Abstract:
A sequential spectrophotometer system having a light source, a scanning type monochromator, a stepper motor means for changing the monochromator wavelength over a light spectrum being scanned, a photomultiplier for measuring the intensity of light absorption or passage through a sample being tested and generating a signal corresponding thereto, data acquisition means for compiling data corresponding to said signals and means for recording such data generally as a function of light measured for each wavelength, the improvement comprising:a method and means to effect the data acquisition conversion at or about each desired wavelength during a respective stepper motor rotor displacement period, i.e., during each corresponding period of diffraction grating vibration or oscillation following a stepper motor disposition thereof to another wavelength position angle.
Abstract:
An improvement in a spectrophotometer of an improved apparatus for automatic initialization of the wavelength indexing function of the spectrophotometer. A drive mechanism drives the wavelength indexing movement of the spectrophotometer diffraction grating. The grating is initialized to a grating initialization position by physical opposition of a stop mechanism to the driving when a drive linkage reaches a drive linkage initialization position.
Abstract:
A slow scan, frequency limited spectrometer having a screw mechanism for driving a rotatable grating is improved by incorporating and interlinking the following new constituent members with the screw mechanism: a cylindrical cam member with a groove and a constraint to attain a predetermined pitch, so that rapid scanning of a preselected wavelength range is achieved with the grating; a high torque, variable speed, direct current electric motor, so that the rapid scanning may be varied in speed; and, a liner potentiometer with a sliding contact, so that a remote wavelength readout of the variable rapid scanning can be obtained. Cylinder cam members of various pitches are also disclosed for use in scanning different wavelength ranges. At a low cost for improvements, the resulting spectrometer provides a variable fast scan, and is frequency selective.
Abstract:
A spectrometer capable of providing a predetermined wavelength of output light in accordance with a control voltage signal applied to a scanning element is described. The scanning element located at the grating image of the spectrometer is a small mirror attached to the rotor of a galvanometer whose angular position is accurately controlled by a closed-loop electronic control. The spectrum reflected from the mirror is passed through a slit to provide the output light of a predetermined wavelength. Selection of the waveform of the control signal allows the spectrometer to be operated as a dual wavelength spectrometer, to use a linear wavelength scan, or other wavelength scan patterns for absorbance analyses of a sample. The rapid scan capability of this instrument has been utilized to extend the measurement of absorbance changes at one wavelength, corrected for light scattering changes (dual-wavelength spectroscopy), to the measurement of the complete differential absorbance spectrum, similarly corrected for light scattering changes (corrected-differential spectroscopy).
Abstract:
A wavelength reading apparatus for a monochromator comprises a monochromator utilizing a dispersion element for dispersing light in accordance with its wavelengths, a dispersion element driver unit for rotating the dispersion element to effect the tuning wavelength scanning operation of the monochromator and a wavelength counter for adding or subtracting a pulse, which is produced each time when the tuning wavelength of the monochromator changes by a predetermined wavelength increment, depending on whether the wavelength increases or decreases. The wavelength counter is set to a predetermined counting value, in response to a wavelength calibrating pulse produced when the tuning wavelength of the monochromator reaches a predetermined value, so that any counting value of the wavelength counter correctly represents the instant value of the tuning wavelength of the monochromator.
Abstract:
In a recording spectrophotometer the ordinate of the plotter-scriber is controlled by the output of a photomultiplier while the abscissa of the plotter-scriber is controlled by a selectable mode manually adjusted controller.In one mode, the controller furnishes a time base signal of selected rate of change, so that the abscissa of the plotter-scriber varies with the passage of time in accordance with said rate of change.In aother mode, the controller furnishes a stepping signal of selected periodicity, for application to a stepping motor, which changes the wavelength adjustment of the spectrophotometer at a rate determined by the selected periodicity. The spectrophotometer furnishes to the plotter-scriber an analog voltge varying with the instantaneous wavelength setting of the spectrophotometer, so that the abscissa of the plotter-scriber correspondingly varies with the instantaneous value of the wavelength.A common manually adjusted digital setting means is used for adjusting either the said selected rate of change of the time base or the said selected periodicity of the stepping signal.
Abstract:
A scanning monochromator or spectrometer having a reflecting grating whose curvature in the meridian plane is equal to the curvature of a circle upon which the source, detecting means and grating lie and whose lines are ruled with a frequency which varies systematically and directly in proportion to the distance of the lines from a point of origin on the track as determined by the geometry of the equipment, and gratings therefor.
Abstract:
A spectrometer having an entrance aperture, at least one collimating mirror, a prism and an echelle grating which is so mounted to provide rotation in two directions thereby providing adjustment of the vertical and horizontal components of the dispersed energy in the exit focal plane.
Abstract:
This disclosure describes optical systems that have output beams that are spatially invariant to the angle of incidence upon a certain rotatable surface forming a part of the systems, and can be used to select the wavelength of the output of an optical source, such as a laser cavity, or to aid in measuring the reflectance of a material in reflectance spectroscopy. The optical systems comprise various combinations of plane mirrors and plane diffraction gratings (or sample surfaces), in some embodiments, spherical mirrors. The plane mirrors, plane gratings and spherical mirrors are either rotated or fixed in space in accordance with a particular embodiment. The moveable suitable movement mechanism, such as a micrometer. By rotating the shaft of the micrometer to a particular incidence angle, the frequency of the output of a laser cavity can be selected. Alternately, the reflectance of a material can be observed for a particular angle. In either case, the output beam remains spatially invariant as the position of the shaft and its attached elements is changed.