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1.发明授权公开(公告)号：US06951957B2
公开(公告)日：2005-10-04
申请号：US10421924
申请日：2003-04-24
IPC分类号： C07C51/58 , C07B39/00 , C07C51/60 , C07C53/50 , C07C59/135 , C07C67/287 , C07C67/307 , C07C69/63 , C07C69/708 , C07D317/16 , C07D317/42 , C08F16/24
CPC分类号： C07D317/42 , C07B39/00 , C07C51/60 , C07C59/135 , C07C67/08 , C07C67/11 , C07C67/287 , C07C69/63 , C07C69/708 , C07C2601/14 , C07C53/50 , C07C69/734
摘要： The invention provides a process for producing a fluorine-containing compound from an inexpensive material.Namely, Compound I such as RACH2OH is reacted with Compound II such as XCORB to form Compound III such as RACH2OCORB, followed by fluorination in a liquid phase to form Compound IV such as RAFCF2OCORBF, which is converted to Compound V such as RAFCOF and/or Compound VI such as RBFCOF. RA is an alkyl group or the like, RB is a perhalogenoalkyl group or the like, RAF and RBF are fluorinated RA and RB, and X is halogen.
摘要翻译： 本发明提供从廉价材料制备含氟化合物的方法。 也就是说，将化合物I如R“CH 2 OH与化合物II如XCOR B”反应形成化合物III，例如R SUP 然后在液相中氟化以形成化合物IV，例如R AF AF＆lt; SUB＆gt;＆lt; 将其转化为化合物V，例如R AFFFF和/或化合物VI如R BF BF， 中粮 R A是烷基等，R B是全卤代烷基等，R AF和R BF， R 2是氟化的R A和R B，并且X是卤素。
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公开(公告)号：US20050207714A1
公开(公告)日：2005-09-22
申请号：US11075441
申请日：2005-03-09
CPC分类号： G02B6/02038 , G02B6/03627
摘要： A plastic optical fiber low in attenuation in a high order mode and small in mode dispersion, is presented. The plastic optical fiber comprises at least a core and a clad surrounding the core, characterized in that the core has a refractive index which gradually decreases from the core center towards the outside in the radial direction of the plastic optical fiber, and the refractive index of the clad is lower than the refractive index of the core center and higher than the refractive index of the core periphery.
摘要翻译： 提出了一种高阶模式衰减量小，模式色散小的塑料光纤。 所述塑料光纤至少包括芯和围绕所述芯的包层，其特征在于，所述芯具有从所述芯中心向所述塑料光纤的径向方向逐渐减小的折射率，并且所述折射率 包层低于芯心的折射率，高于芯周的折射率。
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公开(公告)号：US07071272B2
公开(公告)日：2006-07-04
申请号：US10307388
申请日：2002-12-02
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masakuni Sato , Hidenobu Murofushi , Koichi Yanase , Yasuhiro Suzuki
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masakuni Sato , Hidenobu Murofushi , Koichi Yanase , Yasuhiro Suzuki
IPC分类号： C08F16/24
CPC分类号： C07C43/17 , C07C41/18 , C07C41/28 , C07C43/172 , C07C2601/14
摘要： The present invention provides a method for preparing a compound of CF3CF2CF2OCF═CF2 by pyrolyzing a compound expressed by CF3CF2CF2OCF(CF3)COOCF2CF(CF3)OCF2CF2CF3 in a gas phase at a temperature of from 200° C. to 500° C.
摘要翻译： 本发明提供了通过以下方法制备CF 3 CF 2 CF 2 OCF-CF 2的化合物的方法： 热解由CF 3 CF 2 CO 2 CF 2（CF 3）COOCF 2表示的化合物， / CF 2 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3在气相中在温度为 从200℃至500℃
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公开(公告)号：US06448452B2
公开(公告)日：2002-09-10
申请号：US09841592
申请日：2001-04-25
IPC分类号： C07C4100
CPC分类号： C07C43/123 , C07C43/17 , C08F16/32 , C08F36/18 , C08F36/20
摘要： A polymer which contains monomer units formed by polymerization of a fluorine-containing diene of formula 1: CF2═CF(CF2)nCXYOCF═CF2 Wherein X and Y are hydrogen and chlorine, hydrogen and-bromine, hydrogen and iodine, fluorine and chlorine, fluorine and bromine, fluorine and iodine, chlorine and bromine, chlorine and iodine, bromine and bromine, bromine and iodine, or iodine and iodine and n is an integer from 1 to 3.
