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    METHOD AND APPARATUS FOR PREPARATION OF GRANULAR POLYSILICON
    11.
    发明申请
    METHOD AND APPARATUS FOR PREPARATION OF GRANULAR POLYSILICON 有权
    用于制备颗粒聚硅氧烷的方法和装置

    公开(公告)号：US20100068116A1

    公开(公告)日：2010-03-18

    申请号：US12609414

    申请日：2009-10-30

    申请人： Hee Young KIM ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    发明人： Hee Young KIM ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC分类号： C01B33/021 ,  B01J8/24

    CPC分类号： C01B33/027 ,  C23C16/24 ,  C23C16/4401 ,  C23C16/442

    摘要： A process for preparing granular polysilicon using a fluidized bed reactor is disclosed. The upper and lower spaces of the bed are defined as a reaction zone and a heating zone, respectively, with the height of the reaction gas outlet being selected as the reference height. The invention maximizes the reactor productivity by sufficiently providing the heat required and stably maintaining the reaction temperature in the reaction zone, without impairing the mechanical stability of the fluidized bed reactor. This is achieved through electrical resistance heating in the heating zone where an internal heater is installed in a space in between the reaction gas supplying means and the inner wall of the reactor tube, thereby heating the fluidizing gas and the silicon particles in the heating zone. The heat generated in the heating zone is transferred to the reaction zone by supplying the fluidizing gas at such a rate that the silicon particles can be intermixed between the reaction zone and the heating zone in a continuous, fluidized state.

    摘要翻译： 公开了一种使用流化床反应器制备颗粒状多晶硅的方法。 床的上部和下部空间分别被定义为反应区和加热区，反应气体出口的高度被选择为参考高度。 本发明通过充分提供所需的热量并稳定地维持反应区域中的反应温度，而不损害流化床反应器的机械稳定性，使反应器生产率最大化。 这是通过加热区域中的电阻加热来实现的，其中内部加热器安装在反应气体供给装置和反应器管的内壁之间的空间中，从而加热流化气体和加热区域中的硅颗粒。 通过以使得硅颗粒能够以连续流化状态在反应区和加热区之间混合的速率供给流化气体，将加热区中产生的热转移到反应区。

    HIGH-PRESSURE FLUIDIZED BED REACTOR FOR PREPARING GRANULAR POLYCRYSTALLINE SILICON
    12.
    发明申请
    HIGH-PRESSURE FLUIDIZED BED REACTOR FOR PREPARING GRANULAR POLYCRYSTALLINE SILICON 有权
    用于制备颗粒状聚硅氧烷的高压流化床反应器

    公开(公告)号：US20100047136A1

    公开(公告)日：2010-02-25

    申请号：US12609364

    申请日：2009-10-30

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC分类号： G05D16/00 ,  B01J8/18

    CPC分类号： C01B33/027 ,  B01J3/046 ,  B01J8/1827 ,  B01J8/1836 ,  B01J2208/00398 ,  B01J2208/00407 ,  C01B33/029 ,  C01B33/03

    摘要： The present invention relates to a high-pressure fluidized bed reactor for preparing granular polycrystalline silicon, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under the inert gas atmosphere, and (d) a controlling means to keep the difference between pressures in the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby enabling to maintain physical stability of the reactor tube and efficiently prepare granular polycrystalline silicon even at relatively high reaction pressure.

