摘要:
A process and apparatus for conditioning crude copper phthalocyanine pigment prepared in a solvent-free process which comprises kneading at a shear gradient of 300-20,000 sec..sup.-1 for 10 seconds to 15 minutes and with an energy comsumption of 0.4-50 KWH/Kg. of copper phthalocyanine, a mixture of1. 1.0 part crude copper phthalocyanine which has not previously been subjected to extractive boiling;2. 0.1-20 parts of a salt which is soluble in water or in aqueous acids or bases; and3. 0.3-5 parts of an organic or inorganic solvent or mixture thereof which does not have significant amounts of the pigment or the salt.
摘要翻译:用于调节在无溶剂方法中制备的粗铜酞菁颜料的方法和装置,其包括以300-20,000秒-1的剪切梯度捏合10秒至15分钟,并且能量消耗为0.4-50KWH / Kg 。 的铜酞菁,1.0的混合物部分原料铜酞菁,其以前未被提供给提取的沸腾; 2. 0.1-20份在水中或水中或酸中溶解的盐的部分; 和3. 0.3-5有机或无机溶剂或其混合物的部件,其中没有颜料或盐的重要组成部分。
摘要:
The conversion of the .alpha.-modification of the tetrabrom-8,8'-dihydroxynaphthazine into the .beta.-modification and the conditioning to a deeply colored, easily dispersible pigment can be performed in one process step by a salt kneading process in the presence of an inorganic or organic salt which is soluble in water or in aqueous acids or bases, of an organic solvent which does not significantly dissolve either the salt or the pigment and of an aromatic solvent.
摘要:
Mixed crystals of dyestuffs of the formula I ##STR1## wherein R denotes alkyl andn denotes a number from 2 to 4, and dyestuffs of the formula II ##STR2## wherein R.sub.1, R.sub.2 and R.sub.3 denote alkyl, with a characteristic X-ray diffraction diagram are distinguished by a high tinctorial strength and liquor stability when they are used for dyeing polyester fibres.
摘要:
Chemical reaction products, obtained in an alkaline medium and which require the addition of a dispersing agent, are neutralized by addition of a free surface-active acid to which, after its preparation, basic agents have not been added or have only been added up to a pH value of 3.
摘要:
The chemical yield and the space-time yield of copper phthalocyanine obtained according to the "baking process" is improved if urea and phthalic anhydride, or its reaction products with ammonia, or the dehydration products thereof, are fed in the liquid form to the reaction vessel.
摘要:
Sifting is improved by the installation of one or more nozzles in the longitudinal axis of a drier. A spray-dried granulate is thereby substantially freed from dust. The effect of heat on low melting products is reduced by cooling the gas.
摘要:
The production of copper phthalocyanine in accordance with German Offenlegungsschrift No. 2,432,564 is improved by the process which is characterized in that the reaction product formed at 130.degree.-300.degree. C from optionally substituted phthalic anhydride, reaction products of optionally substituted phthalic anhydride with ammonia, or the dehydration products thereof, urea and, optionally, a catalyst is reacted with a copper salt and, optionally, a catalyst at temperatures of 150.degree.-350.degree. C and preferably 170.degree.-300.degree. C with the proviso that the catalyst is added either during the preparation of the starting material or during the reaction with the copper salt.
摘要:
Pressing of uniform shape and uniform weight of disperse dyestuffs and optical brightening agents with a solubility in water less than 0.5% at 20.degree.C which are suitable for an automate metering step and which disintegrate in aqueous dye baths to give dispersions are manufactured by compressing the dyestuff or brightening agent, an anionic dispersing agent and a solid water-soluble mould release agent which gives a neutral to weakly alkaline reaction in water.
摘要:
Solid formulations of organic dyestuffs, or of optical brighteners, characterized in that they contain a mixture of(a) 70-90% by weight of a mineral oil,(b) 0.5-10% by weight of an amide of the formula ##STR1## in which R represents C.sub.10 -C.sub.22 -alkyl or -alkenyl,R.sub.1 represents H or C.sub.1 -C.sub.4 -alkyl, or the two R.sub.1 's together represent a 1,2-ethylene bridge andR.sub.2 represents ##STR2## alkylene, and R.sub.3 represents H, C.sub.1 -C.sub.6 -alkyl or phenyl,(c) 0.5-15% by weight of a non-ionic surface-active agent and(d) 0-8% by weight of a cationic or anionic surface-active agent,and processes for the production of low-dust and low-foam solid dyestuff formulations.
摘要:
Leather dyeing agents, which can be obtained by concentrating, by means of a membrane separation process, the mother liquors, which are produced in the salting-out process in the preparation of organic dyestuffs which are water-soluble or which contain groups imparting water-solubility, the mother liquors having an extinction in the absorption maximum which is .gtoreq.500, with a layer thickness of 10 cm, and by drying the concentrate, if appropriate.