Fluorination process
    63.
    发明授权
    Fluorination process 失效
    荧光法

    公开(公告)号:US3787489A

    公开(公告)日:1974-01-22

    申请号:US3787489D

    申请日:1972-05-01

    Applicant: RHONE PROGIL

    Abstract: A PROCESS FOR THE PERFLUORINATION OF PERCHLORO COMPOUNDS CONTAINING A TRICHLOROMETHYL AND/OR PENTACHLOROETHYL GROUOP BY REACTION WITH ANHYDROUS HF IN THE VAPOR PHASE IN THE PRESENCE OF A FIXED BED CATALYST, WHEREIN THE PERCHLORO COMPOUND AND HF ARE PASSED THROUGH A FIRST REACTION ZONE AT AN ELEVATED TEMPERATURE TO CONVERT THE PERCHLORO COMPOUND TO AT LEAST THE CORRESPONDING DIFLUORO DERIVATIVE, THE REACTION GASES ARE PASSED TO A A SECOND ZONE TO PRODUCE A REACTION MIXTURE IN WHICH THE INTERMEDIATE CHLOROFLUORO COMPOUNDS CONTAIN AN AVERAGE RATION OF F ATOMS TO CL ATOMS OF AT LEAST 1.5, AND THE REACTION MIXTURE IS PASSED TO A THIRD ZONE MAINTAINED AT A HIGHER TEMPERATURE, WITH THE PRESSURE IN EACH ZONE BEING WITHIN THE RANGE OF 1-4 BARS AND THE TEMPERATURE IN EACH ZONE BEING AT LEAST 10*C. HIGHER THAN THAT IN THE PRECEDING ZONE.

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