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    N-(2-pyrrolidinonyl) methyl carbamate derivatives
    24.
    发明授权
    N-(2-pyrrolidinonyl) methyl carbamate derivatives 失效
    N-（2-吡咯烷酮基）甲基氨基甲酸酯衍生物

    公开(公告)号：US3903110A

    公开(公告)日：1975-09-02

    申请号：US24802172

    申请日：1972-04-27

    Applicant: GAF CORP

    Inventor： FREYERMUTH HARLAN BENJAMIN ,  RANDALL DAVID I

    IPC: C07D207/26 ,  C07D207/27 ,  C07D27/08

    CPC classification number: C07D207/27

    Abstract: Compounds having the formula

    D R A W I N G
    wherein n is 1 or 2 and R is a monovalent or divalent aliphatic, alicyclic or aryl radical produced by the reaction of n moles of an isocyanate or diisocynate with n moles of N-hydroxymethyl-2pyrrolidinone and uses thereof.

    Abstract translation: 具有式ORH PARALLEL | -CH2-OCN-R的化合物，其中n为1或2，R为通过n摩尔异氰酸酯或二异氰酸酯与n摩尔N反应产生的一价或二价脂族，脂环族或芳基 - 羟甲基-2-吡咯烷酮及其用途。

    Cyclic diamides of 2-chloroethyl phosphonic acid
    25.
    发明授权
    Cyclic diamides of 2-chloroethyl phosphonic acid 失效
    2-氯乙基膦酸的环状二酰胺

    公开(公告)号：US3875157A

    公开(公告)日：1975-04-01

    申请号：US18489971

    申请日：1971-09-29

    Applicant: GAF CORP

    Inventor： RANDALL DAVID I ,  WYNN ROBERT W

    IPC: C07F9/44 ,  C07D87/38

    CPC classification number: C07F9/44

    Abstract: Plant growth regulating compounds are substituted 2chloroethylphosphonic diamides of the formula:

    WHEREIN R1 is cycloalkyl, R2 is hydrogen or cycloalkyl or R1 and R2 together form a heterocyclic ring such as morpholine, piperidine or pyrrolidine. They are prepared by the reaction of 2-chloroethylphosphonic dihalide with the appropriate amine or by the reaction of excess amine with a 2-chloroethyl dichlorophosphite followed by rearrangement of the chloroethyl ester intermediate.

    Abstract translation: 植物生长调节化合物是下式的取代的2-氯乙基膦酸二酰胺：

    2-Chloroethyl-phosphonothioic esters and thioesters
    26.
    发明授权
    2-Chloroethyl-phosphonothioic esters and thioesters 失效
    2-氯乙基 - 膦酰硫酸酯和硫酯

    公开(公告)号：US3870772A

    公开(公告)日：1975-03-11

    申请号：US29136572

    申请日：1972-09-22

    Applicant: GAF CORP

    Inventor： RANDALL DAVID I ,  WYNN ROBERT W

    IPC: C07F9/38 ,  C07F9/42 ,  C07F9/44 ,  C07F9/40 ,  A01N9/36

    CPC classification number: C07F9/3808 ,  C07F9/42 ,  C07F9/4407

    Abstract: Compounds of the following formula:

    WHEREIN X is oxygen or sulfur and R is hydrogen, alkyl, aryl, alkaryl or aralkyl, are useful as plant growth regulators when administered to plants in association with a carrier. The compounds are prepared by reaction of the 2-chloroethylphosphonic acid chloride with phosphorus pentasulfide to form 2chloroethylphosphonothioic acid chloride and reaction of this material with water to form the acid, hydrogen sulfide to form the trithioic acid, and reaction with an alcohol or thioalcohol to form the esters.

    Abstract translation: 下式的化合物：

    Halohydroxyacrylamides and process for making same
    28.
    发明授权
    Halohydroxyacrylamides and process for making same 失效
    羟基甲基丙烯酸酰胺和其制备方法

    公开(公告)号：US3646141A

    公开(公告)日：1972-02-29

    申请号：US3646141D

    申请日：1969-09-18

    Applicant: GAF CORP

    Inventor： RANDALL DAVID I

    IPC: C07C233/02 ,  C07C103/58

    CPC classification number: C07C233/02

    Abstract: THE COMPOUNDS ARE OF THE CLASS OF 2-HALO-3-HYDROXYACRYLAMIDES, A SPECIES BEING 2,3'',4''-TRICHLORO-3-HYDROXYACRYLANILIDE, USEFUL AS HERBICIDES, FUNGICIDES, CORROSION INHIBITORS, ANTIOXIDANTS AND ADDITIVES FOR LUBE OILS.

