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1.发明授权公开(公告)号：US09844782B2
公开(公告)日：2017-12-19
申请号：US14307642
申请日：2014-06-18
申请人： 7685297 Canada Inc.
发明人： Ron J. Emburgh , Ravi K. Kanipayor
CPC分类号： B01L7/00 , B01L3/04 , B01L2300/18 , B01L2300/1822 , B01L2300/1844 , B01L2300/1872 , B01L2300/1894 , G01N1/34 , G01N1/4044 , G01N1/44 , G01N21/0332 , Y10T436/25 , Y10T436/25125
摘要： An apparatus for preparing samples for chemical analysis includes a container receptacle for receiving a sample container having a crucible portion and an expansion portion. The container receptacle includes a heating compartment and a cooling compartment spaced apart from the heating compartment. The heating compartment is shaped to receive the crucible portion of the sample container, and the cooling compartment is shaped to receive the expansion portion of the sample container. The apparatus also includes a heating mechanism for heating the sample within the crucible portion of the sample container, a first cooling mechanism for cooling the expansion portion of the sample container, and a second cooling mechanism for cooling the crucible portion of the sample container.
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2.发明申请METHOD AND APPARATUS FOR MULTIPLE SAMPLE PREPARATION AND SIMULTANEOUS LOSS OF IGNITION/GAIN ON IGNITION ANALYSIS, FOR USE IN X-RAY FLUORESCENCE SPECTROMETRY 审中-公开多种样品制备方法和装置，同时点火点火/点火分析增益，用于X射线荧光光谱法公开(公告)号：US20140161150A1
公开(公告)日：2014-06-12
申请号：US13711915
申请日：2012-12-12
CPC分类号： G01N23/2202 , B01F11/0002 , B01F11/0017 , B01F11/0025 , B01F13/1072 , B01F15/065 , B01F2015/062 , B01L3/00 , B01L3/04 , G01G15/00 , G01N1/44 , G01N5/00 , G01N5/045 , G01N23/223 , G01N25/00 , G01N2035/00524 , G01N2035/0439
摘要： The analyzer mixes the material to be analyzed and the flux in sample holders supported by a movable platform within the furnace. A tilt member is provided having multiple stations. Each station has an upstanding pin offset from the center point of the station in a different direction. The platform is indexed relative to the tilt member such that the sample holder aligns with each station, in sequence. As the sample holder aligns with each station, the platform is moved toward the tilt member such that the pin of the aligned station abuts and tilts the sample holder in a different direction. The repeated tilting of the sample holder in different directions mixes the material and flux. The contents of the sample holder may also be agitated by rapidly moving the platform back and forth with sudden stops. The analyzer can be used with a special sample holder.
摘要翻译： 分析仪将要分析的材料和样品架中的通量混合在由炉内的可移动平台支撑的样品架中。 提供具有多个站的倾斜构件。 每个车站都有一个直立的销轴偏离车站的中心点在不同的方向。 平台相对于倾斜构件进行索引，使得样品架按顺序与每个工位对齐。 当样品架与每个工位对齐时，平台朝向倾斜构件移动，使得对准工位的销以不同的方向邻接和倾斜样品架。 样品架在不同方向上的重复倾斜将材料和焊剂混合。 也可以通过以突然的停止方式快速地移动平台来搅拌样品架的内容物。 分析仪可用于特殊的样品架。
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3.发明申请Nickel Crucible for Melting Analytical Sample, Method of Preparing Analytical Sample and Method of Analysis 有权用于熔融分析样品的镍坩埚，制备分析样品的方法和分析方法公开(公告)号：US20100167407A1
公开(公告)日：2010-07-01
申请号：US12278889
申请日：2007-02-15
CPC分类号： G01N1/44 , B01L3/04 , B01L2300/12 , Y10T436/25875
摘要： A nickel crucible used for melting an analytical sample in the pretreatment of the analytical sample, characterized in that the purity of the nickel crucible is 99.9999 wt % or higher. Also provided is a method of analysis, comprising melting a sample by the use of the nickel crucible for melting having a purity of 99.9999 wt % or higher, and analyzing the melt to thereby obtain an analytical result in which the respective lower limits of determination of Mn, Al, Si, Mg, Pb, Fe, Co, Ti, Cu, Cr, Zr, Mo, and W are Mn: 5 wtppm, Al: 10 wtppm, Si: 10 wtppm, Mg: 5 wtppm, Pb: 5 wtppm, Fe: 5 wtppm, Co: 5 wtppm, Ti: 20 wtppm, Cu: 20 wtppm, Cr: 10 wtppm, Zr: 5 wtppm, Mo: 2 wtppm, and W:10 wtppm. In light of the recent analytical technology demanded of fast and accurate measurement of high purity materials, high purity analysis is attained through inhibition of mixing of impurities from the crucible.
