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    Electrolytic process and apparatus
    31.
    发明授权
    Electrolytic process and apparatus 失效
    电解过程和设备

    公开(公告)号：US6099914A

    公开(公告)日：2000-08-08

    申请号：US401299

    申请日：1999-09-23

    申请人： Yasuki Yoshida ,  Setsuro Ogata ,  Masaharu Uno ,  Masashi Tanaka ,  Yoshinori Nishiki ,  Takayuki Shimamune ,  Hiroshi Inoue ,  Chiaki Iwakura

    发明人： Yasuki Yoshida ,  Setsuro Ogata ,  Masaharu Uno ,  Masashi Tanaka ,  Yoshinori Nishiki ,  Takayuki Shimamune ,  Hiroshi Inoue ,  Chiaki Iwakura

    IPC分类号： C01B3/00 ,  C23C18/16 ,  B05D1/18

    CPC分类号： C01B3/0078 ,  C10G45/00 ,  C10G45/32 ,  C25B1/02 ,  C25B3/00 ,  C10G2300/4056 ,  C10G2300/42 ,  Y02E60/324

    摘要： An electrolytic process and apparatus which can operate in a hydrogen reaction chamber at a hydrogen reaction rate corresponding to the increase in the rate of production of hydrogen accompanying the increase in the electrolysis rate and maintain the current efficiency at a very high value with respect to the electrolytic current for producing hydrogen and a process for the production of an electrode for this purpose. An electrolytic process is provided which comprises effecting electrolysis of an electrolytic solution in an electrolytic chamber separated from a reaction chamber by a hydrogen-storing metal member with one surface of the hydrogen-storing metal member as a cathode opposing an anode so that hydrogen thus produced is adsorbed by the hydrogen-storing metal member while allowing hydrogen thus adsorbed and a material to be treated to undergo continuous catalytic reaction in the reaction chamber on the other surface of the hydrogen-storing metal member to cause hydrogenation or reduction reaction by hydrogen thus adsorbed, wherein an electrolytic apparatus having a porous catalyst layer provided on the catalytic reaction surface of the hydrogen-storing metal member is used. The porous catalyst layer is obtained by reducing metal cations in an electroless plating solution by active hydrogen desorbed from a hydrogen-storing metal so that the hydrogen-storing metal is plated with the metal.

    摘要翻译： 一种电解方法和装置，其可以在氢反应室中以氢反应速率操作，其伴随着电解速率的增加伴随着氢的生成速率的增加，并且将电流效率保持在非常高的值，相对于 用于生产氢的电解电流和用于生产电极的方法。 提供了一种电解方法，其包括通过储氢金属构件在与反应室分离的电解室中电解电解溶液，其中储氢金属构件的一个表面作为与阳极相对的阴极，从而产生氢 被吸氢金属部件吸附，同时允许被吸附的氢，并且被处理材料在储氢金属部件的另一个表面上的反应室中进行连续的催化反应，由此吸附氢气或还原反应 其中，使用具有设置在所述储氢金属构件的催化反应面上的多孔催化剂层的电解装置。 多孔催化剂层是通过从吸氢金属解吸的活性氢还原化学镀溶液中的金属阳离子而得到的，以使储氢金属镀金属。

    Process and apparatus for the production of an aqueous solution of hydrogen peroxide
    32.
    发明授权
    Process and apparatus for the production of an aqueous solution of hydrogen peroxide 失效
    用于生产过氧化氢水溶液的方法和设备

    公开(公告)号：US6045684A

    公开(公告)日：2000-04-04

    申请号：US60814

    申请日：1998-04-16

    申请人： Shuhei Wakita ,  Masaharu Uno ,  Takayuki Shimamune ,  Yoshinori Nishiki ,  Kunio Nishimura

    发明人： Shuhei Wakita ,  Masaharu Uno ,  Takayuki Shimamune ,  Yoshinori Nishiki ,  Kunio Nishimura

    IPC分类号： C01B15/01 ,  B01D61/44 ,  C25B1/30

    CPC分类号： B01D61/44

    摘要： An on-site process and apparatus for producing hydrogen peroxide at a high efficiency substantially from brine and oxygen-containing gas alone as raw materials while removing alkaline earth metals. Sea water concentrated by an electrodialytic apparatus 2 or the like as a raw material is supplied to an impurity removing apparatus 10 where caustic soda produced in an acid-alkali producing apparatus 11 at a subsequent stage and/or carbon dioxide gas is added to remove alkaline earth metals contained in sea water in the form of a hydroxide or carbonate precipitate. Separately, the acid-alkali producing apparatus 11 performs a salt separating operation to produce caustic soda which is then supplied to a hydrogen peroxide generator 28 to produce an alkaline aqueous solution of hydrogen peroxide.