摘要翻译： 含有由式1的含氟二烯聚合形成的单体单元的聚合物：其中X和Y分别是氢和氯，氢和溴，氢和碘，氟和氯，氟和溴，氟和碘，氯 和溴，氯和碘，溴和溴，溴和碘，或碘和碘，n是1至3的整数。
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5.发明授权
公开(公告)号：US5916971A
公开(公告)日：1999-06-29
申请号：US659365
申请日：1996-06-06
CPC分类号： G02B6/02038 , G02B1/046
摘要： A graded-refractive-index optical plastic material composed of an amorphous fluoropolymer (a) which has substantially no C--H bond and at least one material (b) which has substantially no C--H bond and differs from the fluoropolymer (a) in refractive index by at least 0.001, wherein the material (b) is distributed in the fluoropolymer (a) so as to have a concentration gradient in a specific direction, and the optical plastic material has a glass transition temperature which is substantially uniform throughout it.
摘要翻译： 由基本上没有CH键的无定形含氟聚合物（a）和至少一种基本上没有CH键的材料（b）组成的渐变折射率光学塑料材料，其折射率与氟聚合物（a）的不同在于 至少0.001，其中所述材料（b）分布在所述含氟聚合物（a）中以具有在特定方向上的浓度梯度，并且所述光学塑料材料具有在其中基本均匀的玻璃化转变温度。
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6.发明授权
公开(公告)号：US5760139A
公开(公告)日：1998-06-02
申请号：US659867
申请日：1996-06-07
CPC分类号： G02B6/02038 , B29C39/006 , B29D11/00682 , G02B1/046 , B29C39/025 , B29C39/028 , B29K2995/0031 , G02B6/02033
摘要： A graded-refractive-index optical plastic material composed of an amorphous fluoropolymer (a) which substantially has no C-H bond and at least one material (b) which differs from the fluoropolymer (a) in refractive index by at least 0.001, wherein the material (b) is distributed in the fluoropolymer (a) so as to have a concentration gradient in a specific direction.
摘要翻译： 由基本上没有CH键的无定形含氟聚合物（a）和折射率不同于氟聚合物（a）的至少一种材料（b）组成的渐变折射率光学塑料材料至少为0.001，其中材料 （b）分布在含氟聚合物（a）中以具有特定方向的浓度梯度。
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7.发明授权公开(公告)号：US07083705B2
公开(公告)日：2006-08-01
申请号：US10915423
申请日：2004-08-11
IPC分类号： C07C51/04
CPC分类号： C07D317/42 , C07B39/00 , C07C51/60 , C07C59/135 , C07C67/08 , C07C67/11 , C07C67/287 , C07C69/63 , C07C69/708 , C07C2601/14 , C07C53/50 , C07C69/734
摘要： The invention provides a process for producing a fluorine-containing compound from an inexpensive material.Namely, Compound I such as RACH2OH is reacted with Compound II such as XCORB to form Compound III such as RACH2OCORB, followed by fluorination in a liquid phase to form Compound IV such as RAFCF2OCORBF, which is converted to Compound V such as RAFCOF and/or Compound VI such as RBFCOF. RA is an alkyl group or the like, RB is a perhalogenoalkyl group or the like, RAF and RBF are fluorinated RA and RB, and X is halogen.
摘要翻译： 本发明提供从廉价材料制备含氟化合物的方法。 也就是说，将化合物I如R“CH 2 OH与化合物II如XCOR B”反应形成化合物III，例如R SUP 然后在液相中氟化以形成化合物IV，例如R AF AF＆lt; SUB＆gt;＆lt; 将其转化为化合物V，例如R AFFFF和/或化合物VI如R BF BF， 中粮 R A是烷基等，R B是全卤代烷基等，R AF和R BF， R 2是氟化的R A和R B，并且X是卤素。
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公开(公告)号：US07058271B2
公开(公告)日：2006-06-06
申请号：US11075441
申请日：2005-03-09
IPC分类号： G02B6/028
CPC分类号： G02B6/02038 , G02B6/03627
摘要： A plastic optical fiber low in attenuation in a high order mode and small in mode dispersion, is presented. The plastic optical fiber comprises at least a core and a clad surrounding the core, characterized in that the core has a refractive index which gradually decreases from the core center towards the outside in the radial direction of the plastic optical fiber, and the refractive index of the clad is lower than the refractive index of the core center and higher than the refractive index of the core periphery.
