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    Method and apparatus for preparation of granular polysilicon
    2.
    发明授权
    Method and apparatus for preparation of granular polysilicon 有权
    颗粒状多晶硅的制备方法和装置

    公开(公告)号：US08821827B2

    公开(公告)日：2014-09-02

    申请号：US12609414

    申请日：2009-10-30

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC: C01B33/021 ,  B01J8/24

    CPC classification number: C01B33/027 ,  C23C16/24 ,  C23C16/4401 ,  C23C16/442

    Abstract: An apparatus for preparing granular polysilicon comprises a reactor tube, a reactor shell, an internal heater, and components for controlling pressure, supplying a fluidizing gas and a reaction gas, discharging gas, and discharging particles. The reactor tube is associated with an inner space comprising an inner zone that contains a bed of silicon particles and is the site at which silicon deposition occurs. The inner zone comprises a heating zone and a reaction zone. The fluidizing gas supplying component supplies a fluidizing gas for fluidizing the bed of silicon particles to a bottom of the heating zone. The apparatus can minimize the problems occurring during the heating of silicon particles at high temperature for silicon deposition on the surface of the silicon particles.

    Abstract translation: 制备颗粒状多晶硅的装置包括反应器管，反应器壳，内部加热器和用于控制压力的部件，供应流化气体和反应气体，排出气体和排出颗粒。 反应器管与包含含有硅颗粒床的内部区域的内部空间相关联，并且是发生硅沉积的位置。 内部区域包括加热区域和反应区域。 流化气体供应部件提供用于使硅颗粒床流化到加热区的底部的流化气体。 该装置可以最大限度地减少硅粒子在高温下加热硅沉积在硅颗粒表面上的问题。

    Apparatus and methods for preparation of high-purity silicon rods using mixed core means
    4.
    发明授权
    Apparatus and methods for preparation of high-purity silicon rods using mixed core means 有权
    使用混合核心装置制备高纯度硅棒的装置和方法

    公开(公告)号：US08430959B2

    公开(公告)日：2013-04-30

    申请号：US12160241

    申请日：2007-05-11

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Won Wook So

    IPC: C30B25/02

    CPC classification number: C01B33/035 ,  Y10T117/10 ,  Y10T117/1004

    Abstract: Disclosed are a method and an apparatus for preparing a polycrystalline silicon rod using a mixed core means, comprising: installing a first core means made of a resistive material together with a second core means made of silicon material in an inner space of a deposition reactor; electrically heating the first core means and pre-heating the second core by the first core means which is electrically heated; electrically heating the preheated second core means; and supplying a reaction gas into the inner space in a state where the first core means and the second core means are electrically heated for silicon deposition.

    Abstract translation: 公开了一种使用混合芯装置制备多晶硅棒的方法和装置，包括：在沉积反应器的内部空间中安装由电阻材料制成的第一芯装置和由硅材料制成的第二芯装置; 电加热第一芯装置并且通过电加热的第一芯装置预加热第二芯; 电加热预热的第二芯装置; 以及在第一芯装置和第二芯装置被电加热以进行硅沉积的状态下将反应气体供应到内部空间中。

    Methods for preparation of high-purity polysilicon rods using a metallic core means
    5.
    发明授权
    Methods for preparation of high-purity polysilicon rods using a metallic core means 有权
    使用金属芯制备高纯度多晶硅棒的方法

    公开(公告)号：US07923358B2

    公开(公告)日：2011-04-12

    申请号：US12603072

    申请日：2009-10-21

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Sang Jin Moon

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi ,  Sang Jin Moon

    IPC: C23C16/24

    CPC classification number: C23C16/4581 ,  C01B33/035 ,  C23C16/24 ,  Y10T428/2913

    Abstract: The present invention relates to a method for preparing a polysilicon rod using a metallic core means, comprising: installing a core means in an inner space of a deposition reactor used for preparing a silicon rod, wherein the core means is constituted by forming one or a plurality of separation layer(s) on the surface of a metallic core element and is connected to an electrode means; heating the core means by supplying electricity through the electrode means; and supplying a reaction gas into the inner space for silicon deposition, thereby forming a deposition output in an outward direction on the surface of the core means. According to the present invention, the deposition output and the core means can be separated easily from the silicon rod output obtained by the process of silicon deposition, and the contamination of the deposition output caused by impurities of the metallic core element can be minimized, thereby a high-purity silicon can be prepared in a more economic and convenient way.

