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    Solid propellant containing ferrocenyl phosphine derivatives
    11.
    发明授权
    Solid propellant containing ferrocenyl phosphine derivatives 失效
    含有二茂铁基膦衍生物的固体推进剂

    公开(公告)号：US6039819A

    公开(公告)日：2000-03-21

    申请号：US354709

    申请日：1982-03-04

    Applicant: Charles E. Harrod ,  William D. Stephens

    Inventor： Charles E. Harrod ,  William D. Stephens

    IPC: C06B23/00 ,  C06B45/10

    CPC classification number: C06B23/007

    Abstract: A solid propellant composition comprising an organic polymer fuel binder, an inorganic perchlorate oxidizer salt, ferrocenyl phosphine or phosphine oxide derivatives and in particular, triferrocenyl phosphine oxide, which function as stable solid combustion modifiers.

    Abstract translation: 一种固体推进剂组合物，其包含有机聚合物燃料粘合剂，无机高氯酸盐氧化剂盐，二茂铁基膦或氧化膦衍生物，特别是作为稳定的固体燃烧改性剂的三茂铁基氧化膦。

    Mold release composition with polybutadiene and method of coating a mold core
    12.
    发明授权
    Mold release composition with polybutadiene and method of coating a mold core 失效
    具有聚丁二烯的脱模组合物和涂覆模芯的方法

    公开(公告)号：US5601641A

    公开(公告)日：1997-02-11

    申请号：US573000

    申请日：1995-12-15

    Applicant: William D. Stephens

    Inventor： William D. Stephens

    IPC: B29C33/64 ,  C09D183/04 ,  C09D109/00 ,  C08L9/00 ,  C09D4/00 ,  C09D109/10

    CPC classification number: B29C33/64 ,  C09D183/04 ,  B29K2083/00

    Abstract: An aqueous reaction mixture having a pH of 4.5 to 5.5 of a methyl terminated siloxane emulsified polymer, a methyl triethoxysilane, a mixture of nonyl and octyl phenol derivative surfactants, fluorinated alkyl ester surfactant and synthetic ethoxylated amine surfactants, a silanol terminated polydimethylsiloxane hydroxyl terminated polybutadiene and ethanol. The reaction mixture is coated on a mold core surface and cured with heat to form a mold release surface that can be used in excess of twelve times prior to recoating.

    Abstract translation: 甲基封端的硅氧烷乳化聚合物，甲基三乙氧基硅烷，壬基和辛基酚衍生物表面活性剂的混合物，氟化烷基酯表面活性剂和合成乙氧基化胺表面活性剂的pH为4.5至5.5的水性反应混合物，硅烷醇封端的聚二甲基硅氧烷羟基封端的聚丁二烯 和乙醇。 将反应混合物涂覆在模芯表面上并用热固化以形成脱模表面，其可在重涂之前使用超过十二次。

    Mold release composition and method of coating a mold core
    13.
    发明授权
    Mold release composition and method of coating a mold core 失效
    脱模组合物和涂覆模芯的方法

    公开(公告)号：US5219925A

    公开(公告)日：1993-06-15

    申请号：US917772

    申请日：1992-07-21

    Applicant: William D. Stephens

    Inventor： William D. Stephens

    IPC: B29C33/64 ,  C09D183/04

    CPC classification number: B29C33/64 ,  C09D183/04

    Abstract: An aqueous reaction mixture of a multi-functional polydimethyl siloxane emulsified polymer, a methyl triethoxy silane, a mixture of substituted nonyl or octyl phenol derivative surfactants and synthetic ethoxylated amine surfactants, and ethanol. The reaction mixture is coated on a mold core surface and cured with heat to form a mold release surface that can be used in excess of twenty times prior to recoating.

    Abstract translation: 多官能聚二甲基硅氧烷乳化聚合物，甲基三乙氧基硅烷，取代的壬基或辛基苯酚衍生物表面活性剂的混合物和合成的乙氧基化胺表面活性剂的水性反应混合物和乙醇。 将反应混合物涂覆在模芯表面上并用热固化以形成脱模表面，其可在重涂之前使用超过二十次。

    Mold release reaction product and method of coating of a mold core
    14.
    发明授权
    Mold release reaction product and method of coating of a mold core 失效
    脱模反应产物和模芯涂层方法

    公开(公告)号：US06322850B1

    公开(公告)日：2001-11-27

    申请号：US09556283

    申请日：2000-04-24

    Applicant: William D. Stephens ,  Patricia R. Bertolucci

    Inventor： William D. Stephens ,  Patricia R. Bertolucci

    IPC: B05D508

    CPC classification number: C09D4/00 ,  B29C33/60 ,  B29C33/64 ,  C09D183/04 ,  C08G77/04 ,  C08L2666/44

    Abstract: The reaction product is derived from a composition containing one of seven silanes; dimethyldiethoxysilane, methyldiethoxysilane, dimethyldimethoxysilane, diphenyldimethoxysilane, trimethylmethoxysilane, trimethylethoxysilane, or aminopropyltriethoxysilane, a multi-functional polydimethyl siloxane emulsified polymer, a compatible surfactant, ethanol and a majority component of water. In the method, the reaction product is applied to a heated surface of a mold core to create a semi-permanent coating to facilitate multiple releases of molded parts. If not heated, the mold core must be dried to remove water.

