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    Intermediates for dipyrrylmethene dyes
    11.
    发明授权
    Intermediates for dipyrrylmethene dyes 失效
    二吡咯甲烷染料中间体

    公开(公告)号：US3883555A

    公开(公告)日：1975-05-13

    申请号：US25059672

    申请日：1972-05-05

    Applicant: POLAROID CORP

    Inventor： BLOOM STANLEY M ,  GARCIA PAULINA P

    IPC: C09B23/04 ,  C07D27/26

    CPC classification number: C09B23/04

    Abstract: Novel Dipyrrylmethene dyes, particularly 5 and/or 5''-odihydroxyphenyl dipyrrylmethene dyes, and 1:1 metal complexes thereof.

    Abstract translation: 新型二吡咯甲烷染料，特别是5和/或5'-邻二羟基苯基二吡咯甲烷染料及其1：1金属络合物。

    Diffusion transfer photographic processes and elements utilizing ph-sensitive agents to prevent fogging by extraneous actinic radiation during development
    12.
    发明授权
    Diffusion transfer photographic processes and elements utilizing ph-sensitive agents to prevent fogging by extraneous actinic radiation during development 失效
    扩张转印摄影过程和元素利用敏感剂在发展过程中防止超临界辐射引起的潮气

    公开(公告)号：US3702244A

    公开(公告)日：1972-11-07

    申请号：US3702244D

    申请日：1971-01-21

    Applicant: POLAROID CORP

    Inventor： BLOOM STANLEY M ,  BORROR ALAN L ,  HUYFFER PAUL S ,  MACGREGOR PAUL T

    IPC: C09B11/08 ,  G03C8/48 ,  G03C7/00 ,  G03C1/40 ,  G03C5/54

    CPC classification number: G03C8/48 ,  C09B11/08

    Abstract: THIS INVENTION RELATES TO PHOTOGRAPHY, AND MORE PARTICULARLY, IT RELATES TO THE USE OF CERTAIN INDICATOR DYES DERIVED FROM INDOLES AS OPTICAL FILTER AGENTS TO PROTECT A SELECTIVELY EXPOSED PHOTOSENSITIVE MATERIAL FROM POSTEXPOSURE FOGGING IN PHOTOGRAPHIC PROCESSES WHERE DEVELOPMENT OF THE PHOTOSENSITIVE MATERIAL IS CONDUCTED IN THE PRESENCE OF EXTRANEOUS INCIDENT LIGHT. THESE INDICATOR DYES CONTAIN AN INDOLE RADICAL, A SECOND AROMATIC RADICAL AND A RING-CLOSING MOIETY BONDED TO THE AROMATIC RADICAL AND TO THE 2- OR 3-POSITION OF THE INDOLE RADICAL. AT A FIRST PH THEY HAVE A HIGHLY COLORED, LIGHT-ABSORBING FORM CAPABLE OF ABSORBING RADIATION WITHIN A PREDETERMINED WAVELENGTH RANGE IS THE SHORTER WAVELENGTH REGION OF THE VISIBLE SPECTRUM AND AT A SECOND PH HAVE A COLORLESS FORM THAT IS SUBSTANTIALLY NON-LIGHT-ABSORBING IN THE VISIBLE

    SPECTRUM. BY SELECTING A DYE FROM THIS CLASS WHICH IS IN ITS LIGHT-ABSORBING FORM AT THE PH AT WHICH DEVELOPMENT IS PERFORMED, PROTECTION OF THE EXPOSED PHOTOSENSITIVE MATERIAL FROM RADIATION ACTINIC THERETO IS AFFORDED WITHIN THE WAVELENGTH RANGE ABSORBED BY THE DYE AND SUBSEQUENT TO AT LEAST THE INITIAL STAGES OF DEVELOPMENT, THE DYE MAY BE RENDERED SUBSTANTIALLY COLORLESS BY ADJUSTING THE PH TO PERMIT VIEWING OF THE FINAL IMAGE.