    Abstract translation: 本发明涉及一种使用金属芯装置制备多晶硅棒的方法，包括：在用于制备硅棒的沉积反应器的内部空间中安装芯装置，其中芯装置通过形成一个或一个 金属芯体表面上的多个分离层连接到电极装置; 通过电极装置供电来加热芯装置; 并将反应气体供给到用于硅沉积的内部空间中，从而在芯装置的表面上沿向外的方向形成沉积输出。 根据本发明，沉积输出和芯装置可以容易地从通过硅沉积过程获得的硅棒输出分离，并且可以最小化由金属芯元件的杂质引起的沉积输出的污染，由此 可以以更经济和便利的方式制备高纯度硅。

    Method for preparing granular polycrystalline silicon using fluidized bed reactor
    6.
    发明授权
    Method for preparing granular polycrystalline silicon using fluidized bed reactor 有权
    使用流化床反应器制备颗粒状多晶硅的方法

    公开(公告)号：US07771687B2

    公开(公告)日：2010-08-10

    申请号：US12160145

    申请日：2007-02-14

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC: B01J8/18 ,  B01J8/42 ,  B01J9/12 ,  C01B33/02 ,  C01B33/21 ,  C01B33/27

    CPC classification number: C01B33/027 ,  C01B33/029 ,  C01B33/03

    Abstract: The present invention relates to a method for mass preparation of granular polycrystalline silicon in a fluidized bed reactor, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under an inert gas atmosphere, and (d) a controlling means to keep the pressure difference between the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby capable of maintaining physical stability of the reactor tube and efficiently preparing granular polycrystalline silicon even at a relatively high reaction pressure.

    Abstract translation: 本发明涉及一种在流化床反应器中大量制备颗粒状多晶硅的方法，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区 ，其中形成硅颗粒床并发生硅沉积，以及形成在反应器壳和反应器管之间的外部区域，其保持在惰性气体气氛下，以及（d）控制装置，以保持压力差之间的压力差 内部区域和外部区域保持在0至1巴的范围内，从而能够维持反应器管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    Nano-structured metal-carbon composite and process for preparation thereof
    7.
    发明申请
    Nano-structured metal-carbon composite and process for preparation thereof 审中-公开
    纳米结构金属 - 碳复合材料及其制备方法

    公开(公告)号：US20060240256A1

    公开(公告)日：2006-10-26

    申请号：US10553271

    申请日：2004-04-16

    Applicant: Seong Woo ,  Won Choon Choi

    Inventor： Seong Woo ,  Won Choon Choi

    IPC: D01D5/40 ,  B32B5/16

    CPC classification number: B82Y30/00 ,  C01B3/0021 ,  C01B3/0026 ,  C01B3/0078 ,  C01B32/00 ,  Y02E60/325 ,  Y02E60/327 ,  Y10T428/2982

    Abstract: Disclosed are a nano-structured metal-carbon composite and a process for preparation thereof. More specifically, a nano-structured metal-carbon composite is prepared by continuously impregnating a transition metal precursor and a carbon precursor into a nano template and reacting the resultant mixture at high temperature. In the composite according to the present invention, metal is regularly multi-dispersed in a size of less than 1 nano meter, and metal and carbon are chemically bonded, thereby exhibiting the highly excellent hydrogen storage capacity.

