Method of recovering iodine
    1.
    发明授权
    Method of recovering iodine 失效
    回收碘的方法

    公开(公告)号:US5356611A

    公开(公告)日:1994-10-18

    申请号:US144515

    申请日:1993-11-02

    CPC classification number: C01B7/14

    Abstract: A method for recovering iodine from a composition containing iodine and/or iodide in which any iodine present is first reduced to iodide, the iodide is then separated from solution by selective anion exchange absorption, the separated iodide is eluted from the exchanger, the iodide-containing eluate solution is treated with a cation exchanger, H.sub.2 O.sub.2 and H.sub.2 SO.sub.4 are then added to the remaining solution, and the resulting iodine is precipitated and may be separated out in crystalline form. The method is also particularly suitable for separating iodine from solutions which contain organic constituents such as nitrogen-containing organic compounds.

    Abstract translation: 从含有碘和/或碘化物的组合物中回收碘的方法,其中首先将存在碘的碘还原成碘,然后通过选择性阴离子交换吸收将碘离子与溶液分离,从交换器洗脱分离的碘化物, 用阳离子交换剂处理含有洗脱液的溶液,然后将H 2 O 2和H 2 SO 4加入到剩余的溶液中,所得碘沉淀并且可以以结晶形式分离出来。 该方法还特别适用于从含有有机成分如含氮有机化合物的溶液中分离碘。

    Method of preparing LiPF.sub.6
    4.
    发明授权
    Method of preparing LiPF.sub.6 失效
    制备LiPF6的方法

    公开(公告)号:US5866093A

    公开(公告)日:1999-02-02

    申请号:US880510

    申请日:1997-06-23

    CPC classification number: C01D15/005

    Abstract: A method for preparing lithium hexafluorophosphate, which is useful as an electrolyte in primary and secondary cells, involves combining and cooling phosphorus pentachloride and lithium fluoride, and then adding hydrogen fluoride. Using this method, which is simple to perform, a good yield of the product can be obtained.

    Abstract translation: 用于初级和二次电池中的电解质的六氟磷酸锂的制备方法包括组合并冷却五氯化磷和氟化锂,然后加入氟化氢。 使用这种简单的方法,可以获得良好的产率。

    Process for preparing 4-fluoro-1,3-dioxolan-2-one
    6.
    发明授权
    Process for preparing 4-fluoro-1,3-dioxolan-2-one 失效
    4-氟-1,3-二氧戊环-2-酮的制备方法

    公开(公告)号:US07745648B2

    公开(公告)日:2010-06-29

    申请号:US11210868

    申请日:2005-08-25

    CPC classification number: C07D317/42

    Abstract: A process for preparing 4-fluoro-1,3-dioxolan-2-one comprising adding 4-fluoro-1,3-dioxolan-2-one to ethylene carbonate in an amount of from 3 to 20% by weight relative to the ethylene carbonate as a solvent for the ethylene carbonate, and introducing fluorine or a mixture containing fluorine in an inert gas is introduced into the resulting solution at 15 to 45° C.

    Abstract translation: 一种制备4-氟-1,3-二氧戊环-2-酮的方法,包括将相对于乙烯的3-20重量%的4-氟-1,3-二氧戊环-2-酮加入碳酸亚乙酯中 碳酸酯作为碳酸亚乙酯的溶剂,并将氟或含氟的混合物在惰性气体中引入所得溶液中15至45℃。

    Process for preparing 4-fluoro-1,3-dioxolan-2-one
    7.
    发明申请
    Process for preparing 4-fluoro-1,3-dioxolan-2-one 失效
    4-氟-1,3-二氧戊环-2-酮的制备方法

    公开(公告)号:US20060036102A1

    公开(公告)日:2006-02-16

    申请号:US11210868

    申请日:2005-08-25

    CPC classification number: C07D317/42

    Abstract: A process for preparing 4-fluoro-1,3-dioxolan-2-one comprising adding 4-fluoro-1,3-dioxolan-2-one to ethylene carbonate in an amount of from 3 to 20% by weight relative to the ethylene carbonate as a solvent for the ethylene carbonate, and introducing fluorine or a mixture containing fluorine in an inert gas is introduced into the resulting solution at 15 to 45° C.

    Abstract translation: 一种制备4-氟-1,3-二氧戊环-2-酮的方法,包括将相对于乙烯的3-20重量%的4-氟-1,3-二氧戊环-2-酮加入碳酸亚乙酯中 碳酸酯作为碳酸亚乙酯的溶剂,并将氟或含氟的混合物在惰性气体中引入所得溶液中15至45℃。

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