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1.发明授权
公开(公告)号：US5085794A
公开(公告)日：1992-02-04
申请号：US514444
申请日：1990-04-25
IPC分类号： C02F5/14
摘要： A phosphinate containing composition which has as its major ingredient more than 32 mole percent of a phosphinicosuccinic acid oligomer having the probable structural formula: ##STR1## M is H, Na, K, NH.sub.4, or mixtures thereof; and m and n are either 0 or a small whole number with the proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译： 含有次膦酸盐的组合物，其主要成分为具有32摩尔％以下具有可能结构式的次膦酸琥珀酸低聚物：H，Na，K，NH 4或其混合物; 并且m和n为0或小整数，条件是m或n为小整数，m + n的和大于2。
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公开(公告)号：US20100298594A1
公开(公告)日：2010-11-25
申请号：US12468585
申请日：2009-05-19
申请人： Larry E. Brammer, JR. , Barbara E. Fair , Cheng-Sung Huang , Linh Quach , Peter E. Reed , Leonard M. Ver Vers
发明人： Larry E. Brammer, JR. , Barbara E. Fair , Cheng-Sung Huang , Linh Quach , Peter E. Reed , Leonard M. Ver Vers
IPC分类号： C07C67/03
CPC分类号： C07C213/06 , C07C219/08
摘要： A method and apparatus for preparing a N,N-dialkylaminoalkyl acrytate in a continuous transesterification reaction. The reaction involves adding alkyl acrylates such as methacrylate or ethacrylate to a reboiler mechanism and efficiently removing alcohol co-products. Because the reaction is continuous, the alkyl acrylates can be added as needed to increase output, decrease output, or fine-tune the reaction dynamics. An entrainer is used to form a volatile azeotrope which contains both alcohol and entrainer and which is easily removed from the reboiler mechanism. This method reduces the amount of entrainer needed per unit of alkyl acrylate used and eliminates any need to purify the end product from entrainer contamination of the resulting N,N-dialkylaminoalkyl acrylate product.
摘要翻译： 在连续酯交换反应中制备N，N-二烷基氨基烷基丙烯酸酯的方法和装置。 该反应包括将丙烯酸烷基酯如甲基丙烯酸酯或乙基丙烯酸酯加入到再沸器机理中并有效地除去醇共同产物。 因为反应是连续的，所以可以根据需要添加丙烯酸烷基酯以增加产量，降低产量或微调反应动力学。 使用夹带剂形成含有醇和夹带剂并易于从再沸器机构中除去的挥发性共沸物。 该方法减少了每单位使用的丙烯酸烷基酯所需的夹带剂量，并且消除了任何需要净化最终产物对所得的N，N-二烷基氨基烷基丙烯酸酯产物的夹带剂污染。
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公开(公告)号：US08247597B2
公开(公告)日：2012-08-21
申请号：US12691159
申请日：2010-01-21
申请人： Barbara E. Fair , Peter E. Reed , Leonard M. Ver Vers , Larry E. Brammer, Jr. , Charles J. Holada , Cheng-Sung Huang , Kailas B. Sawant
发明人： Barbara E. Fair , Peter E. Reed , Leonard M. Ver Vers , Larry E. Brammer, Jr. , Charles J. Holada , Cheng-Sung Huang , Kailas B. Sawant
IPC分类号： C07C69/52
CPC分类号： C07C213/08 , C07C219/08
摘要： The invention provides a method of continuously producing high quality quaternized N,N-dialkylaminoethyl (meth)acrylates (DMAEA.MCQ) that has a long shelf life and which is stable in water. The method involves placing starting materials into a continuously stirred tank reactor in the presence of less than 6% water. This low amount of water causes two liquid phases to form and prevents unwanted side reactions. The denser liquid phase contains DMAEA.MCQ and the lighter phase contains the starting materials. Liquid from the denser phase is removed from a position where little of the lighter phase has been mixed in. The removed liquid then has any last traces of the starting materials reacted into DMAEA.MCQ and strips away any starting materials with a gas flow. The resulting liquid is high purity DMAEA.MCQ. Water can then safely be added to ease in the transport and use of the produced DMAEA.MCQ.
摘要翻译： 本发明提供了一种连续生产高效季铵化N（N-二烷基氨基乙基（甲基）丙烯酸酯（DMAEA.MCQ））的方法，其具有长的保质期，并且在水中稳定。 该方法包括在少于6％的水的存在下将原料放入连续搅拌的罐式反应器中。 这种少量的水导致形成两个液相并防止不期望的副反应。 密度较高的液相含有DMAEA.MCQ，较浅的相含有原料。 来自较稠相的液体从少量较轻相混合的位置被除去。然后，除去的液体具有反应成DMAEA.MCQ的起始材料的任何最后痕迹，并用气流剥离任何起始材料。 所得液体为高纯度DMAEA.MCQ。 然后可以安全地加入水，以便于运输和使用生产的DMAEA.MCQ。
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公开(公告)号：US4883600A
公开(公告)日：1989-11-28
申请号：US256541
申请日：1988-10-12
摘要： The soluble manganese species can be maintained in aqueous systems in the presence of halogen species by treating the waters with certain water-soluble, nitrogen containing compositions.
