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1.发明申请公开(公告)号：US20120022269A1
公开(公告)日：2012-01-26
申请号：US13138742
申请日：2010-03-31
IPC分类号： C07C311/48 , C07C303/40 , C07D233/58
CPC分类号： C07D233/58 , C07C311/48
摘要： According to the method for producing fluorine-containing N-alkylsulfonylimide compound, the fluorine-containing N-alkylsulfonylimide compound can be produced safely with a high recovery rate by alkylating fluorine-containing sulfonylimide acid or fluorine-containing sulfonylimide acid salt with dialkylsulfuric acid or dialkylcarbonic acid.
摘要翻译： 根据制造含氟N-烷基磺酰亚胺化合物的方法，可以通过用二烷基硫酸或二烷基碳酸烷基化含氟磺酰亚胺酸或含氟磺酰亚胺酸盐，以高回收率安全地制备含氟N-烷基磺酰亚胺化合物 酸。
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2.发明申请PROCESS FOR PRODUCING TRIPHENYLENE COMPOUND AND CRYSTAL OBTAINED BY THE PROCESS 有权用于生产三苯乙烯化合物的方法和由该方法获得的晶体公开(公告)号：US20110201845A1
公开(公告)日：2011-08-18
申请号：US13044975
申请日：2011-03-10
IPC分类号： C07C39/14
CPC分类号： C07C39/12 , C07B2200/13 , C07C37/11 , C07C37/84 , C07C2603/42 , Y02P20/55
摘要： An object of the present invention is to provide a process for producing high-purity hydroxytriphenylenes in which not only inexpensive raw materials can be used but also no complicated steps of deprotection such as dealkylation, and reduction and the like are necessary, and which is thereby advantageous in industrial production. Also there is provided a novel crystal of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate, which has satisfactory thermal stability. The process for producing a compound represented by the general formula (2) is characterized by reacting a compound represented by the general formula (1) in the presence of a metal oxide comprising a metal selected from trivalent iron, pentavalent vanadium and hexavalent molybdenum and of a nonvolatile strong acid: wherein, Rs are each independently a hydrogen atom, a halogen atom, an alkyl group having 1 to 3 carbon atoms or an alkoxy group having 1 to 3 carbon atoms.
摘要翻译： 本发明的目的是提供一种生产高纯度羟基三苯并噻吩的方法，其中不仅可以使用便宜的原料，而且还不需要复杂的脱保护步骤如脱烷基化和还原等，从而 有利于工业生产。 还提供了具有令人满意的热稳定性的2,3,6,7,10,11-六羟基三亚苯一水合物的新晶体。 由通式（2）表示的化合物的制备方法的特征在于使通式（1）表示的化合物在包含选自三价铁，五价钒和六价钼的金属的金属氧化物的存在下反应， 非挥发性强酸：其中，R 5各自独立地为氢原子，卤素原子，碳原子数为1〜3的烷基或碳原子数为1〜3的烷氧基。
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3.发明授权Process for producing triphenylene compound and crystal obtained by the process 有权通过该方法得到的三亚苯化合物和晶体的生产方法公开(公告)号：US07964757B2
公开(公告)日：2011-06-21
申请号：US12670707
申请日：2008-08-06
CPC分类号： C07C39/12 , C07B2200/13 , C07C37/11 , C07C37/84 , C07C2603/42 , Y02P20/55
摘要： An object of the present invention is to provide a process for producing high-purity hydroxytriphenylenes in which not only inexpensive raw materials can be used but also no complicated steps of deprotection such as dealkylation, and reduction and the like are necessary, and which is thereby advantageous in industrial production. Also there is provided a novel crystal of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate, which has satisfactory thermal stability. The process for producing a compound represented by the general formula (2) is characterized by reacting a compound represented by the general formula (1) in the presence of a metal oxide comprising a metal selected from trivalent iron, pentavalent vanadium and hexavalent molybdenum and of a nonvolatile strong acid: wherein, Rs are each independently a hydrogen atom, a halogen atom, an alkyl group having 1 to 3 carbon atoms or an alkoxy group having 1 to 3 carbon atoms.
