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公开(公告)号：US5814228A
公开(公告)日：1998-09-29
申请号：US685778
申请日：1996-07-24
CPC分类号： C02F1/24 , B01D17/0205 , B01D17/12 , B01D21/34 , B03D1/028 , B03D1/1412 , B03D1/245 , B03D1/1487
摘要： Flotation apparatus (10) for removing finely divided bodies of an insoluble substance dispersed in an aqueous medium, such as oil and solids dispersed in water, comprises a vertical flotation column (12) having a feed inlet (14) and an outlet (22) for the aqueous medium, a sparging system (16) for generating gas bubbles rising upwardly in the aqueous medium to capture and raise the finely divided bodies of the insoluble substance to the surface of the aqueous medium in the column to form a layer (31) of the insoluble substance on the surface of the aqueous medium, a launder (18) for receiving an overflow of the insoluble substance and an outlet (20) for the insoluble substance in the launder. The apparatus (10) can be used in both countercurrent and co-current fashion. In a particular embodiment, the apparatus includes a mechanism for the intermittent dumping of the layer (31) of insoluble substance from the column (12).
摘要翻译： 用于除去分散在水性介质（例如分散在水中的油和固体）的水性介质中的细分散体的浮选装置（10）包括具有进料口（14）和出口（22）的垂直浮选塔（12） 对于水性介质，用于产生在水性介质中向上升起的气泡的吸气系统（16），以将不溶性物质的细分散体吸收并升高到塔中水性介质的表面，形成层（31） 在水性介质的表面上的不溶物质，用于接收不溶物质溢出的流槽（18）和用于流体中不溶物质的出口（20）。 装置（10）可以以逆流和并流方式使用。 在一个具体实施方案中，该装置包括用于从塔（12）间歇倾倒不溶物质层（31）的机构。
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公开(公告)号：US5580463A
公开(公告)日：1996-12-03
申请号：US329958
申请日：1994-10-27
申请人： Gale L. Hubred
发明人： Gale L. Hubred
摘要： A method for removing residual oil from oily water under pressure is provided. The method comprises flowing a liquid stream of an oily water downward through a vertically extended zone to remove the residual oil. A gas is injected into the lower end of the zone and at a rate sufficient to generate bubbles of a predetermined volume in the liquid stream. A sufficient pressure is maintained in the zone to control the rate of expansion of the bubbles to a volume compatible with oil droplets in the liquid stream during upward migration of the bubbles and the oil droplets. The rate of flow of the liquid stream from the lower end of the zone and the rate of flow of the gas from the upper end of the zone are regulated to collect residual oil from a quiescent volume within the upper portion of the zone.
摘要翻译： 提供了一种在压力下从油性水中除去残余油的方法。 该方法包括使油水的液体流向下流动通过垂直延伸的区域以除去残留的油。 气体被注入到该区域的下端，并以足以产生液体流中预定体积的气泡的速率被注入。 在该区域中保持足够的压力以将气泡膨胀速率控制在与气泡和油滴向上迁移期间在液体流中与油滴相容的体积。 来自该区域的下端的液体流的流速和来自该区域的上端的气体的流速被调节以从该区域上部的静止体积收集残留的油。
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3.发明授权
公开(公告)号：US4434141A
公开(公告)日：1984-02-28
申请号：US422987
申请日：1982-09-24
IPC分类号： B01D11/04 , B01J23/94 , C01G1/00 , C01G31/00 , C01G39/00 , C01G41/00 , C01G51/00 , C01G51/12 , C01G53/00 , C01G53/12 , C22B3/26 , C22B3/28 , C22B3/30 , C22B7/00 , C22B23/00 , C22B23/02 , C22B34/22 , C22B34/34
CPC分类号： C22B23/0446 , B01J23/94 , C01G31/003 , C01G39/003 , C01G41/006 , C01G51/003 , C01G51/12 , C01G53/003 , C01G53/12 , C22B23/005 , C22B23/026 , C22B23/0461 , C22B3/0016 , C22B3/0017 , C22B3/0021 , C22B34/22 , C22B34/34 , C22B7/008 , C22B7/009 , Y02P10/214 , Y02P10/224 , Y02P10/234 , Y02P20/584
摘要： A method of recovering metal values from an aqueous stream. The metal values are preferably obtained from leaching spent hydroprocessing catalysts, and include nickel, cobalt, vanadium and molybdenum. The metal values are extracted, isolated and purified by liquid, liquid extraction techniques.
