公开(公告)号：US20210037818A1

公开(公告)日：2021-02-11

申请号：US16947585

申请日：2020-08-07

Applicant: ECOLAB USA INC.

Inventor： Ashish Dhawan ,  Junzhong Li ,  David D. McSherry ,  Carter M. Silvernail ,  Chris Nagel

IPC: A01N25/22 ,  C07C407/00 ,  A01N37/16 ,  C08F8/30 ,  A01N59/00

Abstract: Stabilized peroxycarboxylic acid compositions and the solid supported peracid stabilizers are provided. Methods of producing the solid supported peracid stabilizers are provided. The solid supported peracid stabilizers and the stable peroxycarboxylic acid compositions are particularly suitable for use in sanitizing equipment and surfaces to reduce yeasts, spores and bacteria, including those having contact with food, food products and/or components thereof, which require or benefit from infection control suitable for direct contact with such food sources.

公开(公告)号：US10555523B2

公开(公告)日：2020-02-11

申请号：US16353355

申请日：2019-03-14

Applicant: ECOLAB USA INC

Inventor： David D. McSherry ,  Junzhong Li ,  Richard K. Staub

IPC: A01N37/16 ,  C12Q1/18 ,  A01N25/02 ,  C12Q1/22 ,  C12Q1/28

Abstract: Self-indicating chemistries are provided for visual detection by a user of efficacious levels of peroxycarboxylic acid concentrations in a solution produced in situ. The self-indicating chemistries include a combination of dyes providing a visual color indication, such as a tri-color indicator system, such as a yellow, green, and red color system indicating in situ threshold levels of peroxycarboxylic acid concentrations in a solution employing the self-indicating chemistry. Systems, kits and compositions for a quantitative assessment of an in situ perhydrolysis reaction to generate peroxycarboxylic acids are provided. Methods of use are further provided.

公开(公告)号：US20200029560A1

公开(公告)日：2020-01-30

申请号：US16590478

申请日：2019-10-02

Applicant: ECOLAB USA INC.

Inventor： Junzhong Li ,  David D. McSherry ,  Richard Staub

IPC: A01N37/16 ,  A01N37/12 ,  C07C409/24

Abstract: The present disclosure is related to percarboxylic acid compositions formed in situ in non-equilibrium reactions. The peroxycarboxylic acid compositions are formed using ester based starting materials. Methods for using the percarboxylic acid compositions are also disclosed.

公开(公告)号：US10017403B2

公开(公告)日：2018-07-10

申请号：US13798311

申请日：2013-03-13

Applicant: ECOLAB USA INC.

Inventor： Victor Keasler ,  Renato De Paula ,  Junzhong Li ,  David D. McSherry ,  Brandon Herdt ,  Richard Staub

IPC: A01N25/22 ,  A01N25/32 ,  A01N37/16 ,  C02F1/50 ,  C02F1/70 ,  C02F1/72 ,  C02F3/34 ,  C09K8/60 ,  C09K8/66 ,  E21B21/06 ,  E21B43/00 ,  C02F1/76 ,  C02F103/08 ,  C02F103/10 ,  C02F103/36

CPC classification number: C02F1/70 ,  A01N25/22 ,  A01N25/32 ,  A01N37/16 ,  C02F1/50 ,  C02F1/722 ,  C02F1/76 ,  C02F3/342 ,  C02F2103/08 ,  C02F2103/10 ,  C02F2103/365 ,  C02F2303/04 ,  C02F2303/08 ,  C02F2303/18 ,  C02F2303/20 ,  C02F2305/02 ,  C09K8/605 ,  C09K8/66 ,  C09K2208/28 ,  C09K2208/32 ,  E21B21/068 ,  E21B43/00 ,  Y02W10/37 ,  A01N59/00

Abstract: Compositions and methods for the use of peracid compositions having low to substantially no hydrogen peroxide for various water treatments, including oil- and gas-field operations, and/or other aseptic treatments are disclosed. In numerous aspects, peracetic acid is the preferred peracid and is treated with a peroxide-reducing agent to substantially reduce the hydrogen peroxide content. Methods for using the treated peracid compositions for treatment of drilling fluids, frac fluids, flow back waters and disposal waters are also disclosed for improving water condition, reducing oxidizing damage associated with hydrogen peroxide and/or reducing bacteria infestation.

