Use of vinyl alcohol homopolymer and copolymers for tableting active
materials
    1.
    发明授权
    Use of vinyl alcohol homopolymer and copolymers for tableting active materials 失效
    乙烯醇均聚物和共聚物用于压片活性物质的应用

    公开(公告)号:US4990335A

    公开(公告)日:1991-02-05

    申请号:US165230

    申请日:1988-05-12

    IPC分类号: A61K9/20 C11D17/00

    CPC分类号: C11D17/0073 A61K9/2027

    摘要: Method of making tablets for active ingredient delivery by compressing a mixture of active ingredient and granular, high viscosity, fully hydrolyzed polyvinyl alcohol or copolymer of vinyl alcohol with methyl acrylate or methyl methacrylate. By use of a crystalline, heat treated polymer, a tablet providing quick active ingredient release is obtained. By using an amorphous, non-heat treated polymer a tablet providing prolonged active ingredient release is obtained. By using blends of crystalline and amorphous polymers, tablets having a range of active ingredient release characteristics can be obtained. The granular, high viscosity, fully hydrolyzed polymers provide flowability, compressibility and processing versatility advantages over conventional tablet binders.

    摘要翻译: 通过压缩活性成分和颗粒状,高粘度,完全水解的聚乙烯醇或乙烯醇与丙烯酸甲酯或甲基丙烯酸甲酯的共聚物的混合物制备用于活性成分递送的片剂的方法。 通过使用结晶的经热处理的聚合物,获得了提供快速活性成分释放的片剂。 通过使用无定形的未加热处理的聚合物,获得延长的活性成分释放的片剂。 通过使用结晶和无定形聚合物的混合物,可以获得具有一定范围的活性成分释放特性的片剂。 颗粒状,高粘度,完全水解的聚合物提供了流畅性,压缩性和加工多功能性优于传统的片剂粘合剂。

    Process for the manufacture of chloroprene
    2.
    发明授权
    Process for the manufacture of chloroprene 失效
    制造氯丁二烯的工艺

    公开(公告)号:US4605800A

    公开(公告)日:1986-08-12

    申请号:US458554

    申请日:1983-01-17

    摘要: An improved process for the catalytic dehydrochlorination of 3,4-dichlorobutene-1 with aqueous alkali, wherein the effluent from the dehydrochlorination reactor is separated into phases, and the organic phase is steam-stripped at low temperature (below about 80.degree. C.) to recover chloroprene product, while the steam stripper heels are returned to the dehydrochlorination reactor. A small portion of the heels are purged prior to being recycled. Most of the catalyst is recovered and returned to the reaction, but a small amount of make-up catalyst is added. Chloroprene made in this process is a valuable monomer which finds use in the manufacture of a broad line of synthetic elastomers of considerable industrial interest.

    摘要翻译: 用碱水溶液对3,4-二氯丁烯-1进行催化脱氯化氢的改进方法,其中将来自脱氯化氢反应器的流出物分离成相,有机相在低温(低于约80℃)下蒸汽汽提。 以回收氯丁二烯产物,而蒸汽汽提塔高跟鞋则返回脱氯化氢反应器。 高跟鞋的一小部分在被回收之前被清除。 大部分催化剂被回收并返回到反应中,但加入少量补充催化剂。 在该方法中制备的氯丁二烯是一种有价值的单体,可用于生产具有相当大的工业感兴趣的广泛的合成弹性体系。

    Continuous process for preparing poly(butylene terephthalate) oligomer
or poly(butylene isophthalate) oligomer
    4.
    发明授权
    Continuous process for preparing poly(butylene terephthalate) oligomer or poly(butylene isophthalate) oligomer 失效
    制备聚(对苯二甲酸丁二醇酯)低聚物或聚(邻苯二甲酸丁二醇酯)低聚物的连续方法

    公开(公告)号:US5064935A

    公开(公告)日:1991-11-12

    申请号:US561468

    申请日:1990-08-01

    IPC分类号: C08G63/183 C08G63/78

    CPC分类号: C08G63/78

    摘要: Economic and efficient process for preparing an oligomer of poly(butylene terephthalate) or an oligomer of poly(butylene isophthalate) from a transesterification reaction mass by using a countercurrent column reactor system wherein the transesterification reaction mass is fed into the countercurrent column reactor and continuously flows downward while simultaneously a heated inert gas stream continuously flows upward to scrub out volatiles from the transesterification reaction mass, thereby yielding from the bottom of the countercurrent column reactor an oligomer of poly(butylene terephthalate) or an oligomer of poly(butylene isophthalate) suitable for use in a polycondensation reaction. Butanediol is recycled throughout the process through an absorber column.