摘要翻译： 提出了一种高阶模式衰减量小，模式色散小的塑料光纤。 所述塑料光纤至少包括芯和围绕所述芯的包层，其特征在于，所述芯的折射率在塑料光纤的径向方向上从芯心中心向外逐渐减小，折射率 包层低于芯心的折射率，高于芯周的折射率。
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9.发明申请PROCESS FOR PRODUCING A FLUORINATED ESTER, A FLUORINATED ACYL FLUORIDE AND A FLUORINATED VINYL ETHER 有权氟化氟化物，氟化氟乙烯和氟化乙烯醚的制备方法公开(公告)号：US20050261516A1
公开(公告)日：2005-11-24
申请号：US10619784
申请日：2003-07-16
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Hidenobu Murofushi , Masakuni Sato , Masahiro Ito , Koichi Yanase , Yasuhiro Suzuki
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Hidenobu Murofushi , Masakuni Sato , Masahiro Ito , Koichi Yanase , Yasuhiro Suzuki
CPC分类号： C07C67/287 , C07C41/24 , C07C51/60 , C07C67/03 , C07C67/14 , C07C59/135 , C07C69/708 , C07C69/63 , C07C43/17
摘要： A process for producing a fluorinated ester through a small number of steps, is presented. The process for producing a fluorinated ester, comprises a transesterification step in which RAF—COOCF2—RAF and RA—CH2OH are subjected to a transesterification reaction to obtain RAF—COOCH2—RA, and a fluorination step in which the obtained compound is fluorinated to obtain a reaction product containing RAF—COOCF2—RAF. Here, in the formulae, RA is a monovalent organic group, and RAF is the same group as RA or a monovalent organic group obtained by fluorination of RA.
摘要翻译： 提出了通过少量步骤生产氟化酯的方法。 氟化酯的制备方法包括酯交换步骤，其中R AF -OCOCF 2 -R AF和R A A < / O 2 CH 2 OH进行酯交换反应，得到R AF-COOCH 2 -R A A / O >和氟化步骤，其中所得化合物被氟化以获得含有R AF -OCOCF 2 -R AF的反应产物。 这里，在式中，R A A为一价有机基团，R AF为与R A A或单价有机基团相同的基团 通过R A A的氟化获得。
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10.发明申请公开(公告)号：US20050020855A1
公开(公告)日：2005-01-27
申请号：US10915423
申请日：2004-08-11
IPC分类号： C07C51/58 , C07B39/00 , C07C51/60 , C07C53/50 , C07C59/135 , C07C67/287 , C07C67/307 , C07C69/63 , C07C69/708 , C07D317/16 , C07D317/42 , C08F16/24 , C07C53/38
CPC分类号： C07D317/42 , C07B39/00 , C07C51/60 , C07C59/135 , C07C67/08 , C07C67/11 , C07C67/287 , C07C69/63 , C07C69/708 , C07C2601/14 , C07C53/50 , C07C69/734
摘要： The invention provides a process for producing a fluorine-containing compound from an inexpensive material. Namely, Compound I such as RACH2OH is reacted with Compound II such as XCORB to form Compound III such as RACH2OCORB, followed by fluorination in a liquid phase to form Compound IV such as RAFCF2OCORBF, which is converted to Compound V such as RAFCOF and/or Compound VI such as RBFCOF. RA is an alkyl group or the like, RB is a perhalogenoalkyl group or the like, RAF and RBF are fluorinated RA and RB, and X is halogen.
摘要翻译： 本发明提供从廉价材料制备含氟化合物的方法。 也就是说，化合物I如R“A CH 2 OH与化合物II例如XCOR B反应形成化合物III，例如R”A CH 2 OCOR B“，然后在液相中氟化形成化合物IV，例如 转化为化合物V如R AFF和/或化合物VI如R“COF”的CF 2 OCOR
。 R A是烷基等，R B是全卤代烷基等，R AF和R B均为氟化的R A和R B，X是卤素。
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