摘要翻译： 本发明的目的是提供一种生产高纯度羟基三苯并噻吩的方法，其中不仅可以使用便宜的原料，而且还不需要复杂的脱保护步骤如脱烷基化和还原等，从而 有利于工业生产。 还提供了具有令人满意的热稳定性的2,3,6,7,10,11-六羟基三亚苯一水合物的新晶体。 由通式（2）表示的化合物的制备方法的特征在于使通式（1）表示的化合物在包含选自三价铁，五价钒和六价钼的金属的金属氧化物的存在下反应， 非挥发性强酸：其中，R 5各自独立地为氢原子，卤素原子，碳原子数为1〜3的烷基或碳原子数为1〜3的烷氧基。
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4.发明申请ADAPTER AND INTERFACE AND ELECTRONIC DEVICE TEST APPARATUS PROVIDED WITH ADAPTER 审中-公开适配器和接口和电子设备测试装置提供适配器公开(公告)号：US20090027060A1
公开(公告)日：2009-01-29
申请号：US11912709
申请日：2006-05-18
申请人： Daisuke Takano , Yoshiyuki Masuo
发明人： Daisuke Takano , Yoshiyuki Masuo
IPC分类号： G01R1/02
CPC分类号： G01R1/07378
摘要： An adapter able to reduce the costs of an electronic device test apparatus, the adapter having a frame member interposed, between an opening formed at a handler and a HIFIX attached to a test head and inserted in the opening for adapting the shape of the HIFIX to the shape of the opening.
摘要翻译： 一种适配器，其能够降低电子设备测试装置的成本，所述适配器具有框架构件，插入在处理器形成的开口和附接到测试头的HIFIX之间，并插入到开口中以使HIFIX的形状适应于 开口的形状。
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公开(公告)号：US20130137899A1
公开(公告)日：2013-05-30
申请号：US13814801
申请日：2010-09-21
申请人： Tsunetoshi Honda , Daisuke Takano
发明人： Tsunetoshi Honda , Daisuke Takano
IPC分类号： C07C303/38
CPC分类号： C07C303/38 , C07C311/48
摘要： In this process for producing a fluorine-containing sulfonylimide compound, a process for producing a fluorine-containing sulfonylimide compound ((Rf1SO2)(Rf2SO2)2N.M) is employed that comprises a first step of obtaining a reaction liquid by reacting a perfluoroalkylsulfonyl fluoride (Rf1SO2F) with ammonia, a second step of obtaining a mixture containing an alkaline metal salt of a perfluoroalkylsulfonamide (Rf'SO2NH.M) by reacting the reaction liquid with at least one type of alkaline metal compound selected from among hydroxides, carbonates and bicarbonates of alkaline metals M of either Li, Na or K, and a third step of reacting the mixture with a perfluoroalkylsulfonyl halide (Rf2SO2X), wherein Rf1 and Rf2 represent linear or branched perfluoroalkyl groups having 1 to 4 carbon atoms, and X represents fluorine or chlorine.
摘要翻译： 在该含氟磺酰亚胺化合物的制造方法中，使用含氟磺酰亚胺化合物（（Rf1SO2）（Rf2SO2）2N.M）的制造方法，该方法包括：通过使全氟烷基磺酰氟 （Rf 1 SO 2 F），第二步是通过使反应液与至少一种选自氢氧化物，碳酸盐和碳酸氢盐的碱金属化合物反应，得到含有全氟烷基磺酰胺的碱金属盐（Rf'SO2NH.M）的混合物 的Li，Na或K的碱金属M，以及使混合物与全氟烷基磺酰卤（R f 2 SO 2 X）反应的第三步，其中Rf1和Rf2表示具有1-4个碳原子的直链或支链全氟烷基，X表示氟或 氯。
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6.发明授权Process for producing triphenylene compound and crystal obtained by the process 有权通过该方法得到的三亚苯化合物和晶体的生产方法公开(公告)号：US08178731B2
公开(公告)日：2012-05-15
申请号：US13044975
申请日：2011-03-10
CPC分类号： C07C39/12 , C07B2200/13 , C07C37/11 , C07C37/84 , C07C2603/42 , Y02P20/55
摘要： An object of the present invention is to provide a process for producing high-purity hydroxytriphenylenes in which not only inexpensive raw materials can be used but also no complicated steps of deprotection such as dealkylation, and reduction and the like are necessary, and which is thereby advantageous in industrial production. Also there is provided a novel crystal of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate, which has satisfactory thermal stability. The process for producing a compound represented by the general formula (2) is characterized by reacting a compound represented by the general formula (1) in the presence of a metal oxide comprising a metal selected from trivalent iron, pentavalent vanadium and hexavalent molybdenum and of a nonvolatile strong acid: wherein, Rs are each independently a hydrogen atom, a halogen atom, an alkyl group having 1 to 3 carbon atoms or an alkoxy group having 1 to 3 carbon atoms.