摘要翻译： 从含水流中回收金属值的方法。 金属值优选从浸出废加氢处理催化剂获得，并且包括镍，钴，钒和钼。 通过液体，液体萃取技术提取，分离和纯化金属值。
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4.发明授权
公开(公告)号：US4432953A
公开(公告)日：1984-02-21
申请号：US422813
申请日：1982-09-24
IPC分类号： B01J23/94 , C01G31/00 , C01G39/00 , C01G51/00 , C01G51/12 , C01G53/00 , C01G53/12 , C22B3/26 , C22B3/28 , C22B3/30 , C22B7/00 , C22B23/00 , C22B23/02 , C22B34/22 , C22B34/34 , C22B34/36
CPC分类号： C22B23/005 , B01J23/94 , C01G31/003 , C01G39/003 , C01G51/003 , C01G51/12 , C01G53/003 , C01G53/12 , C22B23/026 , C22B23/0446 , C22B23/0461 , C22B3/0016 , C22B3/0017 , C22B3/0021 , C22B34/22 , C22B34/34 , C22B7/008 , C22B7/009 , Y02P10/214 , Y02P10/224 , Y02P10/234 , Y02P20/584
摘要： A process for enhancing recovery of cobalt from spent hydroprocessing catalysts when the spent catalyst particles are first roasted at between 400.degree. C. and 600.degree. C. and then contacted with a first aqueous solution of ammonia and an ammonium salt to recover nickel, cobalt, molybdenum and vanadium. The once-leached spent hydroprocessing catalysts are contacted with a second aqueous solution of sulfur dioxide. The metal values are precipitated with hydrogen sulfide and the precipitate is roasted with unroasted spent hydroprocessing catalysts.
摘要翻译： 一种用于在废催化剂颗粒首先在400℃至600℃下焙烧之后从废加氢处理催化剂中提高钴回收率的方法，然后与第一氨水溶液和铵盐接触以回收镍，钴， 钼和钒。 一次性废弃的加氢处理催化剂与第二二氧化硫水溶液接触。 金属值用硫化氢沉淀，沉淀物用未加工的废加氢处理催化剂进行焙烧。
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公开(公告)号：US4563213A
公开(公告)日：1986-01-07
申请号：US637652
申请日：1984-08-02
申请人： Gale L. Hubred
发明人： Gale L. Hubred
CPC分类号： C22B3/0017 , C01G51/003 , C01G53/003 , Y02P10/234
摘要： A process is disclosed for extracting cobalt values from an aqueous solution containing cobalt and other metal values and stripping the resulting organic solution with an aqueous ammoniacal solution.
摘要翻译： 公开了从含有钴和其他金属值的水溶液中提取钴值并用氨水溶液汽提所得有机溶液的方法。
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公开(公告)号：US4434140A
公开(公告)日：1984-02-28
申请号：US422814
申请日：1982-09-24
IPC分类号： B01J23/94 , C01G1/00 , C01G31/00 , C01G39/00 , C01G51/00 , C01G51/12 , C01G53/00 , C01G53/12 , C22B3/00 , C22B3/26 , C22B3/28 , C22B3/30 , C22B7/00 , C22B23/00 , C22B23/02 , C22B34/22 , C22B34/34
CPC分类号： B01J23/94 , C01G31/003 , C01G39/003 , C22B23/005 , C22B23/026 , C22B23/0446 , C22B23/0461 , C22B3/0016 , C22B3/0017 , C22B3/0021 , C22B34/22 , C22B34/34 , C22B7/008 , C22B7/009 , C01P2002/82 , C01P2006/60 , Y02P10/214 , Y02P10/224 , Y02P10/234 , Y02P20/584
摘要： A method of stripping an organic extraction solvent containing quaternary alkyl ammonium complexes. The extraction solvent is contacted with an aqueous stripping solution having at least 75 g/l bicarbonate ion, while maintained at between pH 7 and 9 at a temperature of no more than 50.degree. C.