    摘要翻译： 本发明涉及一种用于制备颗粒状多晶硅的高压流化床反应器，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区，其中 形成硅颗粒床并发生硅沉积，并且在反应器壳体和反应器管之间形成的外部区域保持在惰性气体气氛下，以及（d）控制装置，以保持在 内部区域和外部区域保持在0至1巴的范围内，从而能够保持反应管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    Apparatus and Methods for Preparation of High-Purity Silicon Rods Using Mixed Core Means
    14.
    发明申请
    Apparatus and Methods for Preparation of High-Purity Silicon Rods Using Mixed Core Means 有权
    使用混合核心装置制备高纯度硅棒的装置和方法

    公开(公告)号：US20090130333A1

    公开(公告)日：2009-05-21

    申请号：US12160241

    申请日：2007-05-11

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    IPC分类号： B05D3/14 ,  B05C9/08

    CPC分类号： C01B33/035 ,  Y10T117/10 ,  Y10T117/1004

    摘要： Disclosed are a method and an apparatus for preparing a polycrystalline silicon rod using a mixed core means, comprising: installing a first core means made of a resistive material together with a second core means made of silicon material in an inner space of a deposition reactor; electrically heating the first core means and pre-heating the second core by the first core means which is electrically heated; electrically heating the preheated second core means; and supplying a reaction gas into the inner space in a state where the first core means and the second core means are electrically heated for silicon deposition.

    摘要翻译： 公开了一种使用混合芯装置制备多晶硅棒的方法和装置，包括：在沉积反应器的内部空间中安装由电阻材料制成的第一芯装置和由硅材料制成的第二芯装置; 电加热第一芯装置并且通过电加热的第一芯装置预加热第二芯; 电加热预热的第二芯装置; 以及在第一芯装置和第二芯装置被电加热以进行硅沉积的状态下将反应气体供应到内部空间中。

    Method for Preparing Granular Polycrystalline Silicon Using Fluidized Bed Reactor
    15.
    发明申请
    Method for Preparing Granular Polycrystalline Silicon Using Fluidized Bed Reactor 有权
    使用流化床反应器制备颗粒状多晶硅的方法

    公开(公告)号：US20090004090A1

    公开(公告)日：2009-01-01

    申请号：US12160145

    申请日：2007-02-14

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC分类号： C01B33/027 ,  C30B28/14 ,  C30B29/06

    CPC分类号： C01B33/027 ,  C01B33/029 ,  C01B33/03

    摘要： The present invention relates to a method for mass preparation of granular polycrystalline silicon in a fluidized bed reactor, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under an inert gas atmosphere, and (d) a controlling means to keep the pressure difference between the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby capable of maintaining physical stability of the reactor tube and efficiently preparing granular polycrystalline silicon even at a relatively high reaction pressure.

    摘要翻译： 本发明涉及一种在流化床反应器中大量制备颗粒状多晶硅的方法，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区 ，其中形成硅颗粒床并发生硅沉积，以及形成在反应器壳和反应器管之间的外部区域，其保持在惰性气体气氛下，以及（d）控制装置，以保持压力差之间的压力差 内部区域和外部区域保持在0至1巴的范围内，从而能够维持反应器管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    High-pressure fluidized bed reactor for preparing granular polycrystalline silicon
    17.
    发明授权
    High-pressure fluidized bed reactor for preparing granular polycrystalline silicon 有权
    用于制备颗粒状多晶硅的高压流化床反应器

    公开(公告)号：US07972562B2

    公开(公告)日：2011-07-05

    申请号：US12093513

    申请日：2007-02-07

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC分类号： G05D16/00 ,  B01J19/00 ,  B01J8/18 ,  F27B15/08 ,  F27B15/14 ,  F27B15/16 ,  C01B33/02

    CPC分类号： C01B33/027 ,  B01J3/046 ,  B01J8/1827 ,  B01J8/1836 ,  B01J2208/00398 ,  B01J2208/00407 ,  C01B33/029 ,  C01B33/03

    摘要： The present invention relates to a high-pressure fluidized bed reactor for preparing granular polycrystalline silicon, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under the inert gas atmosphere, and (d) a controlling means to keep the difference between pressures in the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby enabling to maintain physical stability of the reactor tube and efficiently prepare granular polycrystalline silicon even at relatively high reaction pressure.

