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    ISOXAZOLINE-SUBSTITUTED BENZAMIDE COMPOUND AND PESTICIDE
    1.
    发明申请
    ISOXAZOLINE-SUBSTITUTED BENZAMIDE COMPOUND AND PESTICIDE 审中-公开
    ISOXAZOLINE-替代苄基化合物和杀虫剂

    公开(公告)号：US20150105398A1

    公开(公告)日：2015-04-16

    申请号：US14568964

    申请日：2014-12-12

    Applicant: Nissan Chemical Industries, Ltd.

    Inventor： Takeshi MITA ,  Takamasa KIKUCHI ,  Takashi MIZUKOSHI ,  Manabu YAOSAKA ,  Mitsuaki KOMODA

    IPC: C07D413/04 ,  C07D261/04

    CPC classification number: A61K31/421 ,  A01N43/80 ,  A61K9/0053 ,  C07C25/02 ,  C07C25/06 ,  C07C25/08 ,  C07C25/13 ,  C07C25/24 ,  C07C43/1742 ,  C07C43/1745 ,  C07C205/11 ,  C07C205/12 ,  C07C211/52 ,  C07C251/48 ,  C07C255/29 ,  C07C255/50 ,  C07C255/60 ,  C07C281/02 ,  C07C323/09 ,  C07D261/04 ,  C07D261/16 ,  C07D413/04 ,  C07D413/06 ,  C07D413/12 ,  C07D413/14 ,  C07D417/06 ,  C07D417/12 ,  C07F7/0812

    Abstract: A substituted alkenylbenzene compound of formula (4): wherein X1 is selected from the group consisting of a halogen atom, —SF5, C1-C6haloalkyl, hydroxy C1-C6haloalkyl, C1-C6alkoxy C1-C6haloalkyl, C3-C8halocycloalkyl, C1-C6 haloalkoxy C1-C3haloalkoxy C1-C3haloalkoxy, C1-C6haloalkylthio, C1-C6haloalkylsulfinyl and C1-C6haloalkylsulfonyl; X3 is selected from the group consisting of a hydrogen atom, halogen atom, cyano, nitro, C1-C6alkyl, C1-C6haloalkyl, C1-C6alkoxy and C1-C6 alkylthio; X4 is selected from the group consisting of a hydrogen atom, halogen atom, cyano, C1-C4alkyl, C1-C4alkoxy and C1-C4haloalkoxy; R3 is —C(R3a)(R3b)R3c, where R3a and R3b independently of each other are a halogen atom, or R3a and R3b together form 3- to 6-membered ring together with the carbon atom bonding them by forming a C2-C5haloalkylene chain, and R3c is selected from the group consisting of a hydrogen atom, halogen atom, C1-C5alkyl, C1-C5haloalkyl, C1-C4haloalkoxy and C1-C4haloalkylthio, with a proviso that in case here X1 is a fluorine atom, chlorine atom or trifluoromethyl, and both X2 and X3 are a hydrogen atom, in case where both X1 and X2 are fluorine atom and X3 is a hydrogen atom, and in case where both X1 and X2 are trifluoromethyl and X3 is a hydrogen atom, R3c is a hydrogen atom, chlorine atom, bromine atom, iodine atom, C1-C5alkyl, C1-C5haloalkyl, C1-C4haloalkoxy or C1-C4haloalkylthio.

    Abstract translation: 式（4）的取代烯基苯化合物：其中X 1选自卤素原子，-SF 5，C 1 -C 6卤代烷基，羟基C 1 -C 6卤代烷基，C 1 -C 6烷氧基C 1 -C 6卤代烷基，C 3 -C 8卤代环烷基，C 1 -C 6卤代烷氧基 C 1 -C 3卤代烷氧基C 1 -C 3卤代烷氧基，C 1 -C 6卤代烷硫基，C 1 -C 6卤代烷基亚磺酰基和C 1 -C 6卤代烷基磺酰基; X 3选自氢原子，卤素原子，氰基，硝基，C 1 -C 6烷基，C 1 -C 6卤代烷基，C 1 -C 6烷氧基和C 1 -C 6烷硫基; X 4选自氢原子，卤素原子，氰基，C 1 -C 4烷基，C 1 -C 4烷氧基和C 1 -C 4卤代烷氧基; R3是-C（R3a）（R3b）R3c，其中R3a和R3b彼此独立地是卤素原子，或者R3a和R3b与通过形成C2- C5卤代烷基链，R3c选自氢原子，卤素原子，C1-C5烷基，C1-C5卤代烷基，C1-C4卤代烷氧基和C1-C4卤代烷硫基，条件是在这里X1是氟原子的情况下，氯原子 或三氟甲基，X2和X3均为氢原子，X1和X2均为氟原子，X3为氢原子的情况下，X1和X2均为三氟甲基，X3为氢原子时，R3c为 氢原子，氯原子，溴原子，碘原子，C1-C5烷基，C1-C5卤代烷基，C1-C4卤代烷氧基或C1-C4卤代烷硫基。

