公开了用于制备环状脲产物的两步法，该方法包括：在约120℃至140℃的温度下，以约1摩尔比的尿素加热二胺，直到释放出一摩尔氨 并用醇或聚醚溶剂将中间体缓慢加热至约160℃至200℃的温度以产生环状尿素产物。

    Cyanoethylation of alcohols
    17.
    发明授权
    Cyanoethylation of alcohols 失效
    醇的氰基乙基化

    公开(公告)号：US5159101A

    公开(公告)日：1992-10-27

    申请号：US833199

    申请日：1992-02-10

    申请人： Donald H. Champion ,  George P. Speranza

    发明人： Donald H. Champion ,  George P. Speranza

    IPC分类号： C07C255/13

    CPC分类号： C07C255/13

    摘要： Disclosed is a process wherein cyanoethylation is accomplished by reacting a compound of the formula: ##STR1## where R=H or CH.sub.3, n=1 to 3 and m=0 to 50, and acrylonitrile over a heterogeneous catalyst comprising, potassium fluoride or cesium fluoride supported on an oxide of an element from the group consisting of Group IA, IIA or IIIA of the Periodic Table.

    摘要翻译： 公开了一种方法，其中氰基乙基化是通过使下式化合物（其中R = H或CH 3，n = 1-3和m = 0至50）与丙烯腈反应，在包含氟化钾或铯 氟化物负载在元素的氧化物上，该元素来自元素周期表的IA，IIA或IIIA族元素。

    Amidoamines derived from amines with aminopropyl and secondary amine termini
    19.
    发明授权
    Amidoamines derived from amines with aminopropyl and secondary amine termini 失效
    衍生自胺与氨基丙基和仲胺末端的酰氨基胺

    公开(公告)号：US5103056A

    公开(公告)日：1992-04-07

    申请号：US648771

    申请日：1991-01-31

    申请人： George P. Speranza ,  Donald H. Champion

    发明人： George P. Speranza ,  Donald H. Champion

    IPC分类号： C07C231/02

    CPC分类号： C07C231/02

    摘要： Disclosed is a method for selective formation of amidoamines which comprises reacting a carboxylic acid group, such as, for example, a diacid or an aliphatic acid terminated amide with an aminopropylated disecondary amine which contains a secondary amine terminus in the same molecule at a temperature of about 150.degree. C. to about 260.degree.0 C.

    摘要翻译： 公开了一种选择性形成酰氨基胺的方法，其包括使羧酸基团，例如二酸或脂族酸封端的酰胺与在相同分子中含有仲胺末端的氨基丙基化的二仲胺在温度为 约150℃至约260℃。