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    N-substituted tetrahydroquinolines for use as antioxidants in lubricants
    62.
    发明授权
    N-substituted tetrahydroquinolines for use as antioxidants in lubricants 失效
    用作润滑剂中抗氧化剂的N-取代四氢喹啉

    公开(公告)号：US4919832A

    公开(公告)日：1990-04-24

    申请号：US305037

    申请日：1989-02-02

    申请人： Hans R. Meier ,  Samuel Evans

    发明人： Hans R. Meier ,  Samuel Evans

    IPC分类号： C07D215/06 ,  C10M133/40 ,  C10M135/32

    CPC分类号： C07D215/06 ,  C10M133/40 ,  C10M135/32 ,  C10M2201/02 ,  C10M2215/22 ,  C10M2215/221 ,  C10M2215/225 ,  C10M2215/226 ,  C10M2215/30 ,  C10M2219/09 ,  C10N2240/06 ,  C10N2240/08 ,  C10N2240/40

    摘要： Composition containing(a) at least one lubricant, hydraulic oil or metal-working fluid based on mineral oil or synthetic oils and(b) 0.05-5% by weight, based on the total weight of the lubricant, hydraulic oil or metal-working fluid composition, of at least one compound of the formula V ##STR1## where R.sup.1 and R.sup.2 are independently alkyl, aryl, substituted aryl or benzyl, R.sup.3 is hydrogen or methyl, R.sup.4 and R.sup.5 are independently hydrogen, methyl, methoxy, chloro or nitro, R.sup.13 is hydrogen or methyl, and R.sup.17 is a direct bond, alkylene or vinylene.

    摘要翻译： 组合物，其含有（a）至少一种基于矿物油或合成油的润滑剂，液压油或金属加工液，和（b）基于润滑剂，液压油或金属加工的总重量的0.05-5重量％ （I）的化合物（VI）其中R 1和R 2独立地是烷基，芳基，取代的芳基或苄基，R 3是氢或甲基 ，R 4和R 5独立地是氢，甲基，甲氧基，氯或硝基，R 13是氢或甲基，R 17是直接键，亚烷基或亚乙烯基。

    Phenol phosphorus compounds as polyolefin stabilizers
    63.
    发明授权
    Phenol phosphorus compounds as polyolefin stabilizers 失效
    酚类磷化合物作为聚烯烃稳定剂

    公开(公告)号：US4246170A

    公开(公告)日：1981-01-20

    申请号：US4612

    申请日：1979-01-18

    申请人： Samuel Evans

    发明人： Samuel Evans

    IPC分类号： C07C67/00 ,  C07C69/96 ,  C07C301/00 ,  C07C301/02 ,  C07C303/06 ,  C07C303/08 ,  C07C303/24 ,  C07C305/22 ,  C07C325/00 ,  C07C329/00 ,  C07C329/04 ,  C07F9/08 ,  C07F9/12 ,  C07F9/145 ,  C07F9/32 ,  C07F9/40 ,  C07F9/48 ,  C08K5/00 ,  C08K5/10 ,  C08K5/13 ,  C08K5/36 ,  C08K5/51 ,  C08K5/52 ,  C08L23/00 ,  C08L101/00 ,  C09K15/08 ,  C09K15/14 ,  C09K15/32

    CPC分类号： C09K15/322 ,  C07C301/02 ,  C07C305/24 ,  C07C323/16 ,  C07C329/04 ,  C07F9/12 ,  C07F9/145 ,  C07F9/4075 ,  C07F9/4084 ,  C07F9/4875 ,  C08K5/005 ,  C08K5/51 ,  C09K15/14