    Diffusion transfer employing ringclosure to release color-providing material for transfer
    14.
    发明授权
    Diffusion transfer employing ringclosure to release color-providing material for transfer 失效
    扩张转移使用环形释放颜色提供的材料进行转印

    公开(公告)号：US3443940A

    公开(公告)日：1969-05-13

    申请号：US3443940D

    申请日：1967-07-24

    Applicant: POLAROID CORP

    Inventor： BLOOM STANLEY M ,  ROGERS HOWARD G

    IPC: C07C205/59 ,  C09B1/515 ,  C09B1/54 ,  C09B43/00 ,  C09B43/32 ,  C09B45/16 ,  G03C8/04 ,  G03C8/08 ,  G03C8/12 ,  G03C7/30

    CPC classification number: G03C8/12 ,  C07C205/59 ,  C09B1/503 ,  C09B1/515 ,  C09B1/545 ,  C09B43/00 ,  C09B43/32 ,  C09B43/325 ,  C09B45/16 ,  G03C8/045 ,  G03C8/08

    Abstract: 1,243,048. Azo and anthraquinone dyes. INTERNATIONAL POLAROID' CORP. 23 July; 1968 [24 July, 1967], No. 1734/71 Divided out of 1,243,045. Heading C4P. [Also in Division C2] Mono-azo, dis-azo or anthraquinone dyes for photographic transfer processes are-of formula wherein A represents the atoms necessary to complete a benzene or naphthalene radical that may be further substituted; D is a monoazo, disazo or anthraquinone colour providing moiety, Z is hydrogen, chloro, bromo, carboxy sulpho, hydroxy, alkoxy, hydroxyalkyl, or an aromatic amino radical unsubstituted ortho to said amino group; Y is the residue'of an acid group forming an amide with and reducing the basic character of the nitrogen atom to which it is bonded; X is hydroxy; or when Z is an anilino or naphthylamino radical containing, a y-amino or p-hydroxy substituent but unsubstituted ortho to said amino group joined to the ring completed by A, X may also be hydrogen or a primary, secondary or tertiary amino group or an alkyl, aromatic or heterpcyclic substituent; R 1 is hydrogen, alkyl, cycloalkyl or substituted alkyl, and wherein the values of A, X, Z and R 1 are such that the compound is non-diffusible in alkaline photographic processing solution. The examples describe (1) reacting (2- hydroxy - 4 - amine-HCl - 5 - chloro - 4 1 - carbon-dodecylamide) diphenyl and 4- (2-naphthol- 1 - azo) benzene sulphonyl chloride (A) to form a dye of Formula (I) (2) reacting N'-(o-aminophenyl)-4-methoxy-3- (N 1 ,-dodecylamidoethyl) aniline (B) and sulphonyl chloride (A) to form a dye of Formula (XIX) (3) repeating (2) but using an octadecamido compound to form a dye of Formula (XX) (4) reacting diazotized sulphanilic and 1-phenyl- 3. - carbethoxy - pyrazolone - 5 to form 1- phenyl - 3 - carbethoxy - 4 - (p -,'ulphophenylaze)- pyrazolone-5 sodium salt which,is reacted with propylamine to form the corresponding 3-propylamido compound which is reacted with thionyl chloride to form the corresponding pchlorosulphonylphenylazo compound which is reacted with compound (B) to form a methoxy compound which is demethylated with BBr 3 to form a due of Formula (XXI) (5) 2 - amino - 4 - stearylamide. - N - (41.- methoxy - 3 1 - carboxyphenyl) aniline is reacted with 4 1 - (sulphonylchloride) - phenylazo - 2 - naphthol to form a methoxy compound which is demethylated to a dye of Formula (XVI).

    Differential mobility of color moiety in color transfer
    15.
    发明授权
    Differential mobility of color moiety in color transfer 失效
    彩色传输中色彩运动的差异移动

    公开(公告)号：US3443939A

    公开(公告)日：1969-05-13

    申请号：US3443939D

    申请日：1967-07-24

    Applicant: POLAROID CORP

    Inventor： BLOOM STANLEY M ,  STEPHENS ROBERT K

    IPC: C07C205/59 ,  C09B1/515 ,  C09B1/54 ,  C09B43/00 ,  C09B43/32 ,  C09B45/16 ,  G03C8/04 ,  G03C8/08 ,  G03C8/12 ,  G03C7/00 ,  G03C5/54

    CPC classification number: G03C8/12 ,  C07C205/59 ,  C09B1/503 ,  C09B1/515 ,  C09B1/545 ,  C09B43/00 ,  C09B43/32 ,  C09B43/325 ,  C09B45/16 ,  G03C8/045 ,  G03C8/08