摘要翻译： 本发明的目的是提供一种生产高纯度羟基三苯并噻吩的方法，其中不仅可以使用便宜的原料，而且还不需要复杂的脱保护步骤如脱烷基化和还原等，从而 有利于工业生产。 还提供了具有令人满意的热稳定性的2,3,6,7,10,11-六羟基三亚苯一水合物的新晶体。 由通式（2）表示的化合物的制备方法的特征在于使通式（1）表示的化合物在包含选自三价铁，五价钒和六价钼的金属的金属氧化物的存在下反应， 非挥发性强酸：其中，R 5各自独立地为氢原子，卤素原子，碳原子数为1〜3的烷基或碳原子数为1〜3的烷氧基。
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7.发明申请PROCESS FOR PRODUCING TRIPHENYLENE COMPOUND AND CRYSTAL OBTAINED BY THE PROCESS 有权用于生产三苯乙烯化合物的方法和由该方法获得的晶体公开(公告)号：US20100191020A1
公开(公告)日：2010-07-29
申请号：US12670707
申请日：2008-08-06
CPC分类号： C07C39/12 , C07B2200/13 , C07C37/11 , C07C37/84 , C07C2603/42 , Y02P20/55
摘要： An object of the present invention is to provide a process for producing high-purity hydroxytriphenylenes in which not only inexpensive raw materials can be used but also no complicated steps of deprotection such as dealkylation, and reduction and the like are necessary, and which is thereby advantageous in industrial production. Also there is provided a novel crystal of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate, which has satisfactory thermal stability. The process for producing a compound represented by the general formula (2) is characterized by reacting a compound represented by the general formula (1) in the presence of a metal oxide comprising a metal selected from trivalent iron, pentavalent vanadium and hexavalent molybdenum and of a nonvolatile strong acid: wherein, Rs are each independently a hydrogen atom, a halogen atom, an alkyl group having 1 to 3 carbon atoms or an alkoxy group having 1 to 3 carbon atoms.
摘要翻译： 本发明的目的是提供一种生产高纯度羟基三苯并噻吩的方法，其中不仅可以使用便宜的原料，而且还不需要复杂的脱保护步骤如脱烷基化和还原等，从而 有利于工业生产。 还提供了具有令人满意的热稳定性的2,3,6,7,10,11-六羟基三亚苯一水合物的新晶体。 由通式（2）表示的化合物的制备方法的特征在于使通式（1）表示的化合物在包含选自三价铁，五价钒和六价钼的金属的金属氧化物的存在下反应， 非挥发性强酸：其中，R 5各自独立地为氢原子，卤素原子，碳原子数为1〜3的烷基或碳原子数为1〜3的烷氧基。
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8.发明授权Fluorine-containing n-alkylsulfonylimide compound, manufacturing method therefor, and method of manufacturing an ionic compound 有权含氟的正烷基磺酰亚胺化合物及其制造方法以及离子化合物的制造方法公开(公告)号：US08436198B2
公开(公告)日：2013-05-07
申请号：US13138742
申请日：2010-03-31
IPC分类号： C07C309/05
CPC分类号： C07D233/58 , C07C311/48
摘要： According to the method for producing fluorine-containing N-alkylsulfonylimide compound, the fluorine-containing N-alkylsulfonylimide compound can be produced safely with a high recovery rate by alkylating fluorine-containing sulfonylimide acid or fluorine-containing sulfonylimide acid salt with dialkylsulfuric acid or dialkylcarbonic acid.
摘要翻译： 根据制造含氟N-烷基磺酰亚胺化合物的方法，可以通过用二烷基硫酸或二烷基碳酸烷基化含氟磺酰亚胺酸或含氟磺酰亚胺酸盐，以高回收率安全地制备含氟N-烷基磺酰亚胺化合物 酸。
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