    摘要翻译： 本发明涉及一种用于制备颗粒状多晶硅的高压流化床反应器，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区，其中 形成硅颗粒床并发生硅沉积，并且在反应器壳体和反应器管之间形成的外部区域保持在惰性气体气氛下，以及（d）控制装置，以保持在 内部区域和外部区域保持在0至1巴的范围内，从而能够保持反应管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    APPARATUS AND METHODS FOR PREPARATION OF HIGH-PURITY SILICON RODS USING MIXED CORE MEANS
    18.
    发明申请
    APPARATUS AND METHODS FOR PREPARATION OF HIGH-PURITY SILICON RODS USING MIXED CORE MEANS 审中-公开
    使用混合核心方法制备高纯度硅棒的装置和方法

    公开(公告)号：US20100040803A1

    公开(公告)日：2010-02-18

    申请号：US12603278

    申请日：2009-10-21

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    IPC分类号： C23C16/24 ,  B05C11/00

    CPC分类号： C01B33/035 ,  Y10T117/10 ,  Y10T117/1004

    摘要： Disclosed are a method and an apparatus for preparing a polycrystalline silicon rod using a mixed core means, comprising: installing a first core means made of a resistive material together with a second core means made of silicon material in an inner space of a deposition reactor; electrically heating the first core means and pre-heating the second core by the first core means which is electrically heated; electrically heating the preheated second core means; and supplying a reaction gas into the inner space in a state where the first core means and the second core means are electrically heated for silicon deposition.

    摘要翻译： 公开了一种使用混合芯装置制备多晶硅棒的方法和装置，包括：在沉积反应器的内部空间中安装由电阻材料制成的第一芯装置和由硅材料制成的第二芯装置; 电加热第一芯装置并且通过电加热的第一芯装置预加热第二芯; 电加热预热的第二芯装置; 以及在第一芯装置和第二芯装置被电加热以进行硅沉积的状态下将反应气体供应到内部空间中。

    Method and Apparatus for Preparation of Granular Polysilicon
    20.
    发明申请
    Method and Apparatus for Preparation of Granular Polysilicon 有权
    颗粒多晶硅的制备方法和装置

    公开(公告)号：US20090047204A1

    公开(公告)日：2009-02-19

    申请号：US12282604

    申请日：2007-08-09

    申请人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    发明人： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC分类号： C01B33/021 ,  B01J8/24

    CPC分类号： C01B33/027 ,  C23C16/24 ,  C23C16/4401 ,  C23C16/442

    摘要： A process for preparing granular polysilicon using a fluidized bed reactor is disclosed. The upper and lower spaces of the bed are defined as a reaction zone and a heating zone, respectively, with the height of the reaction gas outlet being selected as the reference height. The invention maximizes the reactor productivity by sufficiently providing the heat required and stably maintaining the reaction temperature in the reaction zone, without impairing the mechanical stability of the fluidized bed reactor. This is achieved through electrical resistance heating in the heating zone where an internal heater is installed in a space in between the reaction gas supplying means and the inner wall of the reactor tube, thereby heating the fluidizing gas and the silicon particles in the heating zone. The heat generated in the heating zone is transferred to the reaction zone by supplying the fluidizing gas at such a rate that the silicon particles can be intermixed between the reaction zone and the heating zone in a continuous, fluidized state.

    摘要翻译： 公开了一种使用流化床反应器制备颗粒状多晶硅的方法。 床的上部和下部空间分别被定义为反应区和加热区，反应气体出口的高度被选择为参考高度。 本发明通过充分提供所需的热量并稳定地维持反应区域中的反应温度，而不损害流化床反应器的机械稳定性，使反应器生产率最大化。 这是通过加热区域中的电阻加热来实现的，其中内部加热器安装在反应气体供给装置和反应器管的内壁之间的空间中，从而加热流化气体和加热区域中的硅颗粒。 通过以使得硅颗粒能够以连续流化状态在反应区和加热区之间混合的速率供给流化气体，将加热区中产生的热转移到反应区。