Process for synthesizing a palladium replenisher for electroplating baths
    3.
    发明授权
    Process for synthesizing a palladium replenisher for electroplating baths 有权
    用于合成电镀浴的钯补充剂的方法

    公开(公告)号:US06346222B1

    公开(公告)日:2002-02-12

    申请号:US09323607

    申请日:1999-06-01

    IPC分类号: C01G5500

    摘要: This invention provides a process of making a palladium replenisher comprising a complex of palladium tetraammine sulfate. The process includes distilling a palladium nitrate solution at a temperature maintained at or below about 115° C. Palladium sulfate and ammonium hydroxide are then added to make the palladium tetraamine sulfate replenisher from solution. The replenisher of the invention is used to replenish depleted palladium during palladium electroplating to maintain the palladium concentration in the bath within from about 5 to about 10 weight percent of recommended plating bath levels.

    摘要翻译: 本发明提供一种制备包含四氨基硫酸钯复合物的钯补充剂的方法。 该方法包括在保持在约115℃或低于约115℃的温度下蒸馏出硝酸钯溶液。然后加入硫酸钯和氢氧化铵以从溶液中制备四胺硫酸钯补充剂。 本发明的补充剂用于在钯电镀期间补充贫化的钯,以将浴中的钯浓度保持在推荐的电镀浴水平的约5至约10重量%内。