摘要翻译： 通过用某些水溶性含氮组合物处理水，可以在卤素物质的存在下将可溶性锰物质保持在含水体系中。
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公开(公告)号：US07829738B1
公开(公告)日：2010-11-09
申请号：US12468585
申请日：2009-05-19
申请人： Larry E. Brammer, Jr. , Barbara E. Fair , Cheng-Sung Huang , Linh Quach , Peter E. Reed , Leonard M. Ver Vers
发明人： Larry E. Brammer, Jr. , Barbara E. Fair , Cheng-Sung Huang , Linh Quach , Peter E. Reed , Leonard M. Ver Vers
IPC分类号： C07C69/52
CPC分类号： C07C213/06 , C07C219/08
摘要： A method and apparatus for preparing a N,N-dialkylaminoalkyl acrylate in a continuous transesterification reaction. The reaction involves adding alkyl acrylates such as methacrylate or ethacrylate to a reboiler mechanism and efficiently removing alcohol co-products. Because the reaction is continuous, the alkyl acrylates can be added as needed to increase output, decrease output, or fine-tune the reaction dynamics. An entrainer is used to form a volatile azeotrope which contains both alcohol and entrainer and which is easily removed from the reboiler mechanism. This method reduces the amount of entrainer needed per unit of alkyl acrylate used and eliminates any need to purify the end product from entrainer contamination of the resulting N,N-dialkylaminoalkyl acrylate product.
摘要翻译： 在连续酯交换反应中制备丙烯酸N，N-二烷基氨基烷基酯的方法和装置。 该反应包括将丙烯酸烷基酯如甲基丙烯酸酯或乙基丙烯酸酯加入到再沸器机理中并有效地除去醇共同产物。 因为反应是连续的，所以可以根据需要添加丙烯酸烷基酯以增加产量，降低产量或微调反应动力学。 使用夹带剂形成含有醇和夹带剂并易于从再沸器机构中除去的挥发性共沸物。 该方法减少了每单位使用的丙烯酸烷基酯所需的夹带剂量，并且消除了任何需要净化最终产物对所得的N，N-二烷基氨基烷基丙烯酸酯产物的夹带剂污染。
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公开(公告)号：US4963267A
公开(公告)日：1990-10-16
申请号：US501438
申请日：1990-03-26
摘要： The precipitate species of manganese in the presence of an oxidative condition in the waters of an aqueous system can be diminished by treating such waters with certain amide-containing polymer.
摘要翻译： 通过用某些含酰胺的聚合物处理这种水，在含水体系的水中存在氧化条件下的锰的沉淀物质可以减少。
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公开(公告)号：US20110178327A1
公开(公告)日：2011-07-21
申请号：US12691159
申请日：2010-01-21
申请人： Barbara E. Fair , Peter E. Reed , Leonard M. Ver Vers , Larry E. Brammer, JR. , Charles J. Holada , Cheng-Sung Huang , Kailas B. Sawant
发明人： Barbara E. Fair , Peter E. Reed , Leonard M. Ver Vers , Larry E. Brammer, JR. , Charles J. Holada , Cheng-Sung Huang , Kailas B. Sawant
IPC分类号： C07C227/00
CPC分类号： C07C213/08 , C07C219/08
摘要： The invention provides a method of continuously producing high quality quaternized N,N-dialkylaminoethyl (meth)acrylates (DMAEA.MCQ) that has a long shelf life and which is stable in water. The method involves placing starting materials into a continuously stirred tank reactor in the presence of less than 6% water. This low amount of water causes two liquid phases to form and prevents unwanted side reactions. The denser liquid phase contains DMAEA.MCQ and the lighter phase contains the starting materials. Liquid from the denser phase is removed from a position where little of the lighter phase has been mixed in. The removed liquid then has any last traces of the starting materials reacted into DMAEA.MCQ and strips away any starting materials with a gas flow. The resulting liquid is high purity DMAEA.MCQ. Water can then safely be added to ease in the transport and use of the produced DMAEA.MCQ.
摘要翻译： 本发明提供了一种连续生产高效季铵化N（N-二烷基氨基乙基（甲基）丙烯酸酯（DMAEA.MCQ））的方法，其具有长的保质期，并且在水中稳定。 该方法包括在少于6％的水的存在下将原料放入连续搅拌的罐式反应器中。 这种少量的水导致形成两个液相并防止不期望的副反应。 密度较高的液相含有DMAEA.MCQ，较浅的相含有原料。 来自较稠相的液体从少量较轻相混合的位置被除去。然后，除去的液体具有反应成DMAEA.MCQ的起始材料的任何最后痕迹，并用气流剥离任何起始材料。 所得液体为高纯度DMAEA.MCQ。 然后可以安全地加入水，以便于运输和使用生产的DMAEA.MCQ。
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公开(公告)号：US5023000A
公开(公告)日：1991-06-11
申请号：US521627
申请日：1990-05-10
摘要： Calcium carbonate scale is controlled by treating calcium carbonate containing waters with a predominantly phosphinate containing composition where has as its major ingredient more than 32 mole percent of a phosphinicosuccinic acid oligomer having the probable structural formula . ##STR1## M is H, Na, K, NH.sub.4, or mixtures thereof; and m and n are either 0 or a small whole number with proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译： 通过用主要含有次膦酸盐的组合物处理含碳酸钙的水，以其主要成分超过32摩尔％的具有可能结构式的次膦酸琥珀酸低聚物来控制碳酸钙垢。 M是H，Na，K，NH 4或其混合物; m和n为0或小整数，条件是m或n为小整数，m + n之和大于2。
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