公开(公告)号：US10010075B2

公开(公告)日：2018-07-03

申请号：US14562960

申请日：2014-12-08

Applicant: Ecolab USA Inc.

Inventor： Brandon Herdt ,  Richard Staub ,  Thomas C. Rustad ,  Junzhong Li ,  David D. McSherry ,  Paul R. Kraus ,  Richard Walsh

IPC: B05C3/00 ,  B08B3/04 ,  A01N37/16 ,  C02F1/50 ,  C07C407/00 ,  A01N59/00 ,  B01J19/00 ,  B01J4/00 ,  A61L2/24 ,  C07C409/24 ,  A61L2/18 ,  B01J19/24 ,  B01J14/00 ,  C02F1/72 ,  C02F103/08

CPC classification number: A01N37/16 ,  A01N37/02 ,  A01N59/00 ,  A61L2/18 ,  A61L2/186 ,  A61L2/24 ,  A61L2202/14 ,  B01J4/001 ,  B01J4/008 ,  B01J14/00 ,  B01J19/0006 ,  B01J19/0013 ,  B01J19/24 ,  B01J2219/00049 ,  B01J2219/00121 ,  B01J2219/00159 ,  B01J2219/24 ,  C02F1/50 ,  C02F1/722 ,  C02F2103/08 ,  C07C407/00 ,  C07C409/24 ,  A01N2300/00

Abstract: Methods and systems for temperature-controlled, on-site generation of peracids, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions are disclosed. In particular, methods for using an adjustable biocide formulator or generator system overcome the limitations of temperature on the kinetics of the peracid generation and/or peracid decomposition inside an adjustable biocide formulator or generator system. The methods include the controlling of the temperature of at least one raw starting material, namely water, to improve upon methods of on-site generation of peracids. The methods allow for the generation of user-selected chemistry without regard to the ambient temperatures of the raw starting materials and/or the biocide formulator or generator system.

公开(公告)号：US20170339952A1

公开(公告)日：2017-11-30

申请号：US15678756

申请日：2017-08-16

Applicant: ECOLAB USA INC.

Inventor： Junzhong Li ,  David D. McSherry ,  Richard Staub

IPC: A01N37/16 ,  C07C409/24 ,  A01N37/12

CPC classification number: A01N37/16 ,  A01N37/12 ,  C07C409/24 ,  A01N31/02 ,  A01N2300/00 ,  A01N59/00

Abstract: The present disclosure is related to percarboxylic acid compositions formed in situ in non-equilibrium reactions. The peroxycarboxylic acid compositions are formed using ester based starting materials. Methods for using the percarboxylic acid compositions are also disclosed.

公开(公告)号：US09763442B2

公开(公告)日：2017-09-19

申请号：US14497427

申请日：2014-09-26

Applicant: Ecolab USA Inc.

Inventor： Junzhong Li ,  David D. McSherry ,  Richard Staub

IPC: A01N37/16 ,  A01N37/12 ,  C07C409/24 ,  C07C69/30

CPC classification number: A01N37/16 ,  A01N37/12 ,  C07C409/24 ,  A01N31/02 ,  A01N2300/00 ,  A01N59/00

Abstract: The present disclosure is related to percarboxylic acid compositions formed in situ in non-equilibrium reactions. The peroxycarboxylic acid compositions are formed using ester based starting materials. Methods for using the percarboxylic acid compositions are also disclosed.

公开(公告)号：US09675076B2

公开(公告)日：2017-06-13

申请号：US15413582

申请日：2017-01-24

Applicant: Ecolab USA Inc.

Inventor： Junzhong Li ,  David D. McSherry ,  Allison Brewster ,  Richard Staub

IPC: A01N59/00 ,  A01N37/02 ,  A01N37/16 ,  G01N21/64

CPC classification number: G01N21/6486 ,  A01N25/16 ,  A01N37/02 ,  A01N37/16 ,  A01N41/04 ,  A01N59/00 ,  A01N59/02 ,  G01N21/01 ,  G01N21/64 ,  G01N21/643 ,  G01N2021/6439 ,  Y10T436/206664

Abstract: Peracid stable fluorescent active compounds in highly acidic, equilibrium peroxycarboxylic acid sanitizing compositions are disclosed as having improved fluorescent stability allowing for monitoring of peroxycarboxylic acid concentration by conductivity and/or optical sensors. Beneficially, the compositions are also low odor and low/no VOC dual functioning acid wash and sanitizing compositions.

