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    Siloxane monomers and oligomers
    76.
    发明授权
    Siloxane monomers and oligomers 有权
    硅氧烷单体和低聚物

    公开(公告)号：US07534901B2

    公开(公告)日：2009-05-19

    申请号：US10559847

    申请日：2004-04-16

    Applicant: James V. Crivello

    Inventor： James V. Crivello

    IPC: C07F7/08

    CPC classification number: C07F7/1892 ,  B33Y70/00 ,  C07F7/0874 ,  C08G77/04 ,  C08G77/045 ,  C08G77/38 ,  C09D183/06

    Abstract: A process for preparing α, ω-functional siloxane compounds in a purity of greater than or equal to 90% includes contacting a monohydrosiloxane compound of formula 1 with oxygen in the presence of a platinum group catalyst, without adding water, to form the α, ω-functional siloxane compound in a purity of greater than or equal to 90%; wherein n is 0, 1, or 2; R1 is fluoroethyl, methyl or phenyl; and R2 is substituted alkyl, epoxyalkyl, oxetanylalkyl, substituted oxaalkyl, epoxyoxaalkyl, oxetanyloxaalkyl, alkenyl, alkylalkoxysilyl, substituted alkylaryl, and substituted arylalkyl.

    Abstract translation: 制备纯度大于或等于90％的α，ω-官能的硅氧烷化合物的方法包括在铂族催化剂的存在下使式1的一氢硅氧烷化合物与氧接触而不添加水，形成α， 具有大于或等于90％纯度的ω-官能硅氧烷化合物; 其中n为0,1或2; R1是氟乙基，甲基或苯基; 环烷氧基烷基，环氧基烷基，氧杂环氧烷基，烯基，烷基烷氧基甲硅烷基，取代烷基芳基和取代芳基烷基。

    Diaryliodonium salt catalysts made from iodotoluene and a method for preparing them
    77.
    发明授权
    Diaryliodonium salt catalysts made from iodotoluene and a method for preparing them 失效
    由碘甲苯制备的二芳基碘盐催化剂及其制备方法

    公开(公告)号：US06632960B2

    公开(公告)日：2003-10-14

    申请号：US10177549

    申请日：2002-06-21

    Applicant: James V. Crivello ,  Georg Feldmann-Krane ,  Sascha Oestreich

    Inventor： James V. Crivello ,  Georg Feldmann-Krane ,  Sascha Oestreich

    IPC: C07C30900

    CPC classification number: C07C43/23 ,  C07F5/027 ,  C07F9/902

    Abstract: Diaryliodonium salts are disclosed, as well as a method for preparing them, in which one of the aryl groups bonded to the positively-charged iodine ion contains a methyl substituent, and the other one contains a hydroxyl-substituted alkoxy group. The salts are synthesized from (o, m, or p)-iodotoluene, as opposed to iodobenzene, and therefore do not pose a carcinogenic risk. In addition, the present salts are unexpectedly more soluble in most organic solvents, as well as in nonpolar monomers, than the corresponding benzene catalysts. The salts are useful as cationic photoinitiators, cationic thermal initiators (often combined with a cocatalyst, e.g. copper), and as starting materials in the synthesis of urethane-containing iodonium salts.

    Abstract translation: 公开了二芳基碘鎓盐及其制备方法，其中与正电荷的碘离子键合的一个芳基含有甲基取代基，另一个含有羟基取代的烷氧基。 盐与（o，m或p） - 碘甲苯合成，而不是碘苯，因此不会造成致癌风险。 此外，与相应的苯催化剂相比，本发明的盐在大多数有机溶剂以及非极性单体中意外地更易溶。 这些盐可用作阳离子光引发剂，阳离子热引发剂（通常与助催化剂例如铜组合）和作为合成含氨基甲酸酯的碘鎓盐的起始原料。

    Epoxidation of ricinic compounds using a phase-transfer catalyst
    78.
    发明授权
    Epoxidation of ricinic compounds using a phase-transfer catalyst 失效
    使用相转移催化剂对蓖麻毒素化合物进行环氧化

    公开(公告)号：US06414168B1

    公开(公告)日：2002-07-02

    申请号：US09473116

    申请日：1999-12-28

    Applicant: James V. Crivello ,  Srinivasan Chakrapani

    Inventor： James V. Crivello ,  Srinivasan Chakrapani

    IPC: C07D30112

    CPC classification number: C07D301/12 ,  C07D303/42

    Abstract: Unsaturated or polyunsaturated, conjugated or nonconjugated hydrocarbons are reacted with an oxidizing agent including hydroperoxides and monopersulfate compounds in the presence of phase-transfer catalysts. Suitable hydrocarbons include ricinic compounds such as castor oil and dehydrated castor oil. The phase-transfer catalysts include novel tungsten peroxo complexes, such as quaternary ammonium tetrakis (diperoxotungsto) phosphates, and crown ethers. Other additives utilized include pH buffers and alkaline compounds including alkali metal and alkaline earth metal carbonates, and solvents.

    Abstract translation: 在相转移催化剂存在下，不饱和或多不饱和的共轭或非共轭烃与包括氢过氧化物和单过硫酸盐化合物在内的氧化剂反应。 合适的烃包括蓖麻油和蓖麻油等蓖麻油。 相转移催化剂包括新型钨过氧配合物，例如季铵四（二过氧钨）磷酸盐和冠醚。 所用的其它添加剂包括pH缓冲剂和包括碱金属和碱土金属碳酸盐在内的碱性化合物和溶剂。

    Photopolymerizible compositions containing cycloaliphatic epoxyalcohol monomers
    79.
    发明授权
    Photopolymerizible compositions containing cycloaliphatic epoxyalcohol monomers 有权
    含有脂环族环氧醇单体的光聚合组合物

    公开(公告)号：US06268403B1

    公开(公告)日：2001-07-31

    申请号：US09637954

    申请日：2000-08-11

    Applicant: James V. Crivello

    Inventor： James V. Crivello

    IPC: C08G5920

    CPC classification number: C08G59/68 ,  B33Y70/00 ,  C08G65/105 ,  C08G65/22

    Abstract: A method of accelerating the cure rate of an epoxy curing composition includes combining a cycloaliphatic epoxyalcohol monomer, a non-hydroxyl-containing epoxy monomer and a cationic photoinitiator to form an epoxy curing composition, and exposing the curing composition to a source of radiation. The resulting polymers and copolymers are branched polyethers containing hydroxyl functionality.

    Abstract translation: 一种加速环氧固化组合物固化速率的方法包括组合环脂族环氧醇单体，非含羟基环氧单体和阳离子光引发剂以形成环氧固化组合物，并将固化组合物暴露于辐射源。 所得的聚合物和共聚物是含有羟基官能团的支链聚醚。

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