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    Oxidative process for the preparation of copper quinolinate
    1.
    发明授权
    Oxidative process for the preparation of copper quinolinate 失效
    用于制备喹啉铜的氧化工艺

    公开(公告)号：US4420616A

    公开(公告)日：1983-12-13

    申请号：US236945

    申请日：1981-02-20

    申请人： Seishi Ikegami ,  Yoshihiro Hatano

    发明人： Seishi Ikegami ,  Yoshihiro Hatano

    IPC分类号： C07D215/30 ,  C07D213/79 ,  C07D213/80 ,  C07D213/803 ,  C07D213/807 ,  C07D213/87

    CPC分类号： C07D213/803 ,  C07D213/80

    摘要： A process for the preparation of copper quinolinate in which quinoline is oxidized by hydrogen peroxide in sulfuric acid in the presence of copper sulfate wherein the reaction is carried out at a pressure of less than 400 mm Hg. The reduced pressure enables the reaction to be performed at higher temperatures and with greater control; also the reaction time is shortened and the yield improved.Copper quinolinate is used to prepare quinolinic acid which is the starting material for some chromogenic materials used in the pressure-sensitive record material field.

    摘要翻译： 一种制备喹啉铜的方法，其中喹啉在硫酸铜存在下用硫酸中的过氧化氢氧化，其中反应在小于400mmHg的压力下进行。 减压使反应在更高的温度和更好的控制下进行; 反应时间也缩短，产率提高。 使用喹啉酸钾制备作为压敏记录材料领域中使用的一些显色材料的起始原料的喹啉酸。

    Process for the preparation of copper quinolinate
    2.
    发明授权
    Process for the preparation of copper quinolinate 失效
    制备喹啉铜的方法

    公开(公告)号：US4316026A

    公开(公告)日：1982-02-16

    申请号：US177694

    申请日：1980-08-12

    申请人： Yoshihiro Hatano ,  Seishi Ikegami ,  Kenji Itoh ,  Mansuke Matsumoto

    发明人： Yoshihiro Hatano ,  Seishi Ikegami ,  Kenji Itoh ,  Mansuke Matsumoto

    IPC分类号： C07D213/80 ,  C07D213/807 ,  C07F1/08

    CPC分类号： C07D213/80

    摘要： A process for the preparation of copper quinolinate in which quinoline is oxidized by hydrogen peroxide in 10 to 30% sulfuric acid in the presence of copper sulfate at a temperature of 55.degree. to 75.degree. C., the molar ratio of sulfuric acid to quinoline being greater than 1:1. The concentration and amount of sulfuric acid enable greater control of the reaction temperature and result in copper quinolate in improved yield and purity.Copper quinolinate is used to prepare quinolinic acid which is the starting material for some chromogenic materials used in the pressure-sensitive record material field.

    摘要翻译： 一种制备喹喔啉的方法，其中在硫酸铜存在下，在55〜75℃的温度下，在10〜30％的硫酸中，喹啉被过氧化氢氧化，硫酸与喹啉的摩尔比为 大于1：1。 硫酸的浓度和用量可以更好地控制反应温度，从而提高了产品和纯度。 使用喹啉酸钾制备作为压敏记录材料领域中使用的一些显色材料的起始原料的喹啉酸。

    Process for preparation of 2-(amylbenzoyl)benzoic acid
    3.
    发明授权
    Process for preparation of 2-(amylbenzoyl)benzoic acid 失效
    2-（戊基苯甲酰基）苯甲酸的制备方法

    公开(公告)号：US4087458A

    公开(公告)日：1978-05-02

    申请号：US794620

    申请日：1977-05-06

    申请人： Fumitoshi Emori ,  Yasuhisa Iwasaki ,  Takao Yoshimura

    发明人： Fumitoshi Emori ,  Yasuhisa Iwasaki ,  Takao Yoshimura

    IPC分类号： C07C51/373 ,  C07C65/20

    CPC分类号： C07C51/373

    摘要： This invention relates to an improvement in the process for preparation of 2-(amylbenzoyl)benzoic acid containing a high percentage of 2-(t-amylbenzoyl)benzoic acid. More particularly it relates to a process for preparation of 2-(amylbenozyl)benzoic acid wherein said 2-(amylbenzoyl)benzoic acid is prepared by reacting t-amylbenzene with phthalic anhydride in the presence of Lewis acid, characterized by that 2-(amylbenzoyl)benzoic acid containing a high percentage of 2-(t-amylbenzoyl)benzoic acid is produced by suppressing the undesirable isomerization reaction of the amyl radical by applying one of the means selected from the group consisting of the means of introducing an inert gas into the reaction system and the means of reducing the pressure of the reaction system. 2-(Amylbenzoyl)benzoic acid is a compound useful as the starting material of preparation of 2-amylanthraquinone which is an effective organic catalyst in the manufacture of hydrogen peroxide.