    摘要翻译： 一种现有的过程和装置，其以高效率生产基本上从盐水和含氧气体为原料的过氧化氢，同时除去碱土金属。 通过电渗析装置2等作为原料浓缩的海水被供给到杂质除去装置10中，在除去装置10中，在后续阶段的酸碱生产装置11中产生苛性钠和/或二氧化碳气体以除去碱 包含在海水中的以氢氧化物或碳酸盐沉淀形式的地球金属。 单独地，酸碱生产装置11进行盐分离操作以产生苛性钠，然后将其供应到过氧化氢发生器28以产生碱性过氧化氢水溶液。

    Process and electrolytic cell for producing hydrogen peroxide
    34.
    发明授权
    Process and electrolytic cell for producing hydrogen peroxide 有权
    用于生产过氧化氢的工艺和电解槽

    公开(公告)号：US06254762B1

    公开(公告)日：2001-07-03

    申请号：US09405002

    申请日：1999-09-27

    申请人： Masaharu Uno ,  Shuhei Wakita ,  Yoshinori Nishiki

    发明人： Masaharu Uno ,  Shuhei Wakita ,  Yoshinori Nishiki

    IPC分类号： C25B130

    CPC分类号： C25B1/30

    摘要： A process and apparatuses for producing hydrogen peroxide which provides good current density and production efficiency from an electrolytic liquid having an exceedingly low conductivity, such as ultrapure water. An electrolytic cell main body containing an anode 5 and a cathode 6 which are electrically connected to each other via ion-exchange resin particles 9 is used to conduct electrolysis while maintaining the electrical connection. High-purity, high-concentration hydrogen peroxide is produced at a high current efficiency even when the electrolytic liquid has an exceedingly low conductivity.

    摘要翻译： 一种生产过氧化氢的方法和装置，其从具有极低导电性的电解液（例如超纯水）提供良好的电流密度和生产效率。 使用含有通过离子交换树脂粒子9电连接的阳极5和阴极6的电解槽主体进行电解，同时保持电连接。 即使当电解液具有极低的电导率时，也能以高电流效率生产高纯度，高浓度的过氧化氢。

    Process for the production of hydrogen peroxide solution
    37.
    发明授权
    Process for the production of hydrogen peroxide solution 失效
    生产过氧化氢溶液的方法

    公开(公告)号：US06761815B2

    公开(公告)日：2004-07-13

    申请号：US10095482

    申请日：2002-03-13

    申请人： Yasuo Nakajima ,  Yoshinori Nishiki ,  Masaharu Uno ,  Akira Katsumoto ,  Kunio Nishimura

    发明人： Yasuo Nakajima ,  Yoshinori Nishiki ,  Masaharu Uno ,  Akira Katsumoto ,  Kunio Nishimura

    IPC分类号： C25B100

    CPC分类号： C25B1/30

    摘要： A process for the production of hydrogen peroxide solution from seawater as a starting material substantially free of effective chlorine or organic halogen compounds. An electric current is passed through an insoluble anode and an oxygen gas diffusion cathode while keeping the halide ion concentration of anolyte supplied to the anode chamber to a level not greater than 1 g/l. Hydrogen peroxide thus generated dissolves in the catholyte. Anodic oxidation of halide ions is suppressed, to thereby inhibit the production of effective chlorine.

    摘要翻译： 一种从海水中生产过氧化氢溶液作为起始原料基本上不含有效氯或有机卤素化合物的方法。 将电流通过不溶性阳极和氧气扩散阴极，同时将供给阳极室的阳极电解液的卤离子浓度保持在不高于1g / l的水平。 因此产生的过氧化氢溶解在阴极电解液中。 卤离子的阳极氧化被抑制，从而抑制有效氯的产生。

    Electrolyte process using a hydrogen storing metal member
    39.
    发明授权
    Electrolyte process using a hydrogen storing metal member 失效
    使用储氢金属部件的电解液处理

    公开(公告)号：US06224741B1

    公开(公告)日：2001-05-01

    申请号：US09131677

    申请日：1998-08-10

    申请人： Yasuki Yoshida ,  Setsuro Ogata ,  Masaharu Uno ,  Masashi Tanaka ,  Yoshinori Nishiki ,  Takayuki Shimamune ,  Hiroshi Inoue ,  Chiaki Iwakura

