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    PROCESS FOR PRODUCING TEREPHTHALIC ACID
    21.
    发明申请
    PROCESS FOR PRODUCING TEREPHTHALIC ACID 有权
    生产过敏性酸的方法

    公开(公告)号：US20120004450A1

    公开(公告)日：2012-01-05

    申请号：US13155553

    申请日：2011-06-08

    申请人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    发明人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC分类号： C07C51/265 ,  C07C51/16

    CPC分类号： C07C51/265 ,  C07C51/42 ,  Y02P20/52 ,  Y02P20/542 ,  C07C63/26

    摘要： A solid terephthalic acid composition and a process for producing terephthalic acid from para-xylene. The process comprises forming a mixture comprising the para-xylene, a solvent, a bromine source, and a catalyst; and oxidizing the para-xylene by contacting the mixture with an oxidizing agent at oxidizing conditions to produce a solid oxidation product comprising terephthalic acid, para-toluic acid, 4-carboxybenzaldehyde. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an dialkyl imidazolium ionic liquid; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium. The solid terephthalic acid composition comprises, less than about 4,000 ppm-wt 4-carboxybenzaldehyde content, and more than about 2,000 ppm-wt a para-toluic acid.

    摘要翻译： 固体对苯二甲酸组合物和由对二甲苯生产对苯二甲酸的方法。 该方法包括形成包含对二甲苯，溶剂，溴源和催化剂的混合物; 并通过在氧化条件下将氧化剂与氧化剂接触来氧化对二甲苯以产生包含对苯二甲酸，对甲苯甲酸，4-羧基苯甲醛的固体氧化产物。 溶剂包括具有1至7个碳原子的羧酸和二烷基咪唑鎓离子液体; 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。 固体对苯二甲酸组合物包含小于约4,000ppm重量的4-羧基苯甲醛含量和大于约2,000ppm重量的对甲苯甲酸。

    PROCESS FOR THE DIRECT PRODUCTION OF METHANOL FROM METHANE
    23.
    发明申请
    PROCESS FOR THE DIRECT PRODUCTION OF METHANOL FROM METHANE 有权
    从甲烷直接生产甲醇的方法

    公开(公告)号：US20070149833A1

    公开(公告)日：2007-06-28

    申请号：US11560960

    申请日：2006-11-17

    申请人： Timothy A. Brandvold ,  Joseph A. Kocal

    发明人： Timothy A. Brandvold ,  Joseph A. Kocal

    IPC分类号： C07C29/03

    CPC分类号： C07C29/48 ,  C07C29/095 ,  C07C29/80 ,  C07C67/035 ,  C07C69/63 ,  C07C31/04

    摘要： A process for the production of methanol from methane has been developed. The process involves reacting methane with an oxidant such as oxygen or a peroxide in the presence of a catalyst and a solvent in a reaction zone to produce an effluent stream comprising a methanol product. The effluent stream is next separated into a gaseous stream comprising unreacted methane and carbon dioxide and a liquid stream comprising the methanol product and solvent. Next the gaseous stream is further separated to provide a methane stream which is recycled to the reaction zone. Finally, a methanol stream is isolated and a solvent stream is recycled to the reaction zone.

    摘要翻译： 已经开发了从甲烷生产甲醇的方法。 该方法包括在反应区中在催化剂和溶剂存在下使甲烷与氧化剂如氧或过氧化物反应，以产生包含甲醇产物的流出物流。 然后将流出物流分离成包含未反应的甲烷和二氧化碳的气流以及包含甲醇产物和溶剂的液体流。 接下来，进一步分离气流以提供甲烷流，其被再循环到反应区。 最后，分离甲醇流，将溶剂流再循环到反应区。

    PROCESS FOR THE PRODUCTION OF METHANOL FROM METHANE USING A METAL TRIFLUOROACETATE CATALYST
    24.
    发明申请
    PROCESS FOR THE PRODUCTION OF METHANOL FROM METHANE USING A METAL TRIFLUOROACETATE CATALYST 审中-公开
    使用金属三氟乙酸酯催化剂从甲烷生产甲醇的方法

    公开(公告)号：US20070149832A1

    公开(公告)日：2007-06-28

    申请号：US11560943

    申请日：2006-11-17

    申请人： Wensheng Chen ,  Timothy A. Brandvold ,  Maureen L. Bricker ,  Joseph A. Kocal ,  Joel T. Walenga

    发明人： Wensheng Chen ,  Timothy A. Brandvold ,  Maureen L. Bricker ,  Joseph A. Kocal ,  Joel T. Walenga

    IPC分类号： C07C29/03

    CPC分类号： C07C29/095 ,  C07C67/035 ,  C07C69/63 ,  C07C31/04

    摘要： A process for converting methane to methanol using a homogeneous catalyst has been developed. The catalyst is a metal compound having an empirical formula of MxXm where M is a metal such as Pd, Cu, Co, and Mn, X is an anion such as acetate, trifluoroacetate, sulfate, propionate, “m” is the oxidation state of M, and “x” is the anion valence of X. Generally the process involves contacting a gas stream containing methane with the homogeneous catalyst and an oxidant such as hydrogen peroxide at oxidation conditions to produce methyl trifluoroacetate. Finally, the methyl trifluoroacetate is hydrolyzed to give a methanol product stream.