    摘要翻译： 本发明涉及含有高百分比的2-（叔戊基苯甲酰基）苯甲酸的2-（戊基苯甲酰基）苯甲酸的制备方法的改进。 更具体地说，涉及制备2-（戊基苯甲酰基）苯甲酸的方法，其中所述2-（戊基苯甲酰基）苯甲酸通过在路易斯酸存在下使叔戊基苯与邻苯二甲酸酐反应来制备，其特征在于2-（戊基苯甲酰基） ）苯甲酸，其含有高百分比的2-（叔戊基苯甲酰基）苯甲酸是通过将选自由惰性气体引入惰性气体的方法中选择的一种方法抑制到所需的戊基自由基的不期望的异构化反应 反应体系和降低反应体系压力的手段。 2-（戊基苯甲酰基）苯甲酸是可用作制备过氧化氢的有效有机催化剂的2-戊基蒽醌的起始原料的化合物。

    Naphthalocyanine compounds
    5.
    再颁专利
    Naphthalocyanine compounds 失效
    萘酞菁化合物

    公开(公告)号：USRE34480E

    公开(公告)日：1993-12-14

    申请号：US940309

    申请日：1992-09-03

    申请人： Tsunehito Eda

    发明人： Tsunehito Eda

    IPC分类号： C09B47/067 ,  C09B47/04

    CPC分类号： C09B47/0673

    摘要： Naphthalocyanine compounds represented by the general formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4, which may be the same or different, are each a straight chain or branched chain alkyl group of 5 to 12 carbon atoms and M is a metal selected from the group consisting of Cu, Ni, Mg, Pb, Pd, V, Co, .[.Nb,.]. Al, Sn, In, Fe and Ge, or its oxide, chloride or bromide, are bluish green or green crystals and are superior in absorption or near infrared rays of 750 and 850 nm, highly resistant to light, heat, acids and alkalis, soluble in organic acids, liquid crystals and resins, and accordingly are very useful as a dyestuff capable of absorbing near infrared rays.

    Lactones of quinoline carboxylic acids
    6.
    发明授权
    Lactones of quinoline carboxylic acids 失效
    喹啉羧酸的内酯

    公开(公告)号：US4200751A

    公开(公告)日：1980-04-29

    申请号：US853781

    申请日：1977-11-21

    申请人： Seiji Ikegami ,  Yoshihiro Hatano

    发明人： Seiji Ikegami ,  Yoshihiro Hatano

    IPC分类号： B41M5/327 ,  C07D491/048 ,  C07D491/14

    CPC分类号： B41M5/327

    摘要： Lactone electron donative color-forming agents of quinoline-carboxylic acid are disclosed having the general formulae (I) and (II) ##STR1## wherein A and B represent a variety of chemical moieties, X represents halo- or nitro- and n.sup.1 is an integer of 0-4. The color-forming agents are useful in recording materials of the pressure-sensitive and heat-sensitive varieties, and the like.

    摘要翻译： 公开了具有通式（I）和（II）的化合物，其中A和B代表多种化学部分，X代表卤代或硝基的喹啉羧酸的内酯电子给体形成剂 - 和n1是0-4的整数。 成色剂可用于记录压敏和热敏感品种的材料等。

    Naphthalocyanine compounds
    7.
    发明授权
    Naphthalocyanine compounds 失效
    萘酞菁化合物

    公开(公告)号：US4622179A

    公开(公告)日：1986-11-11

    申请号：US631700

    申请日：1984-07-17

    申请人： Tsunehito Eda

    发明人： Tsunehito Eda

    IPC分类号： C09B47/04 ,  C09B47/067

    CPC分类号： C09B47/045 ,  C09B47/0673

    摘要： Naphthalocyanine compounds represented by the general formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4, which may be the same or different, are each a straight chain or branched chain alkyl group of 5 to 12 carbon atoms and M is a metal selected from the group consisting of Cu, Ni, Mg, Pb, Pd, V, Co, Nb, Al, Sn, In, Fe and Ge, or its oxide, chloride or bromide, are bluish green or green crystals and are superior in absorption of near infrared rays of 750 to 850 nm, highly resistant to light, heat, acids and alkalis, soluble in organic acids, liquid crystals and resins, and accordingly are very useful as a dyestuff capable of absorbing near infrared rays.

    摘要翻译： 由通式表示的萘酞菁化合物，其中R1，R2，R3和R4可以相同或不同，分别为5-12个碳原子的直链或支链烷基，M是选自 由Cu，Ni，Mg，Pb，Pd，V，Co，Nb，Al，Sn，In，Fe和Ge或其氧化物，氯化物或溴化物组成的组是蓝绿色或绿色晶体， 750至850nm的近红外线，对光，热，酸和碱的耐受性高，可溶于有机酸，液晶和树脂，因此作为能够吸收近红外线的染料非常有用。