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公开(公告)号：US5495058A
公开(公告)日：1996-02-27
申请号：US248758
申请日：1994-05-25
IPC分类号： C07C17/10
CPC分类号： C07C17/10
摘要： A process for the chlorination of a paraffin wax is described which includes the steps of contacting the paraffin wax or partially chlorinated paraffin wax with chlorine wherein the improvement is the use of a non-ozone depleting aromatic solvent with a boiling point less than 180.degree. C., preferably less than 160.degree. C. and which is non-reactive to chlorine in a free radical chlorination environment, in contrast to typical C.sub.1 -C.sub.2 aliphatic solvents.
摘要翻译： 描述了一种用于石蜡氯化的方法，其包括使石蜡或部分氯化石蜡与氯接触的步骤，其中改进是使用沸点低于180℃的非臭氧消耗性芳族溶剂 优选小于160℃，与自由基氯化环境中的氯不反应，与典型的C1-C2脂族溶剂相反。
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公开(公告)号：US06362260B1
公开(公告)日：2002-03-26
申请号：US09471067
申请日：1999-12-22
申请人： Donald R. Stevenson , Duong Nguyen
发明人： Donald R. Stevenson , Duong Nguyen
IPC分类号： C08K549
CPC分类号： C07F9/145 , C07F9/1412 , C08K5/524 , C08L27/06
摘要： Liquid organic phosphites of low volatility, based on pentaerythritol, alkyl alcohols and alkyl phenols, which are essentially phenol-free are disclosed. These phosphites are excellent stabilizers for polymers, especially PVC resins. The phenol-free phosphite stabilizers are compatible with mixed metal stabilizers and give excellent color and processing stability.
摘要翻译： 公开了基本上不含酚的基于季戊四醇，烷基醇和烷基酚的低挥发性的液体有机亚磷酸酯。 这些亚磷酸酯是聚合物，特别是PVC树脂的优异的稳定剂。 无酚亚磷酸酯稳定剂与混合金属稳定剂相容，并具有优异的颜色和加工稳定性。
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13.发明授权Coating process with compositions of active hydrogen compound, unsaturated or epoxy compound, and carbamothioate curing agent 失效具有活性氢化合物，不饱和或环氧化合物和氨基甲酸酯固化剂的组合物的涂覆方法
公开(公告)号：US4133916A
公开(公告)日：1979-01-09
申请号：US812801
申请日：1977-07-05
CPC分类号： C08G18/8006 , C08G18/02 , C08G18/8054 , C08G18/8083 , C08G59/4057 , C09D5/4473 , C08G2150/20
摘要： Process for coating a substrate with a heat-curable coating composition comprising a compound having labile hydrogenation groups, a compound having unsaturated carbon-carbon or epoxy groups, and a carbamothioate curing agent. Heat-curing of the coated substrate above the critical temperature initiates formation of mercaptan and isocyanate curing units from the carbamothioate curing agent which curing units react with said compounds to cure the coating. In preferred embodiments the coating composition is dispersed in water, a fugative organic solvent, or is a powder coating.
摘要翻译： 用含有不稳定氢化基团的化合物，具有不饱和碳 - 碳或环氧基的化合物和氨基硫代硫酸酯固化剂的可热固化涂料组合物涂覆基材的方法。 高于临界温度的涂覆基材的热固化引发硫代硫酸酯固化剂形成硫醇和异氰酸酯固化单元，固化单元与所述化合物反应以固化涂层。 在优选的实施方案中，涂料组合物分散在水，逸出的有机溶剂中，或者是粉末涂料。
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公开(公告)号：US4064194A
公开(公告)日：1977-12-20
申请号：US691134
申请日：1976-05-28
CPC分类号： C08G18/6795 , C08G18/68
摘要： A two-package urethane forming coating composition comprises a hydroxyl-bearing polymer having ethylenic unsaturation dispersed in fugitive solvent; and a multi-isocyanate dispersed in fugitive solvent. The coating composition cures by heating with an in situ reaction of the hydroxyl-isocyanate reaction in combination with an in situ free-radical addition polymerization through the ethylenic unsaturation.