    摘要翻译： 已经开发了使用均相催化剂将甲烷转化成甲醇的方法。 该催化剂是经验式为M x X X m的金属化合物，其中M是诸如Pd，Cu，Co和Mn的金属，X是阴离子 作为乙酸盐，三氟乙酸盐，硫酸盐，丙酸盐，“m”是M的氧化态，“x”是X的阴离子价。通常，该方法包括使含有甲烷的气流与均相催化剂和氧化剂如氢 过氧化物在氧化条件下产生三氟乙酸甲酯。 最后，将三氟乙酸甲酯水解，得到甲醇产物流。

    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME
    28.
    发明申请
    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME 有权
    低氧生物质衍生的热解油及其生产方法

    公开(公告)号：US20110201855A1

    公开(公告)日：2011-08-18

    申请号：US12707433

    申请日：2010-02-17

    申请人： Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    发明人： Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    IPC分类号： C10G1/00

    CPC分类号： C10G3/44 ,  C10G3/45 ,  C10G3/47 ,  C10G3/48 ,  C10G3/49 ,  C10G2400/30 ,  Y02E50/14 ,  Y02P30/20

    摘要： Low oxygen biomass-derived pyrolysis oils and methods for producing them from carbonaceous biomass feedstock are provided. The carbonaceous biomass feedstock is pyrolyzed in the presence of a catalyst comprising base metal-based catalysts, noble metal-based catalysts, treated zeolitic catalysts, or combinations thereof to produce pyrolysis gases. During pyrolysis, the catalyst catalyzes a deoxygenation reaction whereby at least a portion of the oxygenated hydrocarbons in the pyrolysis gases are converted into hydrocarbons. The oxygen is removed as carbon oxides and water. A condensable portion (the vapors) of the pyrolysis gases is condensed to low oxygen biomass-derived pyrolysis oil.

    摘要翻译： 提供了低氧生物质衍生的热解油及其从碳质生物质原料生产它们的方法。 在含有贱金属基催化剂，贵金属基催化剂，经处理的沸石催化剂或其组合的催化剂存在下，碳质生物质原料热解产生裂解气。 在热解期间，催化剂催化脱氧反应，由此将热解气体中的至少一部分氧化烃转化成烃。 作为碳氧化物和水除去氧气。 热解气体的可冷凝部分（蒸汽）被冷凝成低氧生物质衍生的裂解油。

    Mixtures used in oxidizing alkyl aromatic compounds
    30.
    发明授权
    Mixtures used in oxidizing alkyl aromatic compounds 有权
    用于氧化烷基芳族化合物的混合物

    公开(公告)号：US09045407B2

    公开(公告)日：2015-06-02

    申请号：US13155530

    申请日：2011-06-08

    申请人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    发明人： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC分类号： C07C51/265

    CPC分类号： C07C51/265 ,  C07C63/06 ,  C07C63/16 ,  C07C63/26

    摘要： A process and a mixture for oxidizing an alkyl-aromatic compound comprises forming a mixture comprising the alkyl-aromatic compound, a solvent, a bromine source, and a catalyst; and contacting the mixture with an oxidizing agent at oxidizing conditions to produce an oxidation product comprising at least one of an aromatic aldehyde, an aromatic alcohol, an aromatic ketone, and an aromatic carboxylic acid. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an ionic liquid selected from the group consisting of an imidazolium ionic liquid, a pyridinium ionic liquid, a phosphonium ionic liquid, a tetra alkyl ammonium ionic liquid, and combinations thereof. The catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium.

    摘要翻译： 用于氧化烷基 - 芳族化合物的方法和混合物包括形成包含烷基 - 芳族化合物，溶剂，溴源和催化剂的混合物; 以及在氧化条件下使所述混合物与氧化剂接触以产生包含芳族醛，芳族醇，芳族酮和芳族羧酸中的至少一种的氧化产物。 溶剂包括具有1至7个碳原子的羧酸和选自咪唑鎓离子液体，吡啶鎓离子液体，鏻离子液体，四烷基铵离子液体及其组合的离子液体。 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。