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    Process for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the intermediates thereof
    2.
    发明授权
    Process for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the intermediates thereof 失效
    制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂的方法及其中间体

    公开(公告)号：US08242264B2

    公开(公告)日：2012-08-14

    申请号：US12601962

    申请日：2008-05-22

    申请人： Fuqiang Zhu ,  Haihong Li ,  Wenzhong Wang ,  Hui Zhang ,  Jingshan Shen

    发明人： Fuqiang Zhu ,  Haihong Li ,  Wenzhong Wang ,  Hui Zhang ,  Jingshan Shen

    IPC分类号： C07D243/14 ,  C07C205/06

    CPC分类号： C07C211/29 ,  C07C209/52 ,  C07C233/13 ,  C07C251/24 ,  C07D243/14

    摘要： The present invention relates to a process for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the intermediates thereof. The present invention provides a compound represented by formula I and a compound represented by formula II, and processes for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine by using the compound represented by formula I, the compound represented by formula II and o-nitrobenzaldehyde. The invention has the advantages of the shorter synthesis steps, easily available raw materials and simple operation. Moreover, the process is economic and safe by avoiding the use of expensive and dangerous lithium aluminum hydride.

    摘要翻译： 本发明涉及一种制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂的方法及其中间体。 本发明提供由式I表示的化合物和由式II表示的化合物，以及通过使用式（I）表示的化合物制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂 I，式II表示的化合物和邻硝基苯甲醛。 本发明具有合成步骤较短，原料易得，操作简单等优点。 此外，通过避免使用昂贵且危险的氢化铝锂，该方法是经济和安全的。

    FLOCCULATION METHOD
    3.
    发明申请
    FLOCCULATION METHOD 审中-公开
    絮凝法

    公开(公告)号：US20110135797A1

    公开(公告)日：2011-06-09

    申请号：US12858758

    申请日：2010-08-18

    申请人： Haihong LI ,  Zhiang ZHOU ,  Ross Sam CHOW ,  Pablo CONTRERAS

    发明人： Haihong LI ,  Zhiang ZHOU ,  Ross Sam CHOW ,  Pablo CONTRERAS

    IPC分类号： B01D21/01 ,  C02F1/52 ,  A23P1/00 ,  E21B43/00 ,  E02B15/10

    CPC分类号： C02F1/56 ,  B01D21/01 ,  B01D2221/04 ,  C02F1/5236

    摘要： A method is taught for producing freely draining flocculated sediment from a suspension comprising finely divided solids in water. The method comprises dispersing, at increasing concentrations, a charged particle hybrid polymer (CPHP) flocculant into the suspension to determine a minimum concentration of CPHP flocculant above which a freely draining flocculated sediment is produced that has a minimum permeability of 1 Darcy. Then, the concentration of dispersed CPHP flocculant in the suspension is maintained at or above the minimum concentration.A method is further provided for separating fine solids and water from a suspension comprising finely divided solids in water. The method involves dispersing, at increasing concentrations, a charged particle hybrid polymer (CPHP) flocculant into the suspension to determine a minimum concentration of CPHP flocculant above which a freely draining flocculated sediment is produced that has a minimum permeability of 1 Darcy. Then, the concentration of dispersed CPHP flocculant in the suspension is maintained at or above the minimum concentration. The dispersion of CPHP flocculant in the suspension is agitated and the solid floccules are then separated from the supernatant liquid.

    摘要翻译： 教导了一种从包含细分散在水中的固体的悬浮液中产生自由排出的絮凝沉淀物的方法。 该方法包括以增加的浓度将带电粒子杂化聚合物（CPHP）絮凝剂分散到悬浮液中以确定CPHP絮凝剂的最小浓度，在该浓度下，产生具有最小渗透性为1达西的自由排出的絮凝沉积物。 然后，悬浮液中分散的CPHP絮凝剂的浓度保持在或低于最低浓度。 还提供了一种从包含细分散的固体在水中的悬浮液中分离细小固体和水的方法。 该方法包括以增加的浓度将带电粒子杂化聚合物（CPHP）絮凝剂分散到悬浮液中以确定CPHP絮凝剂的最小浓度，其中产生具有最小渗透性为1达西的自由排出的絮凝沉积物。 然后，悬浮液中分散的CPHP絮凝剂的浓度保持在或低于最低浓度。 搅拌CPHP絮凝剂在悬浮液中的分散液，然后将固体絮凝物与上清液分离。

