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公开(公告)号：US4728036A
公开(公告)日：1988-03-01
申请号：US931557
申请日：1986-11-17
CPC分类号： F23D1/005 , B05B7/0433 , B05B7/1633
摘要： An atomizing nozzle assembly is provided having an outwardly diverging frustrum of a cone shaped, deflector core of wear resistant ceramic, a nozzle rim of wear resistant ceramic encircling the core and coextensive with a downstream portion thereof to form a mixing zone therewith for receiving liquid-to-be-atomized therein from an unobstructed passage and atomizing fluid directing the liquid-to-be-atomized away from the core. The mixing zone leads to a nozzle orifice outlet. The core is mounted in a core holder and is adjustable by a screw thread, in close proximity to the mixing zone, to adjust the width of the mixing zone. The liquid-to-be-atomized (e.g. a coal slurry fuel) and the atomizing fluid (e.g. air) are fed along coaxial tubes which are slidably mounted by glands to accommodate differential expansions.
摘要翻译： 提供了一种雾化喷嘴组件，其具有锥形的耐磨陶瓷的锥形偏转芯的向外发散的锥形，环绕芯的耐磨陶瓷的喷嘴边缘并与其下游部分共同延伸以形成其中的混合区， 从不受阻碍的通道将其雾化，并将雾化的液体引导离开核心。 混合区通向喷嘴孔出口。 芯部安装在芯保持器中，并且可以通过紧邻混合区域的螺纹进行调节，以调节混合区域的宽度。 待雾化的液体（例如煤浆燃料）和雾化流体（例如空气）沿着同轴管供给，所述同轴管可由压盖可滑动地安装以适应差异扩展。
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2.发明授权
公开(公告)号：US4601729A
公开(公告)日：1986-07-22
申请号：US656675
申请日：1984-10-01
IPC分类号： C10L1/32
CPC分类号： C10L1/324
摘要： An aqueous phase continuous, fuel slurry is claimed, and its method of production from agglomerates consisting essentially of carbonaceous particles, agglomerating oil and residual water. The slurry may be formed by thoroughly mixing with agglomerates an agglomerate dispersing and coal/oil/water system interfacial tension reducing agent with the agglomerates so that the agglomerates are broken down and an aqueous phase continuous fuel slurry is formed containing residual, oil produced flocs from the agglomerates and having an oil content of the fuel slurry no greater than 10 weight % of the solids content of the fuel slurry. The solids content of the fuel slurry is in the range of the order of 50 weight % and of the order of 80 weight % of the total weight of the fuel slurry, and is preferably in the range of the order of 65 weight % to of the order of 70 weight %. Examples of interfacial tension reducing agents are ethanol, methanol, glycol, butyl alcohol, isopropyl alcohol, lauryl sulfonates, alkyl sulfonates, lignosulfonates, sodium oleate, nonyl-phenolethoxylates, and soaps. With fuel slurries according to the invention, there may be very slow sedimentary consolidation of the carbonaceous particles, but when it does occur there is no difficulty in re-mixing the constituents into a slurry because the residual aggregates or flocs cause the carbonaceous particles to pack down to a porous bed.
摘要翻译： 要求保护水相连续的燃料浆料，以及其基本上由碳质颗粒，附聚油和残余水组成的附聚物的生产方法。 浆料可以通过与附聚物与附聚物分散剂和煤/油/水系统界面张力降低剂与附聚物充分混合而形成，使得附聚物被分解，形成水相连续燃料浆料，其含有残留的，产生油的絮凝物 所述附聚物并且所述燃料浆料的油含量不大于所述燃料浆料的固体含量的10重量％。 燃料浆料的固体含量在燃料浆料的总重量的50重量％数量级和大约80重量％的范围内，优选在65重量％以下的范围内 订单为70重量％。 界面张力降低剂的实例是乙醇，甲醇，乙二醇，丁醇，异丙醇，月桂基磺酸盐，烷基磺酸盐，木质素磺酸盐，油酸钠，壬基 - 苯基乙氧基化物和皂。 根据本发明的燃料浆料，碳质颗粒的沉积固结可能非常缓慢，但是当确实发生时，由于残留的聚集体或絮凝物使碳质颗粒堆积，所以将组分重新混合成浆料是不困难的 到多孔床。
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公开(公告)号：US4033729A
公开(公告)日：1977-07-05
申请号：US680592
申请日：1976-04-26
申请人： Charles E. Capes , Rene J. Germain , Allan E. McIlhinney , Ira E. Puddington , Aurelio F. Sirianni
发明人： Charles E. Capes , Rene J. Germain , Allan E. McIlhinney , Ira E. Puddington , Aurelio F. Sirianni
CPC分类号： C10L9/00
摘要： A high proportion of the inorganic materials, (ash) content is removed from coal by providing the coal as a suspension with a liquid hydrocarbon oil, mixing an aqueous agglomerating liquid comprising water with the suspension, mixing a particulate material having a hydrophilic surface that is readily wetted by liquid water with the suspension, agitating the suspension to agglomerate the ash, and then separating the ash from the remainder. The particulate material having a hydrophilic surface may be ash, agglomerated silica flour, coarse silica chips, limestone or peat moss, and a binder for the ash may be dispersed or dissolved in the aqueous agglomerating liquid. In some instances the coal may be initially in the form of an aqueous suspension, and the coal can either be agglomerated from the suspendant by using a portion of the liquid hydrocarbon oil and then adding the remainder, or filtered therefrom and then the filter cake mixed with the liquid hydrocarbon oil.