    摘要： Phenols of the formula I ##STR1## wherein n has a value from 1 to 15,each of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 independently is a hydrogen atom, a C.sub.1 - .sub.18 -alkyl group, an aryl group, a C.sub.5 -C.sub.12 -cycloalkyl group or a C.sub.7 -C.sub.13 -aralkyl group,R.sub.5 is a hydrogen atom or a C.sub.1 -C.sub.18 -alkyl group,Y is a carbonyl, thiocarbonyl, sulphinyl, sulphonyl, -P(OR.sub.7)-, -P(.dbd.O) (OR.sub.7)-, -P(.dbd.O) (R.sub.7)- or -P(R.sub.7)- group, andR.sub.6 is a radical --CHR.sub.8 --CHR.sub.9 --S--CR.sub.10 R.sub.11 R.sub.12, wherein each of R.sub.8 and R.sub.9 independently is a hydrogen atom or a C.sub.1 -C.sub.6 -alkyl group, R.sub.10 is a hydrogen atom, a C.sub.1 -C.sub.19 -alkyl group, a C.sub.2 -C.sub.4 -alkenyl group or an aryl group, R.sub.11 is a hydrogen atom or a methyl group and R.sub.12 is a hydrogen atom or a methyl group, or, if R.sub.11 is a hydrogen atom, is a C.sub.2 -C.sub.6 -alkyl group, or, if R.sub.10 is a hydrogen atom, R.sub.11 and R.sub.12 together with the carbon atom to which they are attached represent a cycloalkyl group, or R.sub.10, R.sub.11 and R.sub.12 together with the carbon atom to which they are attached represent an aryl group, or if Y is a thiocarbonyl, sulphinyl or sulphonyl group,R.sub.6 can also be a hydrogen atom or a C.sub.1 -C.sub.18 -alkyl group or an aryl group, andR.sub.7 is a hydrogen atom, a C.sub.1 -C.sub.18 -alkyl group or an aryl group,as stabilizers for organic material.

    摘要翻译： 式I的苯酚（1）其中n具有1至15的数值，R 1，R 2，R 3和R 4各自独立地为氢原子，C 1 -C 18 - 烷基，芳基，C 5 -C 12 - 环烷基或C 7 -C 13 - 芳烷基，R 5为氢原子或C 1 -C 18烷基，Y为羰基，硫代羰基，亚磺酰基，磺酰基，-P（OR 7） - ， - P（= O）（OR 7） - ， - P（= O）（R 7） - 或-P（R 7） - 基团，R 6是基团-CHR 8 -CHR 9 -S-CR 10 R 11 R 12，其中R 8和R 9各自独立地为氢 原子或C1-C6-烷基，R10是氢原子，C1-C19 - 烷基，C2-C4-烯基或芳基，R11是氢原子或甲基，R12是氢 或者如果R 11为氢原子，则为C2-C6-烷基，或者，如果R10为氢原子，则R11和R12与它们所连接的碳原子一起代表环烷基 ，或R 10，R 11和R 12与它们所连接的碳原子一起表示芳基，或者如果Y是硫代羰基，则硫 正丁基或磺酰基，R 6也可以是氢原子或C 1 -C 18烷基或芳基，R 7是氢原子，C 1 -C 18烷基或芳基作为有机材料的稳定剂。

    Piperidine stabilizers
    64.
    发明授权
    Piperidine stabilizers 失效
    哌啶稳定剂

    公开(公告)号：US4197236A

    公开(公告)日：1980-04-08

    申请号：US931439

    申请日：1978-08-07

    申请人： Siegfried Rosenberger ,  Samuel Evans

    发明人： Siegfried Rosenberger ,  Samuel Evans

    IPC分类号： C07D211/46 ,  C07D211/58 ,  C08K5/00 ,  C08K5/34

    CPC分类号： C08K5/005 ,  C07C323/00 ,  C07D211/46 ,  C07D211/58

    摘要： Compounds of the general formula I ##STR1## or their acid addition salts in which one of R.sub.1 and R.sub.3 is --OH and the other is hydrogen and R.sub.2 denotes C.sub.1 -C.sub.12 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.6 -C.sub.10 -aryl or C.sub.7 -C.sub.9 -aralkyl and R.sub.4 and R.sub.5 are hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.6 -C.sub.10 -aryl or C.sub.7 -C.sub.9 -aralkyl and R.sub.6 denotes hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, phenyl or benzyl and R.sub.7 is hydrogen or C.sub.1 -C.sub.8 -alkyl and R.sub.8 is hydrogen, oxyl, C.sub.1 -C.sub.12 -alkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.4 -alkinyl, C.sub.2 -C.sub.21 -alkoxyalkyl, C.sub.7 -C.sub.8 -aralkyl, 2,3-epoxypropyl, an aliphatic acyl group with 1-4 C atoms or one of the groups --CH.sub.2 COOR.sub.9, --CH.sub.2 --CH(R.sub.10)--OR.sub.11, --COOR.sub.12 or -- CONHR.sub.12, in which R.sub.9 is C.sub.1 -C.sub.12 -alkyl, C.sub.3 -C.sub.6 -alkenyl, phenyl, C.sub.7 -C.sub.8 -aralkyl or cyclohexyl and R.sub.10 is hydrogen, methyl or phenyl and R.sub.11 denotes hydrogen or an aliphatic or aromatic, araliphatic or alicyclic acyl group with 1-18 C atoms, in which the aromatic part can optionally be substituted by chlorine, C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.8 -alkoxy and/or by hydroxyl, or a group ##STR2## and R.sub.12 denotes C.sub.1 -C.sub.12 -alkyl, cyclohexyl, phenyl or benzyl and X is --O-- or --NR.sub.13 --, in which R.sub.13 denotes hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or C.sub.7 -C.sub.9 -aralkyl and A is one of the groups --(C.sub.n H.sub.2n)--, which can optionally be interrupted by --S-- or ##STR3## in which n denotes 0 to 12 and Y is one of the groups ##STR4## in which R.sub.7, R.sub.8 and X have the meaning defined above and R.sub.14 denotes C.sub.1 -C.sub.12 -alkyl, phenyl or tolyl as stabilizers for organic material.