    Abstract translation: 反应产物衍生自含有七种硅烷之一的组合物; 二甲基二乙氧基硅烷，甲基二乙氧基硅烷，二甲基二甲氧基硅烷，二苯基二甲氧基硅烷，三甲基甲氧基硅烷，三甲基乙氧基硅烷或氨基丙基三乙氧基硅烷，多官能聚二甲基硅氧烷乳化聚合物，相容表面活性剂，乙醇和多数成分组分。 在该方法中，将反应产物施加到模芯的加热表面以产生半永久性涂层以促进模制部件的多次释放。 如果不加热，模芯必须干燥以除去水分。

    Solid fuel gas generator for ducted rocket engine
    15.
    发明授权
    Solid fuel gas generator for ducted rocket engine 失效
    用于管道火箭发动机的固体燃料气体发生器

    公开(公告)号：US06258188B1

    公开(公告)日：2001-07-10

    申请号：US09415708

    申请日：1999-10-12

    Applicant: Richard C. Hatcher ,  William D. Stephens ,  Robert L. Stanley

    Inventor： Richard C. Hatcher ,  William D. Stephens ,  Robert L. Stanley

    IPC: C06B4510

    CPC classification number: C06B45/105 ,  C06D5/00

    Abstract: In the development of new minimum signature ducted rocket technology, the U.S. Army MICOM Propulsion Directorate has conducted studies for the development of fuel-rich gas generators for ducted rockets. The propellant formulation goals of this study include increasing burning rate, pressure exponent, and combustion efficiency without significantly decreasing fuel value. Formulations described in this application contain an energetic nitramine-prepolymer, a range of curing agents, and zirconium hydride (ZrH2) fuel element and carbon (C) as an optional fuel element.

    Abstract translation: 在开发新的最小签名管道火箭技术时，美国陆军MICOM推进局已经开发研制用于管道火箭的富燃料气体发生器。 本研究的推进剂配方目标包括提高燃烧速率，压力指数和燃烧效率，而不会显着降低燃油价值。 在本申请中描述的制剂含有能量的硝胺预聚物，一系列固化剂和氢化锆（ZrH 2）燃料元件和碳（C）作为任选的燃料元件。

    Lightweight pyrotechnic compressor
    16.
    发明授权
    Lightweight pyrotechnic compressor 失效
    轻型烟火压缩机

    公开(公告)号：US5511481A

    公开(公告)日：1996-04-30

    申请号：US380171

    申请日：1995-01-23

    Applicant: William D. Stephens

    Inventor： William D. Stephens

    IPC: C06D5/00 ,  F42B3/00 ,  F42B3/04 ,  F42B5/02

    CPC classification number: F42B3/006 ,  C06D5/00 ,  F42B3/04

    Abstract: A breech assembly similar to a modified shotgun breech is used to fire gaus combustion products from a shotgun type pyrotechnic cartridge into a tank that holds the compressed gas. This compressed gas can then be used to drive power tools, inflation assemblies or any device which normally operates on compressed air.

    Abstract translation: 使用类似于改进的霰弹枪后膛的后膛组件将气体燃烧产物从霰弹枪型烟火药筒射入容纳压缩气体的罐中。 然后，该压缩气体可用于驱动动力工具，充气组件或通常在压缩空气上操作的任何装置。

    High burn rate ammonium perchlorate propellant
    17.
    依法登记的发明
    High burn rate ammonium perchlorate propellant 失效
    高燃烧率高氯酸铵推进剂

    公开(公告)号：USH717H

    公开(公告)日：1989-12-05

    申请号：US243539

    申请日：1988-09-12

    Applicant: William D. Stephens ,  Larry C. Warren

    Inventor： William D. Stephens ,  Larry C. Warren

    IPC: C06B23/00 ,  C06B45/10

    CPC classification number: C06B23/007 ,  C06B45/10

    Abstract: A solid propellant composition employing 2,2-bis(t-butyldicyclopentadienyon)propane (TBD) as the burn rate enhancer in a weight percent from about 2 to about 6 weight percent yields higher threshold values for ignition by impact and improved friction and spark testing values to thereby render the solid propellant composition less hazardous to personnel during handling as compared to similar solid propellant compositions containing Catocene, (2,2-bis(ethyldicylopentadienyliron)propane). The TBD solid propellant composition also comprises from about 9 to about 10 weight percent of hydroxyterminated polybutadiene binder system including an isocyanate curative added in amount of up to 1.0 weight percent and optional modifiers in small amounts with adjustment of the weight percent of other ingredients. Other propellant ingredients comprise a trimodal mix of 200, 1.7, and 0.7 micron particle sizes of ammonium perchlorate oxidizer in amounts from about 66 to about 70 weight percent, and aluminum metal powder in amounts from about 18 to about 20 weight percent. TBD is synthesized to contain no alpha hydrogens, i.e., does not have hydrogens on carbon adjacent to the aromatic ring structure which contributes to long term oxidation and migration problems of Hycat 6D and Catocene.

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