    FLOCCULATION METHOD
    4.
    发明申请
    FLOCCULATION METHOD 审中-公开
    絮凝法

    公开(公告)号：US20120138543A1

    公开(公告)日：2012-06-07

    申请号：US13152212

    申请日：2011-06-02

    申请人： Haihong LI ,  Zhiang ZHOU ,  Ross Sam CHOW ,  Pablo CONTRERAS

    发明人： Haihong LI ,  Zhiang ZHOU ,  Ross Sam CHOW ,  Pablo CONTRERAS

    IPC分类号： B01D21/01 ,  C02F1/56

    CPC分类号： C02F1/56 ,  B01D21/01 ,  B01D2221/04 ,  C02F1/5236 ,  C02F2103/10

    摘要： A charged particle polymer hybrid (CPPH) flocculant is taught, comprising sub-micron size charged particles and a polymer which has been polymerized in the presence of the charged particles wherein the intrinsic viscosity of the hybrid polymer flocculant is less than 930 ml/g. A method is provided for producing freely draining flocculated sediment from a suspension comprising finely divided solids in water. The method comprises dispersing, at increasing concentrations, a charged particle polymer hybrid (CPPH) flocculant into the suspension to determine a starting plateau concentration of CPPH flocculant above which concentration no further increase in the solids loading of the produced floccules is observed. Then, the concentration of dispersed CPPH flocculant in the suspension is maintained at or above the starting plateau concentration. A method is further provided for separating fine solids and water from a suspension comprising finely divided solids in water. The method involves dispersing, at increasing concentrations, a charged particle polymer hybrid (CPPH) flocculant into the suspension to determine a starting plateau concentration of CPPH flocculant above which concentration no further increase in the solids loading of the produced floccules is observed. Then, the concentration of dispersed CPPH flocculant in the suspension is maintained at or above the starting plateau concentration. The dispersion of CPPH flocculant in the suspension is agitated and the solid floccules are then separated from the supernatant liquid.

    摘要翻译： 教导了带电粒子聚合物杂化物（CPPH）絮凝剂，其包含亚微米级带电粒子和在带电粒子存在下聚合的聚合物，其中杂化聚合物絮凝剂的特性粘度小于930ml / g。 提供了一种从包含在水中的细分散固体的悬浮液产生自由排出的絮凝沉淀物的方法。 该方法包括以增加的浓度将带电粒子聚合物杂化物（CPPH）絮凝剂分散到悬浮液中以确定CPPH絮凝剂的起始平台浓度，其中观察到所产生的絮凝物的固体负载量不再进一步增加。 然后，悬浮液中分散的CPPH絮凝剂的浓度保持在起始平台浓度以上。 还提供了一种从包含细分散的固体在水中的悬浮液中分离细小固体和水的方法。 该方法包括以增加的浓度将带电粒子聚合物杂化物（CPPH）絮凝剂分散到悬浮液中以确定CPPH絮凝剂的起始平台浓度，其中观察到所产生的絮凝物的固体负载浓度没有进一步增加。 然后，悬浮液中分散的CPPH絮凝剂的浓度保持在起始平台浓度以上。 搅拌CPPH絮凝剂在悬浮液中的分散体，然后将固体絮凝物与上清液分离。

    Motorcycle
    6.
    外观设计
    Motorcycle 有权

    公开(公告)号：USD619934S1

    公开(公告)日：2010-07-20

    申请号：US29347414

    申请日：2009-12-28

    申请人： Haihong Li

    设计人： Haihong Li

    PREPARATION METHODS OF 6-SUBSTITUTED AMINO-3-CYANOQUINOLINE COMPOUNDS AND THE INTERMEDIATES THEREOF
    7.
    发明申请
    PREPARATION METHODS OF 6-SUBSTITUTED AMINO-3-CYANOQUINOLINE COMPOUNDS AND THE INTERMEDIATES THEREOF 有权
    6-取代的氨基-3-氰基喹啉化合物的制备方法及其中间体

    公开(公告)号：US20110263860A1

    公开(公告)日：2011-10-27

    申请号：US13125721

    申请日：2009-10-23

    申请人： Yongjun Mao ,  Jianfeng Li ,  Jin Zheng ,  Zheng Liu ,  Kai Xie ,  Haihong Li ,  Jing Shi ,  Ye Li ,  Jingshan Shen

