摘要:
A catalyst for synthesizing 1-hexene from ethylene trimerization and its application are provided. Said catalyst consists of (a) the compound containing P and N, (b) electron donor, (c) Cr compound, (d) carrier and (e) accelerator. The molar ratio of (a), (b), (c), (d) and (e) is 0.5-100:0.5-100:1:0.5-10:50-5000. The catalyst is prepared by mixing the components of (a)-(e) in an ethylene trimerization apparatus in situ and ethylene is introduced into the apparatus continuously. The prepared catalyst can be used to synthesize 1-hexene from ethylene trimerization in the inert solvents. The trimerization is performed at 30-150° C. and 0.5-10.0 MPa for 0.1-4 hours. The catalyst has high catalytic activity and high 1-hexene selectivity. During the process of ethylene trimerization, by-product polyethylene does not stick to the apparatus.
摘要:
A method for synthesis of 1-decene oligomer is provided, wherein 1-decene is polymerized at 80-120° C., 0.8-1.4 MPa in the presence of aluminum trichloride catalyst supported on gamma-alumina and n-hexane solvent where the volume ratio of 1-decene to n-hexane is 3:8-4:1. The catalyst is treated as follows: impregnating gamma-alumina carrier in 0.5-2.0 M of hydrochloric acid, sulfuric acid, nitric acid or mixtures thereof, then vacuum drying at 80-100° C. and calcining at 400-800° C.; dissolving 5-10 g of anhydrous aluminum trichloride in 100 ml of tetrachloromethane, trichloromethane or dichloromethane solvent; adding the obtained solution into 10-20 g of activated alumina carrier and obtaining the catalyst after vacuum drying. The conversion of 1-decene is 50 wt % or more. The oligomer has a kinematic viscosity at 40° C. of 6.0-25 mm2/s and a viscosity index of 160-262.
摘要:
A state retention power gated cell includes a logic cell arranged in two or more rows. The logic cell has an active layer including at least a first well and a second well disposed in first and second rows, respectively. In a normal operation mode, the first well is powered with a first bias voltage, the second well is powered with a second bias voltage, the first power supply line is powered with VDDC, and the second power supply line is powered with VDD. In a standby mode, the first well preferably is powered down, the second well is powered with the second bias voltage, the first power supply line is powered with VDDC, and the second power supply line is powered down.
摘要:
An oscillator circuit includes a charge current source and first and second muxes. The first mux has a common node, a discharge node, a control node and a charge node coupled to the charge current source. The control node couples the common node to either the discharge or charge nodes. The second mux has a shared node, a reference node, a control node and a ground node coupled to ground. The second mux control node couples the shared node to either the reference or ground nodes. A capacitor is coupled between the common node and the shared node. A comparator has a non-inverting input coupled to the common node, an inverting input coupled to the reference node, and an output coupled to the first and second control nodes. A discharge current sink couples the discharge node to ground and an oscillator output is provided by the comparator.
摘要:
The present disclosure provides a microscopic vision measurement method based on the adaptive positioning of the camera coordinate frame which includes: calibrating parameters of a microscopic stereo vision measurement model (201); acquiring pairs of synchronical images and transmitting the acquired images to a computer through an image acquisition card (202); calculating 3D coordinates of feature points in a scene according to the matched pairs of feature points in the scene obtained from the synchronical images and the calibrated parameters of the microscopic stereo vision measurement model (203); and performing specific measurement according to the 3D coordinates of the feature points in the scene (204). With the method, the nonlinearity of the objective function in the microscopic vision calibration optimization is effectively decreased and a better calibration result is obtained.
摘要:
A method for synthesis of 1-decene oligomer is provided, wherein 1-decene is polymerized at 80-120° C., 0.8-1.4 MPa in the presence of aluminum trichloride catalyst supported on gamma-alumina and n-hexane solvent where the volume ratio of 1-decene to n-hexane is 3:8-4:1. The catalyst is treated as follows: impregnating gamma-alumina carrier in 0.5-2.0 mol of hydrochloric acid, sulfuric acid, nitric acid or mixtures thereof, then vacuum drying at 80-100° C. and calcining at 400-800° C.; dissolving 5-10 g of anhydrous aluminum trichloride in 100 ml of tetrachloromethane, trichloromethane or dichloromethane solvent; adding the obtained solution into 10-20 g of activated alumina carrier and obtaining the catalyst after vacuum drying. The conversion rate of 1-decene is 50 wt % or more. The oligomer has a kinematic viscosity at 40° C. of 6.0-25 mm2/s and a viscosity index of 160-262.
摘要:
Embodiments of the present invention address deficiencies of the art in respect to SOA systems migration and provide a method, system and computer program product for SOA lifecycle model migration. In one embodiment of the invention, a method for migrating a process model in a monolithic application to an SOA lifecycle model in an SOA based system can be provided. The method can include selecting process steps implemented by code assets in a code base for the monolithic application, mapping the selected process steps to corresponding ones of the code assets, and determining entry and exit points in the code assets for establishing callbacks into services defining the SOA based system. Thereafter, callbacks to the determined entry and exit points can be established and the services can be deployed.