摘要翻译： 双包装氨基甲酸酯形成涂料组合物包含分散在挥发性溶剂中的具有烯属不饱和度的含羟基聚合物; 和分散在挥发性溶剂中的多异氰酸酯。 涂料组合物通过羟基 - 异氰酸酯反应的原位反应与通过烯属不饱和键的原位自由基加成聚合的组合加热固化。
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公开(公告)号：US5364895A
公开(公告)日：1994-11-15
申请号：US108658
申请日：1993-08-30
IPC分类号： C07F9/6574 , C08K5/527 , C07F9/6578
CPC分类号： C07F9/65746 , C08K5/527
摘要： A class of hydrolytically stable bis(aralkylphenyl)pentaerythritol diphosphites is disclosed, which is suitable as an antioxidant additives in polyolefins, particularly, in polypropylene. The diphosphites are of low volatility, have a high thermal decomposition temperature and resist yellowing when blended into a polyolefin base. A preferred diphosphite is bis(2,4-dicumylphenyl)pentaerythritol diphosphite.
摘要翻译： PCT No.PCT / US93 / 00499 Sec。 371日期：1993年8月30日 102（e）1993年8月30日PCT 1993年1月20日PCT PCT。 第WO94 / 17082号公报 日本1994年8月4日。公开了一类水解稳定的双（芳烷基苯基）季戊四醇二亚磷酸酯，其适合作为聚烯烃中的抗氧化添加剂，特别是在聚丙烯中。 二亚磷酸酯具有低挥发性，具有高的热分解温度，并且当掺入聚烯烃基质时可以防止变黄。 优选的二亚磷酸酯是双（2,4-二枯基苯基）季戊四醇二亚磷酸酯。
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公开(公告)号：US07595412B2
公开(公告)日：2009-09-29
申请号：US10486769
申请日：2002-08-05
IPC分类号： C07C59/147 , C07C59/185
CPC分类号： C10M159/20 , C07C51/414 , C07C53/126 , C07C57/03 , C07C57/12 , C08K5/0091 , C10M2207/26 , C10N2210/02 , C10N2230/06 , C08L27/06
摘要： A novel composition and methods of its use and preparation of polybasic metal carboxylate complexes having the general formula: (A)2M.nD(OH)2.xH2O.m(B)2N wherein: A is an organic fatty acid and is selected from the group consisting of saturated C12-24 carboxylic acids, unsaturated C12-24 carboxylic acids, aromatic C12-24 carboxylic acids, alicyclic C12-24 carboxylic acids, polycarboxylic acid derivatives thereof, anhydride derivatives thereof and blends thereof, preferably stearate; M is a divalent metal cation, preferably calcium; n is a fractional or whole number from about 1 to about 10 inclusive; D is an alkali earth metal, preferably calcium; x is a fractional or whole number from about 0 to about 3 inclusive; N is a divalent metal cation other than calcium, preferably zinc; and m is a fractional or whole number from 0 to about 1.
摘要翻译： 一种新型组合物及其制备具有以下通式的多元金属羧酸盐络合物的新型组合物及其制备方法：<？in-line-formula description =“In-line Formulas”end =“lead”→（A）2M.nD（OH ）2.xH2O.m（B）2N <βin-line-formula description =“In-line Formulas”end =“tail”？>其中：A为有机脂肪酸，选自饱和C12 -24羧酸，不饱和C 12-24羧酸，芳族C 12-24羧酸，脂环族C 12-24羧酸，其多元羧酸衍生物，其酸酐衍生物及其共混物，优选硬脂酸酯; M是二价金属阳离子，优选钙; n为约1至约10的分数或整数; D是碱土金属，优选钙; x是从约0到约3的分数或整数; N是除钙以外的二价金属阳离子，优选锌; m为0〜1左右的分数或整数。
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公开(公告)号：US07470735B2
公开(公告)日：2008-12-30
申请号：US10709578
申请日：2004-05-14
IPC分类号： C08K5/524
CPC分类号： C07F9/145 , C07F9/1411 , C08K5/526 , C08L27/06
摘要： Various phenol-free phosphites for use in PVC as an alternative to the conventional phenol-containing products phenyl diisodecyl phosphite and diphenyl isodecyl phosphite were tested. These phosphites utilize para-cumyl phenol-based derivatives in order to provide a phenol free derivative of the above mentioned conventional phosphites.