    发明人： Yongjun Mao ,  Jianfeng Li ,  Jin Zheng ,  Zheng Liu ,  Kai Xie ,  Haihong Li ,  Jing Shi ,  Ye Li ,  Jingshan Shen

    IPC分类号： C07D215/20 ,  C07D215/38 ,  C07C69/78

    CPC分类号： C07C229/64 ,  C07C237/30 ,  C07C255/30 ,  C07D215/56

    摘要： The present invention relates to a method for preparing 6-substituted amino-3-cyanoquinoline compounds (compound A for short) and the intermediates thereof, more particularly, to a compound of the following formula (I), the preparation method thereof, the intermediates thereof and use thereof for preparing the compound A. The compound of the formula (I) is cyclized in the presence of an alkali to give a compound of formula A, wherein W is OH; or the compound of the formula (I) is cyclized in the presence of an alkali, and then chlorinated to give a compound of the formula A, wherein W is Cl. Compared with the known methods in the literature, the method for preparing the compound A from the compound of formula (I) according to the present invention can avoid using high-temperature condition and high boiling point solvents, and is safe and environment-friendly, mild in reaction condition, easy in operation with a high yield and high product purity.

    摘要翻译： 本发明涉及一种制备6-取代氨基-3-氰基喹啉化合物（简称为化合物A）的方法及其中间体，更具体地涉及下式（I）的化合物，其制备方法，中间体 及其用于制备化合物A的用途。式（I）化合物在碱存在下环化，得到式A化合物，其中W为OH; 或式（I）化合物在碱的存在下环化，然后氯化，得到式A化合物，其中W为Cl。 与文献中已知的方法相比，本发明的式（I）化合物制备化合物A的方法可以避免使用高温条件和高沸点溶剂，且安全环保， 反应条件温和，易于操作，产率高，产品纯度高。

    Preparation methods of 6 substituted amino-3 cyanoquinoline compounds and the intermediates thereof
    8.
    发明授权
    Preparation methods of 6 substituted amino-3 cyanoquinoline compounds and the intermediates thereof 有权
    6取代氨基-3-氰基喹啉化合物的制备方法及其中间体

    公开(公告)号：US08481741B2

    公开(公告)日：2013-07-09

    申请号：US13125721

    申请日：2009-10-23

    申请人： Yongjun Mao ,  Jianfeng Li ,  Jin Zheng ,  Zheng Liu ,  Kai Xie ,  Haihong Li ,  Jing Shi ,  Ye Li ,  Jingshan Shen

    发明人： Yongjun Mao ,  Jianfeng Li ,  Jin Zheng ,  Zheng Liu ,  Kai Xie ,  Haihong Li ,  Jing Shi ,  Ye Li ,  Jingshan Shen

    IPC分类号： C07D215/38

    CPC分类号： C07C229/64 ,  C07C237/30 ,  C07C255/30 ,  C07D215/56

    摘要： The present invention relates to a method for preparing 6-substituted amino-3-cyanoquinoline compounds (compound A for short) and the intermediates thereof, more particularly, to a compound of the following formula (I), the preparation method thereof, the intermediates thereof and use thereof for preparing the compound A. The compound of the formula (I) is cyclized in the presence of an alkali to give a compound of formula A, wherein W is OH; or the compound of the formula (I) is cyclized in the presence of an alkali, and then chlorinated to give a compound of the formula A, wherein W is Cl. Compared with the known methods in the literature, the method for preparing the compound A from the compound of formula (I) according to the present invention can avoid using high-temperature condition and high boiling point solvents, and is safe and environment-friendly, mild in reaction condition, easy in operation with a high yield and high product purity.

    摘要翻译： 本发明涉及一种制备6-取代氨基-3-氰基喹啉化合物（简称为化合物A）的方法及其中间体，更具体地涉及下式（I）的化合物，其制备方法，中间体 及其用于制备化合物A的用途。式（I）化合物在碱存在下环化，得到式A化合物，其中W为OH; 或式（I）化合物在碱的存在下环化，然后氯化，得到式A化合物，其中W为Cl。 与文献中已知的方法相比，本发明的式（I）化合物制备化合物A的方法可以避免使用高温条件和高沸点溶剂，且安全环保， 反应条件温和，易于操作，产率高，产品纯度高。

    Process for Preparing 4-Acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the Intermediates Thereof
    9.
    发明申请
    Process for Preparing 4-Acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the Intermediates Thereof 失效
    制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂的方法及其中间体