摘要翻译： 通过提供作为液体烃油的悬浮液的煤，将包含水的聚集液体与悬浮液混合，将具有亲水性表面的颗粒材料混合在一起，从煤中除去高比例的（灰分） 容易地用液体水用悬浮液润湿，搅拌悬浮液以使灰分聚集，然后将灰分与其余部分分离。 具有亲水性表面的颗粒材料可以是灰分，附聚二氧化硅粉，粗二氧化硅碎片，石灰石或泥炭苔，并且用于灰分的粘合剂可以分散或溶解在含水附聚液中。 在一些情况下，煤可以初始为水性悬浮液的形式，并且煤可以通过使用一部分液体烃油从悬浮液中聚集，然后加入剩余物，或从其中过滤，然后将滤饼混合 与液体烃油。
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公开(公告)号：US3969103A
公开(公告)日：1976-07-13
申请号：US528541
申请日：1974-11-29
CPC分类号： C22B1/2406
摘要： Ball agglomerated particulate material is produced by comminuting the material to produce coarse particles having a size predominantly within the range 0.3 mm to 1.4 mm, and fines, then feeding the coarse particles, fines and an agglomerating liquid into a rotating ball agglomerating mill with the volume fraction of the coarse particles being 20% to 80% by volume of the total solids feed to the mill, continuing rotation of the mill until agglomerated balls are produced having a continuous network of fines interspersed with the coarse particles such that: ##EQU1## WHERE .epsilon. = THE POROSITY OF THE AGGLOMERATES,.epsilon..sub.o = the porosity of similar agglomerates formed entirely of the fines, m is the above mentioned volume fraction of coarse particles, andK = 0.7 to 1.0,And removing the agglomerates thus formed from the ball agglomerating mill. It has been found, according to the invention, that the proportion of coarse particles to fines can be increased, and that the size of the coarse particles can be increased beyond the limits believed practical to obtain ball agglomerates of adequate green strength, and this has the advantage of reducing the costs involved in comminuting the material.
摘要翻译： 球团聚颗粒材料是通过粉碎材料制成的，以产生尺寸主要在0.3mm至1.4mm范围内的粗颗粒和细粉，然后将粗颗粒，细粒和附聚液输送到具有体积的旋转球团聚磨 粗颗粒的分数为总固体进料量的20％至80％（体积），继续旋转研磨机，直到产生具有连续粗粉末颗粒的连续网格，使得：1-ε1 - εε1 = KεεεO 1 -m其中ε= AGGLOMERATES的孔隙度，ε= O =形成细粒度的类似粒子的孔隙度，M是上述上述粒子数的分数，K = 0.7 到1。
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公开(公告)号：US4758332A
公开(公告)日：1988-07-19
申请号：US083355
申请日：1987-08-10
摘要： In a method of agglomerating carbonaceous coal comprising first agglomerating impurity liberated carbonaceous coal, from an impurity liberated coal slurry, with agglomerating oil to form open structured, chain-like, micro-agglomerates and then forming relatively larger, less open structured more robust agglomerates from a portion of the slurry to provide a mixture of micro-agglomerates, relatively larger, more robust agglomerates, water and any inorganic impurities that may be present. The relatively larger, more robust agglomerates are screened and then the micro-agglomerates are separated using an aerating, skimmer tank leaving an inorganic impurity laden waste water. The micro-agglomerates are rendered buoyant by the aeration and are thus rendered separable from the inorganic laden waste water which may be further treated to remove the inorganic waste to provide water for recirculation.
