Abstract:
A crucible handling shuttle includes a pair of opposed dual crucible-gripping arms mounted on a rotatable head and moves between an induction furnace pedestal and a crucible loading station, such that one pair of arms pick up a crucible loaded with a preweighed sample, the shuttle moves to the induction furnace, where the other pair of arms grip and remove a spent crucible. The shutter head then rotates to deposit the new sample-holding crucible onto the pedestal and subsequently moves out of the furnace area to a sample disposal chute positioned between the crucible loading station and the furnace, whereupon the spent crucible is dropped for disposal. The shuttle head is then rotated and moved to the loading station to pick up a new crucible.
Abstract:
An electrode for a resistance analytical furnace has a crucible-engaging surface and an end spaced from the crucible-engaging surface having a plurality of grooves formed therein. A manifold mounted on the end of the electrode defines a dust recovery plenum and includes an outlet communicating with the plenum for coupling to a vacuum source to remove debris from the electrode. The improved electrode and electrode cleaning manifold positioned on the electrode provides a turbulent airflow for removal of dust and debris from an analytical furnace.
Abstract:
A crucible handling shuttle includes a pair of opposed dual crucible-gripping arms mounted on a rotatable head and moves between an induction furnace pedestal and a crucible loading station, such that one pair of arms pick up a crucible loaded with a preweighed sample, the shuttle moves to the induction furnace, where the other pair of arms grip and remove a spent crucible. The shutter head then rotates to deposit the new sample-holding crucible onto the pedestal and subsequently moves out of the furnace area to a sample disposal chute positioned between the crucible loading station and the furnace, whereupon the spent crucible is dropped for disposal. The shuttle head is then rotated and moved to the loading station to pick up a new crucible.
Abstract:
A sample introduction system includes a drop chamber which can be sealed and outgassed and which includes a movable jaw selectively holding the sample in position above a conduit communicating with an open crucible for receiving a sample once the jaw has been moved to an open position releasing the sample. The jaw is actuated by a magnetic field which moves the jaw in an entirely enclosed system, thereby preventing the introduction of atmospheric contaminants during the operation of the sample dropping jaw from a closed, sample holding position to an open sample releasing position. By providing a magnetic actuator, such as a solenoid, for operation of the jaw, the sample chamber remains sealed during the sample dropping operation preventing contaminants from interfering with the analytical results.
Abstract:
A sample mounting system includes a coupon holder having a plurality of apertures defining in part mold cavities for supporting a plurality of printed circuit board coupons on the holder. A removable mold is also provided and engages the coupon holder to define mold cavities into which molding resin is poured. The mold is then removed from the coupon holder which is secured in an annular stop ring and mounted to a polishing machine for polishing coupons molded in place with respect to the holder.
Abstract:
A combustion tube mounting system releasably mounts a combustion tube to an aperture in the floor of a furnace housing. The combustion tube has a base assembly with a cam and can be manually or automatically unlocked by cam pins in the floor for selectively engaging the cam for lowering the combustion tube from the floor of the furnace. When a new combustion tube is placed on the lower seal assembly and raised, it automatically aligns and engages the upper furnace seal and engages cams on the floor of the furnace housing which lock the combustion tube in place as it is introduced into the furnace.
Abstract:
A combustion tube comprises a generally cylindrical body with an outwardly extending annular tube stop spaced from one end of the combustion tube for engaging a combustion tube mounting assembly and fixing the tube in a precise position. Near the opposite end of the tube is an enlarged opening for receiving an upper seal assembly of a combustion furnace with the outer annular shoulder of the upper end of the tube having a rolled edge to facilitate the insertion of the tube through the seal in the upper seal assembly of the furnace. The combustion tube is made of quartz glass to withstand the temperatures encountered in the furnace. The combustion tube is specifically designed and adapted to be precisely positioned in an induction furnace with an easy tube removal system for the furnace.
Abstract:
A crucible handling shuttle includes a pair of opposed dual crucible-gripping arms mounted on a rotatable head. The shuttle is removably plugged into a sliding block of a carriage to move between a furnace and a crucible loading station. The carriage includes mechanical, electrical, and pneumatic plugs or sockets which couple to mating sockets or plugs of the shuttle. A linear actuator extends between the carriage and the furnace base to raise and lower the carriage and shuttle coupled thereto.
Abstract:
An interchangeable module for supporting a receptacle into which a molten sample, prepared by a fluxer, can be poured for analysis. One module can support a resistively heated casting dish into which a molten sample can be poured and cooled to form a solid sample for instrumental analysis. This module includes an insulator having a depression for receipt of a casting dish. A heating coil is positioned below the recession. A cooling gas conduit extends through the insulator support. The insulator is supported on a frame. The frame is supported on a back plate.
Abstract:
A multiple frequency plasma torch activation circuit includes a system driver circuit with a pair of different frequency sources and a selector switch which allows one of the sources to be coupled to a splitter assembly which applies signals to a pair of independent power amplifiers having their outputs applied to a combiner assembly and to the plasma torch inductor. A detector circuit provides signals to a power control circuit which includes forward and reflected power monitoring and an impedance matching circuit for optimum coupling of the frequencies to the inductive load.