    摘要翻译： 通式I的化合物（I）或其酸加成盐，其中R 1和R 3中的一个是-OH，另一个是氢，R 2表示C 1 -C 12 - 烷基，C 5 -C 7 - 环烷基，C 6 -C 10 芳基或C 7 -C 9 - 芳烷基，R 4和R 5是氢，C 1 -C 12 - 烷基，C 5 -C 7 - 环烷基，C 6 -C 10 - 芳基或C 7 -C 9 - 芳烷基，R 6表示氢，C 1 -C 12烷基，C 5 C 7 - 环烷基，苯基或苄基，R 7是氢或C 1 -C 8 - 烷基，R 8是氢，氧基，C 1 -C 12 - 烷基，C 3 -C 6 - 烯基，C 3 -C 4 - 炔基，C 2 -C 21 - 烷氧基烷基， -C 1-8芳烷基，2,3-环氧丙基，具有1-4个C原子的脂族酰基或基团-CH 2 COOR 9，-CH 2 -CH（R 10）-OR 11，-COOR 12或-CONHR 12中的一个，其中R 9为C 1 C 12 - 烷基，C 3 -C 6 - 烯基，苯基，C 7 -C 8 - 芳烷基或环己基，R 10是氢，甲基或苯基，R 11表示氢或具有1-18个C原子的脂族或芳族，芳脂族或脂环族酰基， 其中芳族部分可以任选被氯，C 1 -C 4烷基或C 1 -C 8 - 烷氧基和/或被羟基取代，或基团 并且R 12表示C 1 -C 12烷基，环己基，苯基或苄基，X是-O-或-NR 13 - ，其中R 13表示氢，C 1 -C 12 - 烷基，C 5 -C 7 - 环烷基或C 7 -C 9 - 芳烷基和A是可以任选地被-S-或间隔的基团之一（C n H 2n） - ，其中n表示0至12，Y是其中R7，R8和 X具有上述定义，R 14表示C 1 -C 12 - 烷基，苯基或甲苯基作为有机材料的稳定剂。

    Novel phenol stabilizers
    65.
    发明授权
    Novel phenol stabilizers 失效
    新型苯酚稳定剂

    公开(公告)号：US4196119A

    公开(公告)日：1980-04-01

    申请号：US4611

    申请日：1979-01-18

    申请人： Samuel Evans

    发明人： Samuel Evans

    IPC分类号： C07C317/00 ,  C07F9/12 ,  C07F9/145 ,  C07F9/40 ,  C07F9/48 ,  C08K5/00 ,  C08K5/04 ,  C09K15/14 ,  C09K15/28 ,  C09K15/32 ,  C08K5/41 ,  C07C141/16 ,  C07C145/00

    CPC分类号： C07C305/00 ,  C07C323/00 ,  C07F9/12 ,  C07F9/145 ,  C07F9/4084 ,  C07F9/48 ,  C08K5/005 ,  C09K15/14 ,  C09K15/322