公开(公告)号：US20170064949A1

公开(公告)日：2017-03-09

申请号：US15254559

申请日：2016-09-01

Applicant: Ecolab USA Inc.

Inventor： Paul R. Kraus ,  Benjamin Crew ,  Junzhong Li ,  David D. McSherry ,  Ramakrishnan Balasubramanian ,  Richard Staub ,  Ariel Chatman Kleczewski ,  Minh Tran ,  Catherine Hanson ,  Irwan Yunus ,  Jeffery D. Breshears ,  Brian Paul Brunner

IPC: A01N37/36 ,  B01J19/24 ,  A23L3/3499 ,  C07C51/367

CPC classification number: A01N37/36 ,  A01N37/16 ,  A23L3/3463 ,  A23L3/3481 ,  A23L3/3499 ,  A23V2002/00 ,  B01J19/1812 ,  B01J19/1818 ,  B01J19/2415 ,  B01J2219/00051 ,  B01J2219/00094 ,  B01J2219/00132 ,  B01J2219/00144 ,  C07C51/367 ,  C07C407/00 ,  Y02W10/37 ,  C07C409/24

Abstract: Methods of generating performic acid by contacting aqueous oxidizing agent and aqueous formic acid source in liquid phase are disclosed. A system and apparatus for the in situ production of the performic acid chemistries is further disclosed. In particular, a continuous flow reactor is provided to generate performic acid at variable rates. Methods of employing the oxidizing biocide for various disinfection applications are also disclosed.

Abstract translation: 公开了通过使水相氧化剂和甲酸水溶液与液相中的水相接触来生成甲酸的方法。 进一步公开了用于原位生产甲酸化学物质的系统和设备。 特别地，提供连续流动反应器以以可变速率产生表酸。 还公开了将氧化杀生物剂用于各种消毒应用的方法。

公开(公告)号：US09540598B2

公开(公告)日：2017-01-10

申请号：US14482256

申请日：2014-09-10

Applicant: Ecolab USA Inc.

Inventor： David W. Gohl ,  Robert D. P. Hei ,  Thomas Merz ,  Peter Jens Forth ,  Matthias Kreysel ,  David D. McSherry ,  Junzhong Li ,  Jonathan P. Fast

IPC: A61K31/19 ,  C07D303/34 ,  A01N37/00 ,  C11D3/395 ,  A01N41/04 ,  A01N41/08 ,  A23B4/20 ,  A23B5/14 ,  A23L3/3535 ,  C07D303/16 ,  C11D3/20 ,  C11D3/28 ,  C11D3/33 ,  C11D3/36 ,  C11D3/39 ,  C11D3/48 ,  C11D11/00 ,  C07C409/42

CPC classification number: C11D3/3945 ,  A01N41/04 ,  A01N41/08 ,  A23B4/20 ,  A23B5/14 ,  A23L3/3535 ,  A23V2002/00 ,  C07C409/42 ,  C07D303/16 ,  C11D3/2075 ,  C11D3/2079 ,  C11D3/28 ,  C11D3/33 ,  C11D3/34 ,  C11D3/364 ,  C11D3/3947 ,  C11D3/3955 ,  C11D3/48 ,  C11D11/0017 ,  A01N37/16 ,  A01N59/00 ,  A01N2300/00

Abstract: The present invention relates to novel combined laundry detergent, bleach, and antimicrobial composition incorporating novel sulfoperoxycarboxylic acid compounds, and methods for making and using them. The sulfoperoxycarboxylic compounds used in compositions of the invention are storage stable, water soluble and have low to no odor. Compositions of the invention may be in the form of a liquid, a solid, or a gel. The sulfoperoxycarboxylic compounds useful in preparing compositions of the present invention can be formed from non-petroleum based renewable materials.

Abstract translation: 本发明涉及新型组合洗衣洗涤剂，漂白剂和结合新的磺基过氧羧酸化合物的抗微生物组合物，以及制备和使用它们的方法。 本发明组合物中使用的磺基过氧羧酸化合物是储存稳定的，水溶性的，具有低至无气味。 本发明的组合物可以是液体，固体或凝胶的形式。 可用于制备本发明组合物的磺基过氧化羧酸化合物可由非石油基可再生材料形成。