摘要:
A weighing system of the electromagnetic load compensation type is disclosed including a counter for counting the weight-responsive pulses which are produced during the periods that the compensating current is supplied to the movable coil to return the movable scale member toward its initial no-load position, characterized by the provision of a temperature-responsive device for supplying to the counter a train of temperature-correction pulses that are used to modify the count of the weight-responsive pulses, whereby a more accurate indication of the applied load is obtained. Thus, an analog signal from the temperature sensor is compared with a sawtooth signal to produce a digitalized temperature-responsive signal which modifies the digital weight signal supplied to the microprocessor circuit.
摘要:
An NMR (nuclear magnetic resonance) apparatus has a magnet system disposed in a cryostat (1), the cryostat having at least one nitrogen tank (3b) for receiving liquid nitrogen (5b) and a room temperature bore (7) for receiving an NMR probehead (8), wherein part(s) of the probehead or the overall probehead can be cooled to cryogenic temperatures by supplying liquid nitrogen (5b) via a supply line (14). The nitrogen tank (3b) of the cryostat (1) is connected to the NMR probehead (8) by means of a supply line (14) in such a fashion that liquid nitrogen (5b) is removed from the nitrogen tank (3b) and guided to the NMR probehead (8). The overall apparatus is therefore more compact, the operating comfort of the apparatus is increased, and the costs for acquisition, operation and maintenance are considerably reduced compared to previous comparable devices.
摘要:
A sample tube for an NMR probe head, which extends along a z axis and has an internal cavity that extends in an axial direction of the z axis, is open to the outside at the axially upper end, is closed at the axially lower end and contains a liquid NMR sample substance during operation, wherein the cross-sectional surface of this cavity extending perpendicularly to the z axis and parallel to the xy coordinate plane has an elongated shape in the direction of the x axis with maximum dimensions a in the y direction and b in the x direction, wherein a
摘要:
An NMR spectrometer comprising an NMR magnet system (27) disposed in a helium tank of a cryostat and an NMR probe head (11) disposed in a room temperature bore of the cryostat, which contains a cooled RF resonator (9) for receiving NMR signals from a sample to be investigated, and a cooled pre-amplifier (10), wherein the NMR probe head (11) is cooled by a common multi-stage compressor-operated refrigerator (2), wherein the refrigerator (2) comprises a cold head and several heat exchangers (5, 6) at different temperature levels, wherein the refrigerator (2) is disposed at a spatial separation from the cryostat in a separate, evacuated and thermally insulated housing (1) and wherein at least one cooling circuit with cooling lines, which are thermally insulated by a transfer line (13, 14) is disposed between the housing (1) containing the heat exchangers (5, 6) and the NMR probe head (11), is characterized in that additional cooling lines to an LN2 tank (18) or radiation shield (21) disposed in the cryostat and surrounding the helium tank are provided, and the refrigerator (2) also cools the LN2 tank (18) or the radiation shield (21). The inventive NMR spectrometer comprises a simple and inexpensive device for matching the holding time of LN2 to that of LHe through cooling the LN2 tank using the refrigerator provided for cooling the NMR probe head and without great expense.
摘要:
A transport device for conveying an object to be transported (18) between an input point (A) and a supply point (Z), where the object to be transported (18) can be supplied to an RT tube (4) of a cryostat (1), wherein the input point (A) is both horizontally and also vertically spaced apart from the supply point (Z), wherein a transport tube (14) is provided for pneumatically conveying the object to be transported within the transport tube (14) from a first transfer point (B) to a second transfer point (C), is characterized in that the transport tube (14) is vertically arranged, a first transport container (TB1) and a second transport container (TB2) are provided for receiving the object to be transported (18), a first transfer device is disposed between the input point (A) and the first transfer point (B), and a second transfer device is provided between the second transfer point (C) and the supply point (Z).
摘要:
A tubular capacitor with variable capacitance, including a cylindrical tube (3) of dielectric material, a metallic outer electrode (1) which surrounds the cylindrical tube (3), and an inner electrode which can axially move in the inner bore (41) of the cylindrical tube (3) and which abuts the inner bore (41), wherein the inner electrode includes a metallic rod (2; 2a; 2b; 2c), is characterized in that the metallic rod (2; 2a; 2b; 2c) is axially extended at its end (5′), located in the inner bore (41) of the cylindrical tube (3), using a rod (9; 9a; 9b; 9c) of dielectric material. The inventive tubular capacitor has an increased dielectric strength and improves the resolution of NMR spectrometers.
摘要:
A tubular capacitor with variable capacitance, comprising a cylindrical tube (3) of dielectric material, a metallic outer electrode (1) which surrounds the cylindrical tube (3), and an inner electrode which can axially move in the inner bore (41) of the cylindrical tube (3) and which abuts the inner bore (41), wherein the inner electrode comprises a metallic rod (2; 2a; 2b; 2c), is characterized in that the metallic rod (2; 2a; 2b; 2c) is axially extended at its end (5′), located in the inner bore (41) of the cylindrical tube (3), using a rod (9; 9a; 9b; 9c) of dielectric material. The inventive tubular capacitor has an increased dielectric strength and improves the resolution of NMR spectrometers.
摘要:
An RF receiver coil configuration for NMR spectrometers has at least two largely mutually orthogonal RF receiver coil systems of which at least one is made from superconducting material and is at least partially cooled to a cryogenic temperature lying far below room temperature, with each RF receiver coil system comprising at least one single coil arranged symmetrically about a sample the RF receiver coil systems having differing radial separations from the sample. The inner RF receiver coil system is made from a material having differing physical characteristics in dependence on the actual operating temperature than the material of the outer RF receiver coil system, with the materials and the geometries of the RF receiver coil systems being chosen to minimize the influence of the susceptibility of the RF receiver coil system on the homogeneity of the magnetic field in the vicinity of the sample. In this fashion, the high Q values of the resonator configuration achieved by the use of superconducting material with high electrical RF conductivity can be taken advantage of while, at the same time, avoiding the substantial interfering influences of the high susceptibility of the superconducting material.
摘要:
In a method for compensation of time variant field disturbances in magnetic fields of electromagnets with high field-homogeneity, in particular in sample volumes of superconducting electromagnets for measurements of magnetic resonance, the dispersion signal u.sub.x of the nuclear signal of a reference substance is acquired and taken into consideration for compensation by generation of a current dependent on the dispersion signal in a field correction coil of the electromagnet. The method is characterized in that the absorption signal u.sub.y of the reference substance is additionally acquired and that the compensation is carried out in dependence on the quantity u.sub.x /u.sub.y and/or (1/u.sub.y)(du.sub.x /dt). These are substantially independent of many influencing quantities.