    发明人： Yasuki Yoshida ,  Setsuro Ogata ,  Masaharu Uno ,  Masashi Tanaka ,  Yoshinori Nishiki ,  Takayuki Shimamune ,  Hiroshi Inoue ,  Chiaki Iwakura

    IPC分类号： C25B102

    CPC分类号： C01B3/0078 ,  C10G45/00 ,  C10G45/32 ,  C10G2300/4056 ,  C10G2300/42 ,  C25B1/02 ,  C25B3/00 ,  Y02E60/324

    摘要： An electrolytic process which can operate in a hydrogen reaction chamber at a hydrogen reaction rate corresponding to the increase in the rate of production of hydrogen accompanying the increase in the electrolysis rate and maintain the current efficiency at a very high value with respect to the electrolytic current for producing hydrogen and a process for the production of an electrode for this purpose. An electrolytic process is provided which comprises effecting electrolysis of an electrolytic solution in an electrolytic chamber separated from a reaction chamber by a hydrogen-storing metal member with one surface of the hydrogen-storing metal member as a cathode opposing an anode so that hydrogen thus produced is adsorbed by the hydrogen-storing metal member while allowing hydrogen thus adsorbed and a material to be treated to undergo continuous catalytic reaction in the reaction chamber on the other surface of the hydrogen-storing metal member to cause hydrogenation or reduction reaction by hydrogen thus adsorbed.

    摘要翻译： 一种电解方法，其可以在氢反应室中以氢反应速率操作，其伴随着电解速率的增加伴随着氢气生成速率的增加，并且将电流效率保持在相对于电解电流非常高的值 用于生产氢气和用于生产电极的方法。 提供了一种电解方法，其包括通过储氢金属构件在与反应室分离的电解室中电解电解溶液，其中储氢金属构件的一个表面作为与阳极相对的阴极，从而产生氢 被吸氢金属部件吸附，同时允许被吸附的氢，并且被处理材料在储氢金属部件的另一个表面上的反应室中进行连续的催化反应，由此吸附氢气或还原反应 。

    ACTIVATED CATHODE FOR HYDROGEN EVOLUTION
    40.
    发明申请
    ACTIVATED CATHODE FOR HYDROGEN EVOLUTION 有权
    用于氢演化的活化阴极

    公开(公告)号：US20120305389A1

    公开(公告)日：2012-12-06

    申请号：US13576811

    申请日：2011-01-18

    申请人： Miwako Nara ,  Eri Miyakawa ,  Yoshinori Nishiki

    发明人： Miwako Nara ,  Eri Miyakawa ,  Yoshinori Nishiki

    IPC分类号： C25B11/08 ,  C25B1/02 ,  C25B11/06

    CPC分类号： C25B11/0494 ,  C25B11/0484 ,  Y02E60/366

    摘要： The present invention aims to provide an activated cathode enabling a long-time stable operation with hydrogen overvoltage maintained at a low value, keeping a high remaining rate of the catalyst element after a cease of operation for a short-circuiting and after an electrolysis operation at a high current density, restricting catalyst loss to a little, and having a strong resistance to contamination caused by electrolyte impurity elements.The present invention relates to a cathode for hydrogen evolution with a catalyst layer formed on the cathode substrate, having, at least, three elements comprising platinum, cerium and palladium, as essential element, in a state of metal, metal oxide, or hydroxide, contained, where the mole fraction of respective element being x, y, and z, within a range of 5 mol %≦x≦90 mol %, 5 mol %≦y≦55 mol %, 5 mol %≦z≦65 mol %.

    摘要翻译： 本发明的目的在于提供一种能够在氢过电压保持低值的情况下进行长时间稳定运行的活性阴极，在短路运转停止后和电解运转后保持催化剂元素的高残留率 高电流密度，将催化剂损失限制到少许，并且对电解质杂质元素引起的污染具有很强的抵抗力。 本发明涉及在金属，金属氧化物或氢氧化物的状态下，在阴极基板上形成有催化剂层的阴极，其具有至少三种包含铂，铈和钯作为必需元素的元素， 含有，其中各元素的摩尔分数为x，y和z在5mol％＆amp; NlE; x＆amp; NlE; 90mol％，5mol％＆amp; NlE; y＆amp; NlE; 55mol％，5mol％和nlE; z＆ 65摩尔％。