    O-catechol o-hydrocarbyl-vinyl phosphonates and process for making same
    29.
    发明授权
    O-catechol o-hydrocarbyl-vinyl phosphonates and process for making same 失效
    O-CATECHOL O-烃基苯乙酸酯及其制备方法

    公开(公告)号：US3562363A

    公开(公告)日：1971-02-09

    申请号：US3562363D

    申请日：1967-03-22

    Applicant: GAF CORP

    Inventor： RANDALL DAVID I

    IPC: C07F9/40 ,  C07F9/6571 ,  C23F11/167 ,  D06M13/313 ,  A01N9/36

    CPC classification number: D06M13/313 ,  C07F9/4015 ,  C07F9/4084 ,  C07F9/657181 ,  C10M1/08 ,  C10M2223/065 ,  C23F11/1676

    Abstract: THE COMPOUNDS ARE ESTERS AND HALF ESTERS OF VINYLPHOSPHONIC ACID REPRESENTEDBY THE FOLLOWING STRUCTURAL FORMULA:

    2-(CH2=CH-P(=O)(-O-R5)-O-),3-R1,4-R2,5-R3,6-R4-PHENOL
    WHEREIN R1-R4 ARE EITHER HYDROGEN, ALKYL, ALKOXY, OR HALO AND TWO OF THE SUBSTITUENT GROUPS MAY FORM A CONDENSED RING AND R5 IS EITHER HYDROGEN, AN AROMATIC, A CYCLOALIPHATIC, OR AN ALIPHATIC GROUP, WHEREIN THE CARBON ATOM LINKED TO THE OXYGEN IS NOT TERTIARY. THE COMPOUNDS POSSESS PLANT GROWTH REGULATING PROPERTIES, E.G., CONTROL OF APICAL DOMINANCE, AND MAY ALSO BE EMPLOYED AS MONOMERS FOR THE PROUCTION OF POLYMERS. THE COMPOUNDS ARE PRODUCED FROM THE CATECHOL AND SUBSTITUTED CATECHOL CYCLIC ESTERS OF VINYLPHOSPHONIC ACID, WITH THE HALF ESTERS BEING PRODUCED BY HYDROLYSIS OF THE CYCLIC ESTER AND THE ESTERS BEING PRODUCED BY TRANSESTERIFICATION OF THE CYCLIC ESTER WITH A SUITABLE ALCOHOL.

    Anthraquinone dyestuffs
    30.
    发明授权
    Anthraquinone dyestuffs 失效

    公开(公告)号：US3497527A

    公开(公告)日：1970-02-24

    申请号：US3497527D

    申请日：1966-12-05

    Applicant: GAF CORP

    Inventor： RANDALL DAVID I ,  FREYERMUTH HARLAN B

    IPC: C09B1/32 ,  C09B1/514 ,  C09B1/54 ,  C09B1/50

    CPC classification number: C09B1/547 ,  C09B1/32 ,  C09B1/503 ,  C09B1/5145

    Abstract: 1,200,339. Anthraquinone dyestuffs. GAF CORP. 4 Dec., 1967 [5 Dec., 1966], No. 54961/67. Heading C4P. The invention comprises anthraquinone dyestuffs of general formula wherein X is -NHR or OH, R is H, C 1 -C 4 alkyl, Y is H, C 1 -C 4 alkoxy or halogen, and Z is H, hydroxy or -NHR with the proviso that at least one of Y and Z is the grouping wherein B is -O- or -NH-, R 1 is H, C 1 -C 4 alkyl or C 1 -C 4 alkoxy and R 2 represents the carbon atoms necessary to complete a 5- to 7- membered heterocycle of the lactam series, e.g. a pyrrolidinone, piperidone or e-caprolactam ring. They are prepared by reacting the corresponding anthraquinone compound with an N-methylol lactam at 15‹ to 60‹ C. in an acid medium, e.g. sulphuric acid. The dyes give reddish blue and cerise shades on polyester, polyamide or cellulose.

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