    Abstract translation: 公开了一种纳米结构金属 - 碳复合材料及其制备方法。 更具体地，通过将​​过渡金属前体和碳前体连续浸渍到纳米模板中并在高温下使所得混合物反应来制备纳米结构金属 - 碳复合材料。 在根据本发明的复合材料中，金属规则地以小于1纳米的尺寸多分散，金属和碳化学键合，从而表现出极好的储氢能力。

    Modified magnesium oxide catalyst
    8.
    发明授权
    Modified magnesium oxide catalyst 失效
    改性氧化镁催化剂

    公开(公告)号：US5371306A

    公开(公告)日：1994-12-06

    申请号：US175297

    申请日：1993-12-29

    Applicant: Seong-Ihl Woo ,  Won-Choon Choi ,  Kwang-Ho Park ,  Jin-Do Kim

    Inventor： Seong-Ihl Woo ,  Won-Choon Choi ,  Kwang-Ho Park ,  Jin-Do Kim

    IPC: B01J21/10 ,  B01J23/34 ,  B01J23/889 ,  C07C37/11 ,  C07C37/00 ,  B01J23/00 ,  B01J23/32

    CPC classification number: B01J23/8892 ,  B01J21/10 ,  B01J23/34 ,  C07C37/16

    Abstract: The present invention relates to a novel oxide catalyst, more specifically, a novel modified magnesium oxide catalyst which is highly active and selective for ortho-alkylation of phenol.The catalysts for phenol alkylation of the invention are represented as Mg.sub.a Mn.sub.b L.sub.c T.sub.d Q.sub.e O.sub.x .wherein:L is vanadium or chromium;T is alkali metal, alkali earth metal, lead, bisumth, cobalt, aluminum, silicon., gallium, germanium or molybdenum;Q is antimony, cesium or iron;b/a=0 to 0.35(atomic molar ratio);c/a=0.01 to 0.35(atomic molar ratio);d/a=0 to 0.35(atomic molar ratio);e/c=0.1 to 10(atomic molar ratio); and,x is determined by oxidation state of each component.

    Abstract translation: 本发明涉及一种新型氧化物催化剂，更具体地说，涉及一种对苯酚进行正烷基化反应具有高活性和选择性的新型改性氧化镁催化剂。 本发明的苯酚烷基化催化剂表示为MgaMnbLcTdQeOx。 其中：L为钒或铬; T是碱金属，碱土金属，铅，二价，钴，铝，硅，镓，锗或钼; Q是锑，铯或铁; b / a = 0〜0.35（原子摩尔比）; c / a = 0.01〜0.35（原子摩尔比）; d / a = 0〜0.35（原子摩尔比）; e / c = 0.1〜10（原子摩尔比）; 并且x由每个组分的氧化态决定。

    Method and apparatus for preparation of granular polysilicon
    10.
    发明授权
    Method and apparatus for preparation of granular polysilicon 有权
    颗粒状多晶硅的制备方法和装置

    公开(公告)号：US08747757B2

    公开(公告)日：2014-06-10

    申请号：US12282604

    申请日：2007-08-09

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC: C01B33/021 ,  B01J8/24

    CPC classification number: C01B33/027 ,  C23C16/24 ,  C23C16/4401 ,  C23C16/442

    Abstract: A process for preparing granular polysilicon using a fluidized bed reactor is disclosed. Upper and lower spaces of the bed are the reaction zone and heating zone, respectively, wherein the height of the reaction gas outlet is the reference height. Reactor productivity is maximized by sufficiently providing the heat required and stably maintaining the reaction temperature in the reaction zone, without impairing the mechanical stability of the fluidized bed reactor. This is achieved through electrical resistance heating in the heating zone where an internal heater is installed between the reaction gas supplying means and the inner wall of the reactor tube, thereby heating the fluidizing gas and the silicon particles in the heating zone. The heat generated is transferred to the reaction zone by supplying the fluidizing gas at a rate silicon particles can be intermixed between the reaction zone and the heating zone in a continuous, fluidized state.

    Abstract translation: 公开了一种使用流化床反应器制备颗粒状多晶硅的方法。 床的上部和下部空间分别是反应区和加热区，其中反应气体出口的高度是参考高度。 通过充分提供所需的热量并稳定地维持反应区中的反应温度，而不损害流化床反应器的机械稳定性，使反应器生产率最大化。 这通过在反应气体供给装置和反应器管的内壁之间安装有内部加热器的加热区域中的电阻加热来实现，从而加热流化气体和加热区域中的硅颗粒。 通过以一定速率供应流化气体将产生的热量转移到反应区，硅颗粒可以在连续的流化状态下混合在反应区和加热区之间。

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