Abstract:
Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.
Abstract:
The invention relates to processes for producing nanoparticles, especially pigment particles, comprising the following steps: i) bringing a base substance (1) into the gas phase, ii) generating particles by cooling or reacting the gaseous base substance (1), and iii) applying electrical charge to the particles during particle generation in step ii) in a nanoparticle generation apparatus. The invention further relates to apparatus for producing nanoparticles, having a feed line (28) for transporting the gas stream (29) into the apparatus, a particle generation and charging area for substantially simultaneous generation and charging of nanoparticles, and a takeoff line (30) for transporting the charged nanoparticles from the particle generation and charging area.
Abstract:
An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio Hi of the distance hi from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downward-extending tube (5) with the wall of the middle section (3b) to the diameter di of the downward-extending tube (5) is from 3 to 8, in particular from 4 to 7.
Abstract translation:用于烯烃聚合的装置,特别是乙烯,包括气相流化床反应器(1),连接到反应器的再循环气体管线(2),用于排出和再循环包含未聚合烯烃的循环气流和 旋流器(3),其位于循环气体管线中,用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒,旋风分离器包括具有基本上垂直的中心轴线的上部分(3a),其上壁延伸 沿着旋转对称体并且设置有相对于中心轴线偏心布置的旋风入口(4),邻近上部(3a)并且其壁沿旋转对称体延伸的中间部分(3b) 用于排出邻近中间部分(3b)并且其壁延伸的再循环气体沉淀的固体颗粒的下部分(3c) 旋转对称体和基本上轴向对称地延伸到上部的管(5)以及适当的中间部分用于排出已经没有颗粒的循环气体。 根据本发明,与从下游进入旋风分离器的管(5)的下端距离h i i的距离h i i的比例H i 向下延伸的管(5)的壁与中间部分(3b)的壁与向下延伸的管(5)的直径d iI i的假想延伸为3至 8,特别是4到7。