摘要翻译： 用于在分析样品的预处理中熔化分析样品的镍坩埚，其特征在于，所述镍坩埚的纯度为99.9999重量％以上。 还提供了一种分析方法，包括通过使用纯度为99.9999重量％以上的熔融用镍坩埚来熔解样品，分析熔融物，得到分析结果，其中， Mn，Al，Si，Mg，Pb，Fe，Co，Ti，Cu，Cr，Zr，Mo和W分别为Mn：5重量ppm，Al：10重量ppm，Si：10重量ppm，Mg：5重量ppm，Pb：5 重量ppm，Fe：5重量ppm，Co：5重量ppm，Ti：20重量ppm，Cu：20重量ppm，Cr：10重量ppm，Zr：5重量ppm，Mo：2重量ppm，W：10重量ppm。 鉴于最近需要快速准确地测量高纯度材料的分析技术，通过抑制来自坩埚的杂质的混合来获得高纯度分析。
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4.发明申请Zirconium Crucible for Melting Analytical Sample, Method of Preparing Analytical Sample and Method of Analysis 有权熔融锆石坩埚分析样品，分析样品的制备方法和分析方法公开(公告)号：US20090104082A1
公开(公告)日：2009-04-23
申请号：US12297789
申请日：2007-02-20
IPC分类号： B01L3/04
CPC分类号： B01L3/04 , B01L2300/12 , C30B15/10 , G01N1/38 , G01N1/44
摘要： Proposed is a zirconium crucible used for melting an analytical sample in the pretreatment of the analytical sample, wherein the purity of the zirconium crucible is 99.99 wt % or higher. in light of the recent analytical technology demanded of fast and accurate measurement of high purity materials, the present invention provides a zirconium crucible for melting an analytical sample, a method of preparing such analytical sample, and a method of analysis that enables the analysis of high purity materials by inhibiting the inclusion of impurities from the crucible regardless of difference in the analysts and their skill.
摘要翻译： 提出了用于在分析样品的预处理中熔化分析样品的锆坩埚，其中锆坩埚的纯度为99.99重量％以上。 鉴于最近需要快速准确地测量高纯度材料的分析技术，本发明提供了一种用于熔化分析样品的锆坩埚，这种分析样品的制备方法以及能够分析高纯度材料的分析方法 通过抑制坩埚中杂质的含量，无论分析人员和技术人员的差异如何，都是纯度高的材料。
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公开(公告)号：US20030003016A1
公开(公告)日：2003-01-02
申请号：US09894591
申请日：2001-06-28
IPC分类号： G01N035/00 , B32B005/02 , B32B027/04 , B32B027/12 , G01N033/00 , G01N031/00 , B01L003/00 , G01N021/00
CPC分类号： B01L3/04 , G01G19/00 , G01N1/2208 , G01N31/12 , G01N2001/2223 , G01N2001/245 , Y10T436/11 , Y10T436/111666 , Y10T436/112499
摘要： An apparatus is provided to automatically cover and uncover crucibles according to a predetermined procedure in a proximate analyzer. A series of crucibles mounted in a first carousel is heated in a furnace. A second carousel mounted above the first carousel holds crucible covers. A mechanism synchronizes the movements of the carousels so that the heated crucibles are automatically covered and uncovered at the appropriate times during the analysis with a corresponding cover by lowering or raising the second carousel. The movements of both carousels are automatically controlled so that at appropriate points in the testing cycle they rotate simultaneously about a common central axis and a crucible is deposited on a weighing platform by controlling the vertical motion of the entire carousel apparatus. The crucible is weighed either with or without a crucible cover depending on the stage of the analysis without the need of manual intervention.
摘要翻译： 提供一种根据临近分析仪中的预定程序自动覆盖和揭开坩埚的装置。 安装在第一转盘中的一系列坩埚在炉中加热。 安装在第一转盘上方的第二转盘固定坩埚盖。 一种机构使转盘的运动同步，使得通过降低或升高第二转盘在分析期间的适当时间，加热的坩埚被自动覆盖和未覆盖。 自动控制两个转盘的移动，使得在测试循环中的适当点，它们绕共同的中心轴线同时旋转，坩埚通过控制整个转盘装置的垂直运动而沉积在称重平台上。 根据分析阶段，坩埚被称重，无论是否有坩埚盖，无需手动干预。
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公开(公告)号：US5762865A
公开(公告)日：1998-06-09
申请号：US794536
申请日：1997-02-03
CPC分类号： B01L3/04 , C30B15/10 , C30B35/002
摘要： A pyrolytic boron nitride crucible is disclosed which is suitable for producing a single crystal of a semiconductor compound of Group III and V by the LEC method. The crucible comprises a side part and a bottom part. The bottom part has an absorption coefficient of light of wavelengths between 3,700 cm.sup.-1 and 6,500 cm.sup.-1 of at most 1.7 and/or the absorption coefficient of light of wavelengths between 3,700 cm.sup.-1 to 6,500 cm.sup.-1 of the bottom part is less than that of the side part by at least 0.5. In the crucible, the heat conduction from the bottom part to material melt in the crucible is strengthened, so that the convection flow of the material melt is suppressed and the temperature distribution in the crucible can be easily controlled.