摘要翻译： 在包含第一附聚杂质的释放的碳质煤中，从杂质释放的煤浆中与附聚油形成开放的结构化的链状的微团聚体，然后形成相对较大，较不开放的结构更坚固的附聚物的方法， 一部分浆料提供微团聚物的混合物，相对较大，更坚固的附聚物，水和任何可能存在的无机杂质。 筛选相对较大，更坚固的附聚物，然后使用充气，分离器罐分离微团聚体，留下含有无机杂质的废水。 微团聚体通过通气使其浮起，因此与无机载体废水分离，可以进一步处理以除去无机废物以提供用于再循环的水。
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公开(公告)号：US4592506A
公开(公告)日：1986-06-03
申请号：US685145
申请日：1984-12-21
CPC分类号： B05B7/02 , B05B1/265 , F23D1/005 , Y10S239/19
摘要： A wear resistant atomizing nozzle assembly is provided having an outwardly diverging, frustum of a cone-shaped deflector core of wear resistant ceramic and a nozzle rim of wear resistant ceramic and having an outwardly flared inner surface encircling the core to form a flared, atomizing nozzle orifice therewith. The core is mounted in a flared socket of a deflector core holder and inner and outer sleeves feed, say, atomizing air to the deflector core surface and, say, a coal liquid mixture fuel inwardly around the nozzle rim so that the fuel is held by the air as a film against the nozzle rim inner surface and then atomized as it emerges from the nozzle rim.
摘要翻译： 提供了一种耐磨雾化喷嘴组件，其具有向外发散的锥形的耐磨陶瓷锥形偏转器芯和耐磨陶瓷的喷嘴边缘，并且具有围绕芯的向外扩张的内表面以形成扩张的雾化喷嘴 孔。 芯部安装在偏转器芯保持器的扩口插座中，并且内部和外部套筒将例如雾化空气供给到偏转器芯表面，并且例如将煤液体混合物燃料向内喷射到喷嘴边缘周围，使得燃料被 空气作为薄膜抵靠喷嘴边缘内表面，然后在从喷嘴边缘出现时被雾化。
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7.发明授权Method of removing carbonaceous particles, essentially free of pyritic sulphur, from an aqueous coal slurry 失效从含水煤浆中除去基本上不含硫黄硫的碳质颗粒的方法
公开(公告)号：US4972956A
公开(公告)日：1990-11-27
申请号：US326362
申请日：1989-03-21
摘要： Carbonaceous coal particles, essentially free of pyritic sulphur, are removed from an aqueous coal slurry in two steps. In the first step the carbonaceous particles of the slurry, with the pyritic sulphur essentially free of surface conditioning agent, are micro-agglomerated with agglomerating oil added in an amount varying from about 0.5 wt % (dry basis), when the coal particle average size is about 100 microns, to about 10 wt % (dry basis) when the average coal particle size is about 4 microns to remove relatively coarser particles of pyritic sulphur. Then, without adding any further agglomerating oil, relatively finer pyritic sulphur particles trapped with water in the micro-agglomerates are removed.
摘要翻译： 基本上不含黄铁矿硫的碳质煤颗粒在两个步骤中从含水煤浆中除去。 在第一步中，随着硫酸盐基本不含表面调节剂的浆料的碳质颗粒以约0.5重量％（干基）的量添加的聚集油进行微团聚，当煤粒子平均尺寸 当平均煤粒度为约4微米以除去相对较粗的硫酸盐颗粒时，其为约100微米至约10重量％（干基）。 然后，在不加入任何附加的附聚油的情况下，除去在微团聚体中用水捕获的相对较细的硫铁矿硫颗粒。
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8.发明授权Method of breaking down chemisorption bond of clay-containing heavy oil water emulsions 失效分解含粘土的重油水乳化液的化学吸附键的方法
公开(公告)号：US4648962A
公开(公告)日：1987-03-10
申请号：US830906
申请日：1986-02-18
摘要： Persistent chemisorption bonds of clay solids in clay-containing heavy oil and water emulsions, from oil sands, heavy oil or conventional oil wells, are broken down by mixing the emulsion with an aqueous mixture of coal particles so that the mixture has a suspension density in the range 1 to 50 weight % solids. The coal particles have a particle size in the range 5 to 100 .mu.m so that occluded hydrophilic, inorganic solids are separable from a substantial portion of the hydrophobic, carbonaceous substances of the coal. The mixing of the emulsion with the aqueous suspension of coal particles is continued until agglomerates are formed comprising essentially carbonaceous components of the coal and the heavy oil thereby breaking down the chemisorption bonds by interdependantly dissociating carbonaceous components of the coal and heavy oil from the clay solids and other hydrophilic, inorganic solids and water from the coal and heavy oil. The agglomerates are separated from the dissociated clay solids and other hydrophilic, inorganic components and then volatile components of the agglomerates may be thermally or otherwise extracted from them.