    摘要： Phenols of the formula I ##STR1## wherein n has a value from 1 to 15, each ofR.sub.1, R.sub.2, R.sub.3 and R.sub.4 independently is a hydrogen atom, a C.sub.1 -C.sub.18 -alkyl group, an aryl group, a C.sub.5 -C.sub.12 -cycloalkyl group or a C.sub.7 -C.sub.13 -aralkyl group,R.sub.5 is a hydrogen atom or a C.sub.1 -C.sub.18 -alkyl group,Y is a carbonyl, thiocarbonyl, sulphinyl, sulphonyl, P(OR.sub.7), --P(.dbd.O)(OR.sub.7)--, --P(.dbd.O)(R.sub.7)-- or --P(R.sub.7)-- group, andR.sub.6 is a radical --CHR.sub.8 --CHR.sub.9 --S--CR.sub.10 R.sub.11 R.sub.12, wherein each of R.sub.8 and R.sub.9 independently is a hydrogen atom or a C.sub.1 -C.sub.6 -alkyl group, R.sub.10 is a hydrogen atom, a C.sub.1 -C.sub.19 -alkyl group, a C.sub.2 -C.sub.4 -alkenyl group or an aryl group, R.sub.11 is a hydrogen atom or a methyl group and R.sub.12 is a hydrogen atom or a methyl group, or, if R.sub.11 is a hydrogen atom, is a C.sub.2 -C.sub.6 -alkyl group, or, if R.sub.10 is a hydrogen atom, R.sub.11 and R.sub.12 together with the carbon atom to which they are attached represent a cycloalkyl group, or R.sub.10, R.sub.11 and R.sub.12 together with the carbon atom to which they are attached represent an aryl group, or if Y is a thiocarbonyl, sulphinyl or sulphonyl group,R.sub.6 can also be a hydrogen atom or a C.sub.1 -C.sub.18 -alkyl group or an aryl group, andR.sub.7 is a hydrogen atom, a C.sub.1 -C.sub.18 -alkyl group or an aryl group, as stabilizers for organic material.

    摘要翻译： 式I的苯酚（I）其中n具有1至15的值，R 1，R 2，R 3和R 4各自独立地为氢原子，C 1 -C 18 - 烷基，芳基 ，C 5 -C 12 - 环烷基或C 7 -C 13 - 芳烷基，R 5为氢原子或C 1 -C 18烷基，Y为羰基，硫代羰基，亚磺酰基，磺酰基，P（OR 7） = O）（OR 7） - ， - P（= O）（R 7） - 或-P（R 7） - 基团，R 6是基团-CHR 8 -CHR 9 -S-CR 10 R 11 R 12，其中R 8和R 9各自独立地为 氢原子或C1-C6烷基，R10为氢原子，C1-C19 - 烷基，C2-C4-烯基或芳基，R11为氢原子或甲基，R12为 氢原子或甲基，或者如果R 11是氢原子，则为C 2 -C 6烷基，或者如果R 10是氢原子，则R 11和R 12与它们所连接的碳原子一起代表环烷基 基团或R 10，R 11和R 12与它们所连接的碳原子一起表示芳基，或者如果Y是硫代羰基，则 二苯基或磺酰基，R6也可以是氢原子或C1-C18烷基或芳基，R7是氢原子，C1-C18烷基或芳基作为有机材料的稳定剂。

    5-Triazin-2-yl phosphonates
    66.
    发明授权
    5-Triazin-2-yl phosphonates 失效

    公开(公告)号：US4151356A

    公开(公告)日：1979-04-24

    申请号：US840705

    申请日：1977-10-11

    申请人： Samuel Evans ,  Michael Rasberger

    发明人： Samuel Evans ,  Michael Rasberger

    IPC分类号： C08K5/00 ,  C07F9/6521 ,  C07F9/6558 ,  C08K5/53 ,  C08K5/5373 ,  C08L7/00 ,  C08L21/00 ,  C08L23/00 ,  C08L51/00 ,  C08L51/02 ,  C08L77/00 ,  C08L101/00 ,  C07D251/48