摘要翻译： 公开了一种热解氮化硼坩埚，其适用于通过LEC方法制备III族和V族半导体化合物的单晶。 坩埚包括侧部和底部。 底部的波长在3,700cm -1至6,500cm -1之间的吸收系数至多为1.7，和/或底部波长在3,700cm -1至6,500cm -1之间的光的吸收系数为 小于侧面部分至少0.5。 在坩埚中，坩埚中从底部到材料熔体的热传导得到加强，从而抑制了材料熔体的对流，并且可以容易地控制坩埚中的温度分布。
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公开(公告)号：US5269827A
公开(公告)日：1993-12-14
申请号：US664052
申请日：1991-03-01
IPC分类号： G01N23/223 , B01L3/04 , G01N1/28 , G01N1/44 , C03B5/18
摘要： An instrument and system for the preparation of a sample for analysis provides a crucible holder which improves the holding and control of a melting crucible during operation of the device for agitating a powdered sample and flux while being heated. The crucible holder is coupled to an agitation assembly which provides independently controlled operation on two different axes using separately adjustable variable frequency and amplitude motion along each of the two operating axes to provide an finite number of agitation patterns for the crucible. In one preferred embodiment of the invention, the heating flame is controlled by controlling the supply of compressed air and a combustion gas. In another preferred embodiment of the invention, a pilot burner is provided which both ignites the main burner located under the crucible and preheats the casting dish to a temperature which is substantially the same as the crucible. The pilot also can control air only flow directed to the casting dish for controllably cooling the sample melt to form the sample bead.
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公开(公告)号：US4746362A
公开(公告)日：1988-05-24
申请号：US29989
申请日：1987-03-25
申请人： Jean Morice , Jean-Jacques Perrier
发明人： Jean Morice , Jean-Jacques Perrier
IPC分类号： G01N33/20 , B01L3/04 , C22B21/00 , C22C20060101 , C22C1/02 , C22C21/00 , G01N25/04 , G01N25/06
CPC分类号： B01L3/04
摘要： A crucible for the thermal analysis of aluminum alloys is disclosed. This crucible is characterized in that the internal surface of at least one of its side walls is at least partially covered with a film of refining agent. The crucible finds application in measuring both the silicon content in and the degree of refining of hypereutectic aluminum-silicon alloys.
摘要翻译： 公开了一种用于铝合金热分析的坩埚。 该坩埚的特征在于，其至少一个侧壁的内表面至少部分被一层澄清剂覆盖。 该坩埚可用于测量过共晶铝硅合金的硅含量和精炼度。
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公开(公告)号：US4559201A
公开(公告)日：1985-12-17
申请号：US572890
申请日：1984-01-23
申请人： Takeshi Yamada , Hideki Ohashi , Masahiro Tanimoto
发明人： Takeshi Yamada , Hideki Ohashi , Masahiro Tanimoto
CPC分类号： G01N33/20 , B01L3/04 , G01N31/12 , G01N35/00 , G01N35/026 , Y10T436/176921 , Y10T436/188 , Y10T436/23
摘要： A crucible cassette for use in feeding crucibles to an apparatus for loading and feeding crucibles to a combustion furnace, said cassette having at least one crucible receiving tube capable of receiving a plurality of crucibles stacked one above the other, an engaging member in the bottom of the tube for engaging with the lowermost crucible and supporting it in the receiving tube and a guide member for guiding the rise of the crucibles in the tube, and a pusher for pushing crucibles one by one up out of said tube to enable them to be carried one by one from the cassette means to a sample weighing position in the apparatus.
摘要翻译： 一种坩埚盒，用于将坩埚送入用于将坩埚装载和供给到燃烧炉的装置，所述盒具有至少一个坩埚接收管，所述坩埚接收管能够容纳多个堆叠在一起的坩埚， 用于与最下坩埚接合并将其支撑在接收管中的管和用于引导坩埚在管中的上升的引导构件，以及用于将坩埚一个一个地推出所述管的推动器，以使其能够承载 逐个从盒装置到设备中的样品称重位置。
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