摘要翻译： 通过将乳液与煤颗粒的含水混合物混合，将油泥，重油或常规油井中含粘土的重油和水乳液中的粘土固体的持久化学吸附键分解，使混合物的悬浮密度 范围1至50重量％的固体。 煤粒子的粒径在5至100μm的范围内，因此封闭的亲水性无机固体可与煤的大部分疏水性含碳物质分离。 将乳液与煤颗粒的水性悬浮液混合，直到形成包含煤和重油的基本上含碳成分的附聚物，从而通过相互依赖地从粘土固体中分解煤和重油的碳质成分来分解化学吸附键 和其他亲水，无机固体和来自煤和重油的水。 将附聚物与离解的粘土固体和其它亲水性无机组分分离，然后可以热聚合或从其中提取附聚物的挥发性组分。
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9.发明授权
公开(公告)号：US4303505A
公开(公告)日：1981-12-01
申请号：US86108
申请日：1979-10-18
CPC分类号： B01D15/02 , B01D17/0202 , B01D43/00 , C10G33/00 , C10L1/322 , B01D2215/021
摘要： A process for selectively removing hydrophilic constituents from flowable hydrophobic mixtures and suspensions which comprises forming a tenacious paste by mixing water with finely divided material which is insoluble or substantially insoluble in water and in the organic liquid in the hydrophobic mixture or suspension, which is inert to the organic liquid and the hydrophobic materials in the hydrophobic mixture or suspension and which is capable of selectively adsorbing said hydrophilic constituents. The paste is formed in a mixing-type liquid-liquid contactor so that a layer of the paste forms on and clings to the impellers and other internal surfaces of the contactor. The hydrophilic mixture or suspension is placed in the contactor and the impellers are rotated at a relatively low speed so that the paste is subjected to gentle agitation by shearing and folding effects caused by rotation of the impellers and contact with the flowable hydrophobic mixture or suspension so that the hydrophilic constituents are adsorbed by the paste and are separated from the remainder of the hydrophobic mixture or suspension.
摘要翻译： 一种从可流动的疏水性混合物和悬浮液中选择性地除去亲水成分的方法，其包括通过将水与不溶于或基本上不溶于水的疏水混合物或悬浮液中的有机液体中混合水形成坚固的糊料， 疏水混合物或悬浮液中的有机液体和疏水性材料，并能够选择性地吸附所述亲水组分。 该糊料形成在混合型液 - 液接触器中，使得一层糊状物形成并粘附到叶轮和接触器的其它内表面上。 将亲水性混合物或悬浮液放置在接触器中并且叶轮以相对较低的速度旋转，使得通过由叶轮的旋转引起的剪切和折叠效应以及与可流动的疏水性混合物或悬浮液接触而使糊料受到轻柔的搅拌 亲水组分被糊剂吸附并与疏水混合物或悬浮液的其余部分分离。
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公开(公告)号：US4269699A
公开(公告)日：1981-05-26
申请号：US87698
申请日：1979-10-23
申请人： Ronald G. L. McCready , Richard D. Coleman , Charles E. Capes , Alan G. Kempton , Nayera A. M. Moneib
发明人： Ronald G. L. McCready , Richard D. Coleman , Charles E. Capes , Alan G. Kempton , Nayera A. M. Moneib
CPC分类号： B03B1/04 , B03B9/00 , C10L9/00 , C22B3/18 , Y02P10/234 , Y10S423/17
摘要： The sulfide surfaces of finely-divided impure iron sulfide-containing minerals such as pyritic ores or coals are rendered hydrophilic by the adsorption of conditioned, inorganic sulfide-oxidizing bacteria. This adsorption of conditioned bacteria occurs in a short time to render the surfaces hydrophilic and allows these altered sulfide particles to be separated from hydrophobic solids by flotation, oil-agglomeration or the like. This bioadsorption process has particular applicability to pyritic coal beneficiation.
摘要翻译： 通过吸附被调节的无机硫化物氧化细菌，细碎的不纯的含硫化铁的矿物如黄铁矿或煤的硫化物表面变得亲水。 条件细菌的这种吸附发生在短时间内，使表面亲水，并允许这些改变的硫化物颗粒通过浮选，油聚集等与疏水性固体分离。 这种生物吸附过程特别适用于黄铁矿选矿。
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