    公开(公告)号：US20100256358A1

    公开(公告)日：2010-10-07

    申请号：US12601962

    申请日：2008-05-22

    申请人： Fuqiang Zhu ,  Haihong Li ,  Wenzhong Wang ,  Hui Zhang ,  Jingshan Shen

    发明人： Fuqiang Zhu ,  Haihong Li ,  Wenzhong Wang ,  Hui Zhang ,  Jingshan Shen

    IPC分类号： C07D243/14 ,  C07C233/13 ,  C07C251/24 ,  C07C211/29 ,  C07C209/28

    CPC分类号： C07C211/29 ,  C07C209/52 ,  C07C233/13 ,  C07C251/24 ,  C07D243/14

    摘要： The present invention relates to a process for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine and the intermediates thereof. The present invention provides a compound represented by formula I and a compound represented by formula II, and processes for preparing 4-acetyl-2,3,4,5-tetrahydro-benzo[1,4]diazepine by using the compound represented by formula I, the compound represented by formula II and o-nitrobenzaldehyde. The invention has the advantages of the shorter synthesis steps, easily available raw materials and simple operation. Moreover, the process is economic and safe by avoiding the use of expensive and dangerous lithium aluminum hydride.

    摘要翻译： 本发明涉及一种制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂的方法及其中间体。 本发明提供由式I表示的化合物和由式II表示的化合物，以及通过使用式（I）表示的化合物制备4-乙酰基-2,3,4,5-四氢 - 苯并[1,4]二氮杂 I，式II表示的化合物和邻硝基苯甲醛。 本发明具有合成步骤较短，原料易得，操作简单等优点。 此外，通过避免使用昂贵且危险的氢化铝锂，该方法是经济和安全的。

    Processing aids for enhanced hydrocarbon recovery from oil sands, oil shale and other petroleum residues
    10.
    发明申请
    Processing aids for enhanced hydrocarbon recovery from oil sands, oil shale and other petroleum residues 审中-公开
    加工助剂用于从油砂，油页岩和其他石油残渣中提高烃回收率

    公开(公告)号：US20050194292A1

    公开(公告)日：2005-09-08

    申请号：US10947076

    申请日：2004-09-22

    申请人： Jan Beetge ,  Tshitende Kasongo ,  Bradley Komishke ,  Haihong Li ,  Jun Long ,  Jacob Masliyah ,  Petrus Venter ,  Sanyi Wang ,  Zhenghe Xu

    发明人： Jan Beetge ,  Tshitende Kasongo ,  Bradley Komishke ,  Haihong Li ,  Jun Long ,  Jacob Masliyah ,  Petrus Venter ,  Sanyi Wang ,  Zhenghe Xu

    IPC分类号： C10G1/04 ,  C10G33/04

    CPC分类号： C10G33/04 ,  C10G1/047

    摘要： A method of improving hydrocarbon recovery from oil sands, oil shale, and petroleum residues includes adding a polymeric or nonpolymeric processing aid capable of sequestering cations, such as the multivalent calcium, magnesium and iron cations. The hydrocarbons are preferably contacted with the processing aid before a primary separation of the hydrocarbons in order to increase bitumen recovery. A processing aid is provided in an effective amount to increase the liberation of the hydrocarbons from inorganic solids, particularly when the source is a poor processing ore. Preferred processing aids include citric acid or a polymeric acid selected from polyacrylic acid, polymethacrylic acid, salts of these acids, partial salts of these acids, and combinations thereof. The processing aids significantly increase the hydrocarbon recovery typically with concentrations less than 50 ppm and the polymeric processing aids can also provide beneficial flocculation of solids in tailings slurry.

    摘要翻译： 从油砂，油页岩和石油残渣中提高烃回收的方法包括加入能够螯合阳离子的聚合或非聚合加工助剂，例如多价钙，镁和铁阳离子。 烃优选在烃的一次分离之前与加工助剂接触，以增加沥青回收率。 提供了有效量的加工助剂以增加烃从无机固体中的释放，特别是当源是不良的加工矿石时。 优选的加工助剂包括柠檬酸或选自聚丙烯酸，聚甲基丙烯酸，这些酸的盐，这些酸的部分盐及其组合的聚合酸。 加工助剂通常以低于50ppm的浓度显着增加烃回收率，而聚合加工助剂也可以在尾矿浆料中提供有益的固体絮凝。