    Method for producing p-dichlorobenzene
    4.
    发明申请
    Method for producing p-dichlorobenzene 有权
    对二氯苯的制备方法

    公开(公告)号：US20060106264A1

    公开(公告)日：2006-05-18

    申请号：US10526557

    申请日：2003-09-03

    Applicant: Takashi Wakasugi ,  Tsugio Nonaka ,  Tadashi Miyakawa ,  Takanobu Hanabusa ,  Kazuhiko Sunagawa ,  Shigeru Mizusawa

    Inventor： Takashi Wakasugi ,  Tsugio Nonaka ,  Tadashi Miyakawa ,  Takanobu Hanabusa ,  Kazuhiko Sunagawa ,  Shigeru Mizusawa

    IPC: C07C17/06

    CPC classification number: C07C17/12 ,  C07C25/08

    Abstract: In a process for preparing p-dichlorobenzene by nuclear chlorination of benzene and/or chlorobenzene as the starting material with chlorine molecules, chlorination is carried out using aluminum chloride in an amount of 0.1-3 millimols per mol of the starting material and phenothiazines such as 10H-phenothiazine-10-carboxylic acid phenyl ester in an amount of 0.1-0.9 mols per mol of aluminum chloride so as to be a chlorination degree in a range of 1.2-2.5, by which p-dichlorobenzene can be obtained in a high para-selectivity and a short reaction time.

    Abstract translation: 在通过用氯分子的苯和/或氯苯作为起始原料的核氯化制备对二氯苯的方法中，使用氯化铝使用0.1-3毫摩尔/摩尔原料和吩噻嗪，例如 10 H-吩噻嗪-10-羧酸苯酯，其用量为0.1-0.9摩尔/摩尔氯化铝，氯化度在1.2-2.5范围内，可以以高的比例获得对二氯苯 对位选择性和反应时间短。

    Process for producing p-dichlorobenzene
    10.
    发明授权
    Process for producing p-dichlorobenzene 有权
    对二氯苯生产方法

    公开(公告)号：US08524957B2

    公开(公告)日：2013-09-03

    申请号：US13125933

    申请日：2009-10-23

    Applicant: Tsuyoshi Okamoto

    Inventor： Tsuyoshi Okamoto

    IPC: C07C17/00

    CPC classification number: C07C17/12 ,  C07C25/08

    Abstract: To provide a novel process for producing p-dichlorobenzene satisfying both of high selectivity of p-dichlorobenzene and high conversion of chlorine at the same time.A process for continuously producing p-dichlorobenzene, which is a process for producing p-dichlorobenzene by a nuclear chlorination reaction of benzene and/or chlorobenzene with chlorine, in the presence of a Lewis acid catalyst and a phenothiazine analogue compound, said process comprising; employing a reactor having a first supply route for continuously supplying a mixed solution of benzene and/or chlorobenzene and a Lewis acid catalyst to a reactor, a second supply route for continuously supplying a mixed solution of benzene and/or chlorobenzene and a phenothiazine analogue compound to the above reactor, and a third supply route for continuously supplying chlorine to the above reactor; and supplying these raw materials for the reaction by opening the above first supply route and third supply route in random order at the initiation of reaction, and then opening the above second supply route.

    Abstract translation: 提供同时满足对二氯苯的高选择性和高氯转化率的对二氯苯的新方法。 一种连续生产对二氯苯的方法，该方法是在路易斯酸催化剂和吩噻嗪类似物化合物的存在下，通过苯和/或氯苯与氯的氯化氯反应制备对二氯苯的方法。 使用具有用于将苯和/或氯苯和路易斯酸催化剂的混合溶液连续供应到反应器的第一供给路径的反应器，用于连续供应苯和/或氯苯和吩噻嗪类似物化合物的混合溶液的第二供应途径 和上述反应器连续供给氯的第三供给路径; 并通过在反应开始时以随机的顺序打开上述第一供给路径和第三供给路径来供给这些反应原料，然后打开上述第二供给路径。

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