Methods and apparatus for isolating dicarboxylic acid
    13.
    发明授权
    Methods and apparatus for isolating dicarboxylic acid 有权
    用于分离二羧酸的方法和装置

    公开(公告)号:US09388111B2

    公开(公告)日:2016-07-12

    申请号:US14141639

    申请日:2013-12-27

    CPC classification number: C07C51/47 C07C51/43 C07C63/24 C07C63/26

    Abstract: Disclosed is a method for purifying aromatic dicarboxylic acid such as isophthalic acid or terephthalic acid. The process treats a crude carboxylic acid (CCA) composition by feeding a CCA composition comprising a liquid and a solid to a filter cake formation zone to form a CCA wet cake composition and a first mother liquor stream; dewatering said CCA wet cake composition to form a dewatered CCA wet cake composition having a second liquid level that is lower than the first liquid level or having no liquid level and a second mother liquor stream; and washing the dewatered CCA wet cake composition with a wash stream in a wash zone to forma washed CCA wet cake composition and a wash liquor stream.

    Abstract translation: 公开了一种净化芳族二羧酸如间苯二甲酸或对苯二甲酸的方法。 该方法通过将包含液体和固体的CCA组合物进料到滤饼形成区域来处理粗羧酸(CCA)组合物以形成CCA湿滤饼组合物和第一母液流; 脱水所述CCA湿饼组合物以形成具有低于所述第一液面或不具有液面水平的第二液位的脱水CCA湿滤饼组合物和第二母液流; 并在洗涤区中用洗涤流洗涤脱水的CCA湿饼组合物,以形成洗涤的CCA湿饼组合物和洗涤液流。

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