摘要翻译： 一种汽提含有季铵烷基铵络合物的有机萃取溶剂的方法。 将萃取溶剂与具有至少75g / l碳酸氢根离子的水性汽提溶液接触，同时在不超过50℃的温度下保持在pH7至9之间。
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7.发明授权
公开(公告)号：US4432949A
公开(公告)日：1984-02-21
申请号：US422988
申请日：1982-09-24
IPC分类号： C01G31/00 , C01G39/00 , C01G41/00 , C01G51/00 , C01G53/00 , C22B3/26 , C22B3/28 , C22B3/30 , C22B7/00 , C22B34/22
CPC分类号： C01G53/003 , C01G31/00 , C01G39/003 , C01G41/003 , C01G51/003 , C22B3/0012 , C22B3/0017 , C22B3/0021 , C22B34/22 , C22B7/009 , Y02P10/214 , Y02P10/234
摘要： A process for separating metal values from an aqueous stream containing vanadium, molybdenum, nickel and cobalt. Vanadium is first precipitated, and then nickel, cobalt, and molybdenum are removed by serial ion exchange.
摘要翻译： 从含有钒，钼，镍和钴的含水流中分离金属值的方法。 首先沉淀钒，然后通过串联离子交换除去镍，钴和钼。
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公开(公告)号：US4317730A
公开(公告)日：1982-03-02
申请号：US183111
申请日：1980-09-10
申请人： Gale L. Hubred , Robert T. Lewis
发明人： Gale L. Hubred , Robert T. Lewis
CPC分类号： C22B47/0081 , B03C1/002
摘要： Fine particulate solids are removed from aqueous liquid previously employed in processing manganese nodules by subjecting the liquid to high gradient magnetic separation.
摘要翻译： 通过对液体进行高梯度磁选分离，将细颗粒固体从先前用于加工锰结核的水性液体中除去。
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公开(公告)号：US5863418A
公开(公告)日：1999-01-26
申请号：US590681
申请日：1996-02-09
申请人： John V. Heyse , Bernard F. Mulaskey , Robert A. Innes , Daniel P. Hagewiesche , Gale L. Hubred , Steven C. Moore , Paul F. Bryan , Robert L. Hise , Steven E. Trumbull , Randall J. Harris , Alan G. Kunze
发明人： John V. Heyse , Bernard F. Mulaskey , Robert A. Innes , Daniel P. Hagewiesche , Gale L. Hubred , Steven C. Moore , Paul F. Bryan , Robert L. Hise , Steven E. Trumbull , Randall J. Harris , Alan G. Kunze
IPC分类号： C10G35/04 , C10G35/095
CPC分类号： C10G35/04 , C10G35/095 , Y10T428/12576
摘要： Disclosed is a method for reforming hydrocarbons comprising contacting the hydrocarbons with a catalyst in a reactor system of improved resistance to carburization and metal dusting under conditions of low sulfur.
摘要翻译： 公开了一种重整烃的方法，包括在低硫条件下使碳氢化合物与催化剂在催化剂体系中接触，该反应器系统具有改善的耐渗碳性和金属粉尘的耐受性。
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10.发明授权
公开(公告)号：US5772890A
公开(公告)日：1998-06-30
申请号：US931214
申请日：1992-08-17
申请人： Gale L. Hubred
发明人： Gale L. Hubred
CPC分类号： C12N1/005 , C07C53/10 , Y10S435/803 , Y10S435/813
摘要： A method is provided for removing an anion from an aqueous liquid, such as a fermentation broth. The aqueous broth is contacted with a water-immiscible ion exchange liquid to extract the anion from the broth. The anion exchange liquid is then back extracted with an aqueous phase, to remove the anion, preferably for other uses.
摘要翻译： 提供了从水性液体如发酵液中除去阴离子的方法。 水性肉汤与水不混溶的离子交换液体接触以从肉汤中提取阴离子。 然后将阴离子交换液体用水相反萃取，以除去阴离子，优选用于其它用途。
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