    Abstract: 1,243,048. Azo and anthraquinone dyes. INTERNATIONAL POLAROID' CORP. 23 July; 1968 [24 July, 1967], No. 1734/71 Divided out of 1,243,045. Heading C4P. [Also in Division C2] Mono-azo, dis-azo or anthraquinone dyes for photographic transfer processes are-of formula wherein A represents the atoms necessary to complete a benzene or naphthalene radical that may be further substituted; D is a monoazo, disazo or anthraquinone colour providing moiety, Z is hydrogen, chloro, bromo, carboxy sulpho, hydroxy, alkoxy, hydroxyalkyl, or an aromatic amino radical unsubstituted ortho to said amino group; Y is the residue'of an acid group forming an amide with and reducing the basic character of the nitrogen atom to which it is bonded; X is hydroxy; or when Z is an anilino or naphthylamino radical containing, a y-amino or p-hydroxy substituent but unsubstituted ortho to said amino group joined to the ring completed by A, X may also be hydrogen or a primary, secondary or tertiary amino group or an alkyl, aromatic or heterpcyclic substituent; R 1 is hydrogen, alkyl, cycloalkyl or substituted alkyl, and wherein the values of A, X, Z and R 1 are such that the compound is non-diffusible in alkaline photographic processing solution. The examples describe (1) reacting (2- hydroxy - 4 - amine-HCl - 5 - chloro - 4 1 - carbon-dodecylamide) diphenyl and 4- (2-naphthol- 1 - azo) benzene sulphonyl chloride (A) to form a dye of Formula (I) (2) reacting N'-(o-aminophenyl)-4-methoxy-3- (N 1 ,-dodecylamidoethyl) aniline (B) and sulphonyl chloride (A) to form a dye of Formula (XIX) (3) repeating (2) but using an octadecamido compound to form a dye of Formula (XX) (4) reacting diazotized sulphanilic and 1-phenyl- 3. - carbethoxy - pyrazolone - 5 to form 1- phenyl - 3 - carbethoxy - 4 - (p -,'ulphophenylaze)- pyrazolone-5 sodium salt which,is reacted with propylamine to form the corresponding 3-propylamido compound which is reacted with thionyl chloride to form the corresponding pchlorosulphonylphenylazo compound which is reacted with compound (B) to form a methoxy compound which is demethylated with BBr 3 to form a due of Formula (XXI) (5) 2 - amino - 4 - stearylamide. - N - (41.- methoxy - 3 1 - carboxyphenyl) aniline is reacted with 4 1 - (sulphonylchloride) - phenylazo - 2 - naphthol to form a methoxy compound which is demethylated to a dye of Formula (XVI).

    Galvanic cell
    16.
    发明授权
    Galvanic cell 失效
    电镀电池

    公开(公告)号：US3885990A

    公开(公告)日：1975-05-27

    申请号：US41451173

    申请日：1973-11-09

    Applicant: POLAROID CORP

    Inventor： BLOOM STANLEY M ,  HOFFMAN ARNOLD

    IPC: H01M6/04 ,  H01M10/02 ,  H01M17/00

    CPC classification number: H01M6/04 ,  H01M10/02

    Abstract: A galvanic cell having a zinc anode which includes a source of mercury ion which will provide a relatively continuous source of said ion over an extended period of time for amalgamation with the zinc anode.

    Abstract translation: 具有锌阳极的电池，其包括汞离子源，其将在延长的时间段内提供相对连续的所述离子源以与锌阳极并联。

    Silver image stabilization with noble metal compounds
    18.
    发明授权
    Silver image stabilization with noble metal compounds 失效
    银色图像稳定与金属化合物

    公开(公告)号：US3704126A

    公开(公告)日：1972-11-28

    申请号：US3704126D

    申请日：1970-12-07

    Applicant: POLAROID CORP

    Inventor： LAND EDWIN H ,  BLOOM STANLEY M ,  FARNEY LEONARD C

    IPC: G03C8/00 ,  G03C8/06 ,  G03C5/54

    CPC classification number: G03C8/06 ,  G03C8/00

    Abstract: THE PRESENT INVENTION RELATES TO A PHOTOGRAPHIC SILVER DIFFUSION TRANSFER PROCESS WHICH COMPRISES, IN ESSENCE, EXPOSING A SILVER DIFFUSION TRANSFER FILM UNIT WHICH COMPRISES PHOTOSENSITIVE SILVER HALIDE AND SILVER PRECIPITATING NUCLEI; CONTACTING THE EXPOSED FILM UNIT WITH A PROCESSING COMPOSITION WHICH COMPRISES A SILVER HALIDE DEVELOPING AGENT AND A SILVER HALIDE SOLVENT TO PROVIDE A VISIBLE SILVER IMAGE TO THE UNIT, AS A FUNCTION OF EXPOSURE; AND COACTING THE SILVER IMAGE WITH A NOBLE BELOW SILVER IN THE ELECTROMOTIVE FORCE SERIES OF ELEMENTS AT A CONCENTRATION EFFECTIVE TO ENHANCE STABILITY OF A SILVER IMAGE PROVIDED BY DIFFUSION TRANSFER PROCESSING OF THE FILM UNIT.

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