摘要翻译： 测试了用于PVC中的各种无酚亚磷酸酯作为常规含苯酚产物苯基二异癸基亚磷酸酯和亚磷酸二苯基酯的替代物。 这些亚磷酸酯使用对枯基苯酚基衍生物以提供上述常规亚磷酸酯的无酚衍生物。
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公开(公告)号：US07176252B2
公开(公告)日：2007-02-13
申请号：US10778492
申请日：2004-02-13
CPC分类号： C09K15/322 , C07F9/65746 , C08K5/0008 , C08K5/526
摘要： A solid phosphite composite, having at least a portion in amorphous form, which includes at least one, preferably two or more phosphite antioxidants or alternatively at least one phosphite and at least one other polymer additive. The phosphites, at least one of which can initially be a liquid, are generally uniformly distributed since they are melt blended. A desired class of phosphites are the bis(arylalkylphenyl)pentaerythritol diphosphites, at least a portion of which is in amorphous form.
摘要翻译： 一种具有至少一部分无定形形式的固体亚磷酸酯复合物，其包括至少一种，优选两种或更多种亚磷酸酯抗氧化剂或者至少一种亚磷酸酯和至少一种其它聚合物添加剂。 亚磷酸酯中的至少一种最初可以是液体，由于它们是熔融共混的，所以它们通常是均匀分布的。 所需的亚磷酸酯类是双（芳基烷基苯基）季戊四醇二亚磷酸酯，其至少一部分为无定形形式。
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公开(公告)号：US5780400A
公开(公告)日：1998-07-14
申请号：US897382
申请日：1997-07-21
IPC分类号： C10M105/38 , C10M129/74 , C10M173/00 , C10M173/02 , C10N30/06 , C10N40/20 , C10M129/72
CPC分类号： C10M129/74 , C10M173/00 , C10M173/02 , C10M2201/02 , C10M2207/283 , C10N2240/40 , C10N2250/02
摘要： The invention pertains to chlorine-free extreme pressure metalworking fluid additives and lies in the recognition of the improved hydrolytic stability of alkanoic acid esters of cyclohexane dimethanol and other esters embodying similar structures. The various derivatives which are effective as extreme pressure additives include those which fall within the generic description ##STR1## wherein R.sup.1 through R.sup.4 are independently selected from the group hydrogen and C.sub.1-24 hydrocarbyl groups and R.sup.5 and R.sup.6 are independently selected from the group C.sub.3-24 hydrocarbyl groups.
摘要翻译： 本发明涉及无氯极压金属加工液添加剂，并且在于认识到环己烷二甲醇的链烷酸酯和体现相似结构的其它酯的改进的水解稳定性。 作为极压添加剂有效的各种衍生物包括落入通用描述
中的那些，其中R 1至R 4独立地选自氢和C 1-4烃基，R 5和R 6独立地选自C 3- 24个烃基。 -
公开(公告)号：US5532401A
公开(公告)日：1996-07-02
申请号：US375557
申请日：1995-01-19
CPC分类号： C07F9/145
摘要： An improved process for the preparation of tris(nonylphenyl) phosphite is described which includes the steps of combining at least a 4 weight percent excess of nonylphenol (preferably 8 weight percent excess) with PCl.sub.3 with agitation and heating sufficient to liberate HCl formed during the synthetic reaction as a by-product and removing the excess nonylphenol from the tris(nonylphenyl) phosphite by thin film distillation to reduce the residual chloride level to 90 ppm or less, an acid number of 0.1 or less and a nonylphenol content after stripping of 0.1 weight percent or less. The temperature of the reaction was from room temperature to 130.degree. C., and the temperature of the evaporator which removes the excess nonylphenol is from 100.degree. C. to 350.degree. C., preferably from 150.degree. C. to 250.degree. C., under a system vacuum of from 0.01 mm Hg to 5 mm Hg.
摘要翻译： 描述了制备三（壬基苯基）亚磷酸酯的改进方法，其包括将搅拌和加热至少4重量％过量的壬基酚（优选8重量％过量）与PCl 3组合的步骤，足以释放在合成过程中形成的HCl 作为副产物的反应，并通过薄膜蒸馏从三（壬基苯基）亚磷酸酯除去多余的壬基酚，将残留的氯化物水平降低至90ppm以下，酸值为0.1以下，脱模后的壬基酚含量为0.1重量 百分之以内。 反应温度为室温至130℃，除去过量壬基酚的蒸发器的温度为100℃至350℃，优选150℃至250℃， 在0.01mm Hg至5mm Hg的系统真空下。
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