    CPC分类号： C07F9/65583 ,  C07F9/65216 ,  C08K5/5373

    摘要： A triazine of the formula I ##STR1## in which R.sub.1 and R.sub.2 independently of one another are hydrogen, C.sub.1 -C.sub.18 -alkyl, C.sub.6 -C.sub.18 -aryl, C.sub.7 -C.sub.18 -aralkyl or a radical of the formula II or III ##STR2## in which R.sub.3 is hydrogen or C.sub.1 -C.sub.8 -alkyl and R.sub.4 is hydrogen, oxyl, C.sub.1 -C.sub.12 -alkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.4 -alkinyl, C.sub.2 -C.sub.21 -alkoxyalkyl, C.sub.7 -C.sub.8 -aralkyl, 2,3-epoxypropyl, an aliphatic acyl group with 1-9 C atoms or one of the groups --CH.sub.2 COOR.sub.5, --CH.sub.2 --CH(R.sub.6)--OR.sub.7, --COOR.sub.8 or --CONHR.sub.8, in which R.sub.5 is C.sub.1 -C.sub.12 -alkyl, C.sub.3 -C.sub.6 -alkenyl, phenyl, C.sub.7 -C.sub.8 -aralkyl or cyclohexyl and R.sub.6 is hydrogen, methyl or phenyl and R.sub.7 denotes hydrogen, an aliphatic or aromatic, araliphatic or alicyclic acyl group with 1-18 C atoms, in which the aromatic part can optionally be substituted by chlorine, C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.8 -alkoxy and/or by hydroxyl, and R.sub.8 denotes C.sub.1 -C.sub.12 -alkyl, cyclohexyl, phenyl or benzyl and A is a radical of the formula IV or V ##STR3## in which R.sub.3 and R.sub.4 have the above meaning, n is 1, 2 or 3 and R.sub.9 is hydrogen or hydroxyl and Y is --O-- or --NR.sub.10 --, in which R.sub.10 is hydrogen, C.sub.1 -C.sub.18 -alkyl, C.sub.6 -C.sub.10 -aryl, C.sub.7 -C.sub.18 -aralkyl or a radical of the formula II with the above meaning, or A is --P(=O)(OR.sub.1)OR.sub.2, --S--R.sub.11, --NR.sub.12 R.sub.13 or --OR.sub.14, in which R.sub.1 and R.sub.2 have the above meaning, R.sub.11 is C.sub.1 -C.sub.18 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.6 -C.sub.10 -aryl, C.sub.7 -C.sub.9 -aralkyl or the group --(C.sub.p H.sub.2p)--CO--OR.sub.15, in which R.sub.15 is C.sub.1 -C.sub.18 -alkyl, and p denotes 1 to 6 and R.sub.12 and R.sub.13 independently of one another are hydrogen, C.sub.1 -C.sub.18 -alkyl, C.sub.3 -C.sub.4 -alkenyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.6 -C.sub.10 -aryl, C.sub.7 -C.sub.9 -aralkyl or a radical of the formula II with the above meaning, and R.sub.14 denotes C.sub.1 -C.sub.18 -alkyl, C.sub.6 -C.sub.10 -aryl or C.sub.7 -C.sub.9 -aralkyl, and B is a radical of the formula IV or V with the above meaning or is --P(=O)(OR.sub.1)OR.sub.2, in which R.sub.1 is a radical of the formula II or III with the above meaning and R.sub.2 has the above meaning, and its salts, as additives for stabilizing organic material.

    Nonylcyclohexylphosphite ester polyolefin stabilizers
    69.
    发明申请
    Nonylcyclohexylphosphite ester polyolefin stabilizers 失效
    壬基环己基亚磷酸酯聚烯烃稳定剂

    公开(公告)号：US20050222308A1

    公开(公告)日：2005-10-06

    申请号：US11087267

    申请日：2005-03-23

    申请人： Roswell King ,  Joseph Babiarz ,  Samuel Evans ,  Sai Shum

    发明人： Roswell King ,  Joseph Babiarz ,  Samuel Evans ,  Sai Shum

    IPC分类号： C08K5/34 ,  C08K5/524 ,  C08K5/527 ,  C09K21/00

    CPC分类号： C08K5/524 ,  C08K5/527 ,  C08L23/02

    摘要： The present invention discloses mono-, bis- and tris-nonylcyclohexylphosphite esters, polyolefin compositions stabilized against the deleterious effects of melt processing, heat aging and exposure to combustion products of natural gas which comprise the nonylcyclohexylphosphite esters as stabilizers, and a process towards stabilizing polyolefin compositions by incorporating in or applying thereto the nonylcyclohexylphosphite esters.

    摘要翻译： 本发明公开了单，双和三壬基环己基亚磷酸酯，稳定的聚烯烃组合物抵抗熔体加工，热老化和暴露于天然气的燃烧产物（其包含壬基环己基亚磷酸酯作为稳定剂）的有害作用，以及稳定聚烯烃 通过在其中掺入或施加于其上的壬基环己基亚磷酸酯的组合物。